Retention behaviour of selected alkaloids on bonded stationary phases by HPLC

Journal of Liquid Chromatography and Related Technologies

Volumn 27, Issue 14, 2004, Pages 2247-2267

  Waksmundzka Hajnos, Monika ^a   Petruczynik, Anna ^a  

^a MEDICAL UNIVERSITY OF LUBLIN   (Poland)

Author keywords

Alkaloids; HPLC; NP systems; Polar bonded stationary phases; Retention behaviour; RP systems; Selectivity

Indexed keywords

CHEMICAL BONDS; COMPOSITION; LIQUID CHROMATOGRAPHY; MIXTURES; PH;

ALKALOIDS; ELUENTS; REVERSED PHASE SYSTEMS; STATIONARY PHASES;

CHEMICAL COMPOUNDS;

2 PROPANOL; ACETONITRILE; ALKALOID; AMMONIA; HEPTANE; METHANOL; SILICON DIOXIDE;

ARTICLE; CHEMICAL BOND; CORRELATION ANALYSIS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; INTERMETHOD COMPARISON; PH; REVERSED PHASE LIQUID CHROMATOGRAPHY; SEPARATION TECHNIQUE;

EID: 4444317565     PISSN: 10826076     EISSN: None     Source Type: Journal    
DOI: 10.1081/JLC-200025724     Document Type: Article

References (29)

