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In comparison of related compounds synthesized in our laboratory, the hydroxy proton of the anti-adduct appears at higher field than that of the syn-adduct. On the other hand, the signals of the methin protons at both C2 and C3 positions were shifted more down-field in the anti-adduct than in the syn-adduct.
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In comparison of related compounds synthesized in our laboratory, the hydroxy proton of the anti-adduct appears at higher field than that of the syn-adduct. On the other hand, the signals of the methin protons at both C2 and C3 positions were shifted more down-field in the anti-adduct than in the syn-adduct.
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26
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Since Forsyth's one-pot sulfonylation and cyclization were not effective for our substrate, we employed'step-wise reactions.
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Since Forsyth's one-pot sulfonylation and cyclization were not effective for our substrate, we employed'step-wise reactions.
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8 701.4489, found 701.4492.
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8 701.4489, found 701.4492.
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