Development and validation of sensitive methods for determination of sibutramine hydrochloride monohydrate and direct enantiomeric separation on a protein-based chiral stationary phase

Journal of AOAC International

Volumn 91, Issue 3, 2008, Pages 572-579

  Singh, Anil Kumar ^a   García, Pedro López ^a   Gomes, Fábio Pereira ^a   Yano, Helena Miyoco ^b   Auricchio, Mariangela Tirico ^b   Kedor Hackmann, Erika Rosa Maria ^a   Santoro, Maria Inês Rocha Miritello ^a  

^a UNIVERSITY OF SÃO PAULO   (Brazil)

^b INSTITUTO ADOLFO LUTZ   (Brazil)

Author keywords

[No Author keywords available]

Indexed keywords

CHROMATOGRAPHIC ANALYSIS; SEPARATION;

CHIRAL STATIONARY PHASE (CSP); DIRECT ENANTIOMERIC SEPARATION; SENSITIVE METHODS;

PHASE SEPARATION;

ANOREXIGENIC AGENT; CYCLOBUTANE DERIVATIVE; SIBUTRAMINE;

ARTICLE; CHEMISTRY; COMPARATIVE STUDY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; METHODOLOGY; QUALITY CONTROL; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; SOLID PHASE EXTRACTION; STANDARD; STATISTICS; STEREOISOMERISM; ULTRAVIOLET SPECTROPHOTOMETRY; VALIDATION STUDY;

APPETITE DEPRESSANTS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CYCLOBUTANES; HUMANS; QUALITY CONTROL; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SOLID PHASE EXTRACTION; SPECTROPHOTOMETRY, ULTRAVIOLET; STEREOISOMERISM;

EID: 45849138821     PISSN: 10603271     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (13)

1. Elfhag, K., Rössner, S., Barkeling, B., & Rooth, P. (2005) Pharmacol. Res. 51, 159-163
2. Heusser, K., Tank, J., Diedrich, A., Engeli, S., Klaua, S., Krüger, N., Strauss, A., & Stoffels, G. (2006) Clin. Pharmacol. Ther. 79, 500-508
3. Sucar, D.D., Sougey, E.B., & Neto, J.B. (2002) Rev. Bras. Psiquiatr. 24, 30-33
4. Thevis, M., Sigmund, G., Schiffer, A.K., & Schaenzer, W. (2006) Eur. J. Mass. Spectrom. 12, 129-136
5. Ding, L., Hao, X., Huang, X., & Zhang, S. (2003) Anal. Chim. Acta 492, 241-248
6. Chen, J., Lu, W., Zhang, Q., & Jiang, X. (2003) J. Chromatogr. B 785, 197-203
7. Radhakrishna, T., Narayana, CL., Rao, D.S., Vyas, K., & Reddy, GO. (2000) J. Pharm. Biomed. Anal. 11, 627-639
8. Link, M., Novotna, R., Suchanova, B., Skalova, L., Wsol, V., & Szotakova, B. (2005) J. Pharm. Pharmacol. 57, 405-410
9. Segall, A.I., Collado, E.A., Ricci, R.A., & Pizzorno, M.T. (2003) J. Liq. Chromatogr. Relat. Technol. 26, 977-986
10. Valarmathi, R., Sundari, S.K.K., Puratchikody, A., George, S., Kumar, S.S., & Ruckmani, K. (2003) Indian J. Pharm. Sci. 65, 647-648
11. ICH Q2(R1) (1996) Validation of Analytical Procedures: Text and Methodology, International Conference on Harmonization, Geneva, Switzerland
12. United States Pharmacopeia (2006) 29th Ed., United States Pharmacopeial Convention Inc., Rockville, MD, p. 3050
13. Official Methods of Analysis ( 1990) 15th Ed., AOAC INTERNATIONAL, Gaithersburg, MD