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2 was added. The oxidation reaction was monitored by taking 1 mL samples after reaction times of 0.5, 1.0 and 3.0 h. These samples were analysed by gas chromatography using an internal standard (cyclopentanone for cyclohexane and 1,3-dibromobenzene for cyclooctene). All reactions were performed in triplicate.
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14
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44749089930
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note
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2 as the substrate is in large excess compared to the oxidant.
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2 = 0.3525 [all data].
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