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+) shows five broad signals at 2.58 (4H), 2.94 (4H) (hydrogen atoms of the ethylenic chains linking two nitrogen atoms), 3.00 (4H), 3.70 (4H) (ethylenic chains linking a nitrogen and an oxygen), and 3.80 ppm (s, 4H) (ethylenic chains linking two oxygens). The spectrum recorded on a MeOD solution containing Zn(II), L, and NaOH in equimolecular ratio shows analogous features with broad resonances at 2.67 (4H), 3.00 (4H), 3.05 (4H), 3.75 (4H), and 3.80 ppm (s, 4H).
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