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Volumn 6, Issue 19, 2004, Pages 3265-3268

Microwave-assisted preparation of aryltetrazoleboronate esters

Author keywords

[No Author keywords available]

Indexed keywords

BORONIC ACID DERIVATIVE; ESTER DERIVATIVE; TETRAZOLE DERIVATIVE;

EID: 4644296039     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol048896q     Document Type: Article
Times cited : (41)

References (48)
  • 1
    • 0035813242 scopus 로고    scopus 로고
    • For recent reviews, see: (a) Perreux, L.; Loupy, A. Tetrahedron 2001, 57, 9199-9223. (b) Lidstrom, P.; Tierney, J.; Wathey, B.; Westman, J. Tetrahedron 2001, 57, 9225-9283. (c) Lew, A.; Krutzik, P. O.; Hart, M. E.; Chamberlin, A. R. J. Comb. Chem. 2002, 4, 95-105. (d) Santagada, V.; Perissutti, E.; Caliendo, G. Curr. Med. Chem. 2002, 9, 1251-1283. (e) Mavandadi, F.; Lidstrom, P. Curr. Top. Med. Chem. 2004, 4, 773-792.
    • (2001) Tetrahedron , vol.57 , pp. 9199-9223
    • Perreux, L.1    Loupy, A.2
  • 2
    • 0035813244 scopus 로고    scopus 로고
    • For recent reviews, see: (a) Perreux, L.; Loupy, A. Tetrahedron 2001, 57, 9199-9223. (b) Lidstrom, P.; Tierney, J.; Wathey, B.; Westman, J. Tetrahedron 2001, 57, 9225-9283. (c) Lew, A.; Krutzik, P. O.; Hart, M. E.; Chamberlin, A. R. J. Comb. Chem. 2002, 4, 95-105. (d) Santagada, V.; Perissutti, E.; Caliendo, G. Curr. Med. Chem. 2002, 9, 1251-1283. (e) Mavandadi, F.; Lidstrom, P. Curr. Top. Med. Chem. 2004, 4, 773-792.
    • (2001) Tetrahedron , vol.57 , pp. 9225-9283
    • Lidstrom, P.1    Tierney, J.2    Wathey, B.3    Westman, J.4
  • 3
    • 0041461964 scopus 로고    scopus 로고
    • For recent reviews, see: (a) Perreux, L.; Loupy, A. Tetrahedron 2001, 57, 9199-9223. (b) Lidstrom, P.; Tierney, J.; Wathey, B.; Westman, J. Tetrahedron 2001, 57, 9225-9283. (c) Lew, A.; Krutzik, P. O.; Hart, M. E.; Chamberlin, A. R. J. Comb. Chem. 2002, 4, 95-105. (d) Santagada, V.; Perissutti, E.; Caliendo, G. Curr. Med. Chem. 2002, 9, 1251-1283. (e) Mavandadi, F.; Lidstrom, P. Curr. Top. Med. Chem. 2004, 4, 773-792.
    • (2002) J. Comb. Chem. , vol.4 , pp. 95-105
    • Lew, A.1    Krutzik, P.O.2    Hart, M.E.3    Chamberlin, A.R.4
  • 4
    • 0036294671 scopus 로고    scopus 로고
    • For recent reviews, see: (a) Perreux, L.; Loupy, A. Tetrahedron 2001, 57, 9199-9223. (b) Lidstrom, P.; Tierney, J.; Wathey, B.; Westman, J. Tetrahedron 2001, 57, 9225-9283. (c) Lew, A.; Krutzik, P. O.; Hart, M. E.; Chamberlin, A. R. J. Comb. Chem. 2002, 4, 95-105. (d) Santagada, V.; Perissutti, E.; Caliendo, G. Curr. Med. Chem. 2002, 9, 1251-1283. (e) Mavandadi, F.; Lidstrom, P. Curr. Top. Med. Chem. 2004, 4, 773-792.
    • (2002) Curr. Med. Chem. , vol.9 , pp. 1251-1283
    • Santagada, V.1    Perissutti, E.2    Caliendo, G.3
  • 5
    • 2342474593 scopus 로고    scopus 로고
    • For recent reviews, see: (a) Perreux, L.; Loupy, A. Tetrahedron 2001, 57, 9199-9223. (b) Lidstrom, P.; Tierney, J.; Wathey, B.; Westman, J. Tetrahedron 2001, 57, 9225-9283. (c) Lew, A.; Krutzik, P. O.; Hart, M. E.; Chamberlin, A. R. J. Comb. Chem. 2002, 4, 95-105. (d) Santagada, V.; Perissutti, E.; Caliendo, G. Curr. Med. Chem. 2002, 9, 1251-1283. (e) Mavandadi, F.; Lidstrom, P. Curr. Top. Med. Chem. 2004, 4, 773-792.
    • (2004) Curr. Top. Med. Chem. , vol.4 , pp. 773-792
    • Mavandadi, F.1    Lidstrom, P.2
  • 42
    • 4644293969 scopus 로고    scopus 로고
    • note
    • 2 273.1523, found 273.1519.
  • 45
    • 4644309120 scopus 로고    scopus 로고
    • note
    • The use of 0.05% trifluoroacetic acid as a modifier resulted in hydrolysis of the pinacol ester functionality, during HPLC analysis.
  • 46
    • 4644252229 scopus 로고    scopus 로고
    • note
    • Typical Aqueous Workup. After completion of the reaction, the solvent was removed and the residue was taken up in ether. The ether was extracted with 2 N NaOH, and the combined aqueous layers were washed with ether. The aqueous layer was then acidified to pH 4, and the resulting precipitate was collected.


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