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Volumn 130, Issue 26, 2008, Pages 8120-8121

Effect of water on the ionothermal synthesis of molecular sieves

Author keywords

[No Author keywords available]

Indexed keywords

ADSORBENT; ALUMINUM PHOSPHATE; DESICCANT; IONIC LIQUID; MOLECULAR SIEVE; WATER;

EID: 46049084199     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja802207p     Document Type: Article
Times cited : (111)

References (31)
  • 3
    • 0037142065 scopus 로고    scopus 로고
    • (c) Davis, M. E. Nature 2002, 417, 813.
    • (2002) Nature , vol.417 , pp. 813
    • Davis, M.E.1
  • 7
  • 22
    • 46049111173 scopus 로고    scopus 로고
    • General synthesis procedure: a plastic beaker was charged with IL (0.1 mol, NH4H2PO4, and AlOOH. NH4F and/or H2O was added if required. The beaker was then sealed with laboratory film and stirred electromagnetically at 80°C in an oil bath for 30 min. The mixture was crystallized in the same microwave system as reported elsewhere,5a ramping the temperature to 200°C in 5 min and keeping the system under ambient pressure for required time. For comparison, the crystallization process was also performed in sealed Teflon-line autoclaves (30 mL) under conventional heating at 200°C. After the mixture was cooled to room temperature, the solid was filtered, washed thoroughly with distilled water and ethanol, and dried at 110°C overnight. All the solid products were characterized by powder X-ray diffraction, and the data were normalized to 100, corresponding to complete crystallization. Each curve represent
    • 4-5.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.