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46749090122
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note
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2 (3 × 30 ml), and the extracts were dried over anhydrous sodium sulfate. Light yellow oil was obtained. The oil was then taken in 50 ml ethanol and precipitated with 48% HBr (4 ml) as its HBr salt: L · 8HBr, yield: 60%.
-
-
-
-
30
-
-
46749102592
-
-
note
-
-1): 3441(br), 3165(br), 2927(m), 2876(m), 1638(m), 1469(s), 1450(vs), 1387(s), 1167(w), 1071(m), 1054(m), 966(m), 805(w), 740(m), 706(w).
-
-
-
-
31
-
-
46749121878
-
-
note
-
-1): 3423(br), 3198(br), 2924(m), 2873(m), 1702(w), 1638(m), 1553(m), 1444(s), 1364(s), 1161(m), 1071(m), 995(m), 802(w), 703(w).
-
-
-
-
32
-
-
46749093441
-
-
note
-
2 = 0.1244 (all data).
-
-
-
-
33
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37049096497
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35
-
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46749096447
-
-
note
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2 = 0.2195(all data).
-
-
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