1. Houghton, P.J. Chromatography of the chromone and flavonoid alkaloids. J. Chromatogr. A 2002, 967, 75-84.
2. Molyneux, R.J.; Gardner, D.R.; James, L.F.; Colegate, S.M. Polyhydroxy alkaloids: chromatographic analysis. J. Chromatogr. A 2002, 967, 57-74.
3. McCalley, D.V. Analysis of the Cinchona alkaloids by high performance liquid chromatography and other separation techniques. J. Chromatogr. A. 2002, 967, 1-19.
4. Friedman, M.; Kozuke, N.; Harden, L. A. Preparation and characterization of acid hydrolysis products of the tomato glycoalkaloid. J. Agric. Food Chem. 1998, 46, 2096-2101.
5. El Shazly, A.; El Dominaty, M.; Witte, L.; Wink, M. Pyrrolizidine alkaloids in members of the Boraginaceae from Sinai (Egypt). Biochem. Systematics Ecol. 1998, 26, 619-636.
6. Zwickenpflug, W.; Meger, M.; Richter, E. Occurrence of the tobacco alkaloid myosmine in nuts and nut products of Arachis hypogea and Corylus avellana. J. Agric. Food Chem. 1998, 46, 2703-2706.
7. Ma, X.Q.; Jiang, S.H.; Zhu, D.Y. Alkaloid patterns in Huperzia and some related genera of Lycopodiaceae Sensu Lato occurring in China and their contribution to classification. Biochem. Systematics Ecol. 1998, 26, 723-728.
8. Yuan, L.M.; Zi, M.; Ai, P.; Chen, X.X.; Li, Z.Y.; Fu, R.N.; Zhang, T.Y. Versatile two-phase solvent system for alkaloid separation by high-speed counter-current chromatography. J. Chromatogr. A 2001, 927, 92-96.
9. Cardoso, C.A.L.; Vilegas, W.; Honda, N.K. Qualitative determination of indole alkaloids, triterpenoids and steroids of Tabernaemontana hilariana. J. Chromatogr. A 1998, 808, 264-268.
10. Yang, F.; Quan, J.; Zhang, T.; Ito, Y. Preparative separation of alkaloids from the root of Sophora flavescens Ait by pH-zone-refining counter-current chromatography. J. Chromatogr. A 1998, 822, 316-320.
11. Then, M.; Szentmihalyi, K.; Sarközi, A. Effect of sample handling on alkaloid and mineral content of aqueous extracts of greater celandine (Chelidonium majus L.). J. Chromatogr. A 2000, 889, 6974.
12. Verotta, L.; Peterlongo, F.; Elisabetsky, E.; Amador, T.A.; Nunes, D.S. High performance liquid chromatography-diode array detection-tandem mass spectrometry analyses of the alkaloid extracts of Amazon Psychotria species. J. Chromatogr. A 1999, 841, 165-176.
13. Sun, S.W.; Kuo, C.H.; Lee, S.S.; Chen, C.K. Determination of bisbenzylisoquinoline alkaloids by high performance liquid chromatography (II). J. Chromatogr. A 2000, 891, 189-194.
14. Bajad, S.; Johri, R.K.; Singh, K.; Singh, J.; Bedi, K.L. Sample high performance liquid chromatography method for the simultaneous determination of ketoconazole and piperine in rat plasma and hepatocyle culture. J. Chromatogr. A 2002, 949, 43-47.
15. Rosso, A.; Zuccaro, S. Determination of alkaloids from the colchicine family by reversed-phase high performance liquid chromatography. J. Chromatogr. A 1998, 825, 96-101.
16. Tikhomiroff, C.; Jolicoeur, M. Screening of Catharanthus roseus secondary metabolites by high performance liquid chromatography. J. Chromatogr. A 2002, 955, 87-93.
17. Valverde, J.; Tamayo, G.; Hesse, M. β-Carboline monoterpenoid glucosides from Palicourea adusta. Phytochemistry 1999, 52 (8), 1485-1489.
18. Yang, F.; Ito, Y. Preparative separation of lappaconitine, ranaconitine, W-deacetylloppaconitine and N-deacetylranaconitine from crude alkaloids of sample Aconitum sinomontanum Nokai by high-speed counter-current chromatography. J. Chromatogr. A 2002, 943, 219-225.
19. Yang, F.; Ito, Y. pH-Zone-refining counter-current chromatography of lappaconitine from Aconitum sinomontanum Nokai I. Separation of prepurified extract. J. Chromatogr. A 2001, 923, 281-285.
20. Tesarova, E.; Zaruba, K.; Flieger, M. Enantioseparation of semisynthetic ergot alkaloids on vancomycin and teicoplanin stationary phases. J. Chromatogr. A 1999, 844, 137-147.
21. Fabre, N.; Claparols, C.; Richelme, S.; Angelin, M.L.; Fouraste, I. Direct characterization of isoquinoline alkaloids in a crude plant extract by ion-pair liquid chromatography-electrospray ionization tandem mass spectrometry example of Eschscholtzia californica. J. Chromatogr. A 2000, 904, 35-46.
22. Sun, S.W.; Lee, S.S.; Wu, A.C.; Chen, C.K. Determination of bisbenzylisoquinoline alkaloids by high performance liquid chromatography. J. Chromatogr. A 1998, 799, 337-342.
23. Ciolino, L.A.; Turner, J.A.; McCauley, H.A.; Smallwood, A.W.; Yi, T.Y. Optimization study for the reversed-phase ion-pair liquid chromatographic determination of nicotine in commercial tobacco products. J. Chromatogr. A 1999, 852, 451-463.
24. Mroczek, T.; Glowniak, K. Simultaneous determination of N-oxides and free bases of pyrrolizidine alkaloids by cation-exchange solid-phase extraction and ion-pair high performance liquid chromatography. J. Chromatogr. A 2002, 949, 249-262.
25. Musshoff, F.; Schmidt, P.; Dettmeyer, R.; Priemer, F.; Wittig, H.; Madea, B. A systematic regional study of dopamine and dopamine-derived salsolinol and norsalsolinol levels in human brain areas. Forensic Sci. Int. 1999, 105, 1-11.
26. Petruczynik, A.; Gadzikowska, M.; Waksmundzka-Hajnos, M. Optimization of the separation of some Chelidonium majus L. alkaloids by reversed phase high performance liquid chromatography using cyanopropyl bonded stationary phase. Acta Pol. Pharm. 2002, 59, 61-64.
27. Lau, O.W.; Mok, C.S. High performance liquid chromatographic determination of atropine and atropine-like alkaloids in pharmaceutical preparations with indirect conductometric detection. J. Chromatogr. A 1997, 766, 270-276.
28. Nagy-Turak, A.; Vegh, Z. Extraction and in situ densitometric determination of alkaloids from Catharantus roseus by means of overpressured layer chromatography on amino-bonded silica layers. I. Optimization and validation of the separation system. J. Chromatogr. 1994, 668, 501-507.
29. Golkiewicz, W.; Gadzikowska, M. Isolation of some quaternary alkaloids from the extract of roots of Chelidonium majus L. by column and thin layer chromatography. Chromatographia 1999, 50, 52-56.