Optimization study for the reversed-phase ion-pair liquid chromatographic determination of nicotine in commercial tobacco products

Journal of Chromatography A

Volumn 852, Issue 2, 1999, Pages 451-463

  Ciolino, L A ^a   Turner, J A ^a   McCauley, H A ^a   Smallwood, A W ^a   Yi, T Y ^a  

^a CENTER FOR DRUG EVALUATION AND RESEARCH   (United States)

Author keywords

Alkaloids; Nicotine; Tobacco

Indexed keywords

ALKALOID; ANABASINE; ANATABINE; BUFFER; COTININE; NICOTINE; NORNICOTINE; UNCLASSIFIED DRUG;

ANALYTIC METHOD; ARTICLE; DISSOCIATION CONSTANT; DRUG DETERMINATION; ION PAIR CHROMATOGRAPHY; PH; PRIORITY JOURNAL; REVERSED PHASE LIQUID CHROMATOGRAPHY; TOBACCO;

BUFFERS; CHROMATOGRAPHY, LIQUID; HYDROGEN-ION CONCENTRATION; IONS; NICOTINE; PLANTS, TOXIC; TOBACCO;

NICOTIANA TABACUM;

EID: 0032781088     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0021-9673(99)00639-1     Document Type: Article

References (22)

1. L.A. Ciolino, H.A. McCauley, D.B. Fraser, D.Y. Barnett, T.Y. Yi, J.A. Turner, J. Agric. Food Chem., submitted for publication.
2. J.J. Piade, D. Hoffmann, J. Liq. Chromatogr. 3 (1980) 1505.
3. J.A. Saunders, D.E. Blume, J. Chromatogr 202 ((1981)) 147.
4. P.S.N. Murthy, B.V. Kameswararao, N.C. Gopalachari, J. Saunders, Tob. Res. 12 (1986) 186.
5. L.R. Synder, J.J. Kirkland, J.L. Glajch, Practical HPLC Method Development, 2nd ed, John Wiley and Sons, New York, NY, 1997.
6. L.A. Lin, J. Chromatogr. 632 (1993) 69.
7. A.W. Smallwood, C.S. Tschee, R.D. Satzger, J. Agric. Food Chem. 45 (1997) 3976.
8. CORESTA (Cooperation Centre for Scientific Research Relative to Tobacco) Recommended Method No 39, CORESTA Information Bulletin, 94/3-4 (1994).
9. United States Pharmacopeia, 1995, p. 1777.
10. CRC Handbook of Chemistry and Physics, 76th ed, CRC Press, Boca Raton, FL, 1995, pp. 8-54.
11. L.A. Ciolino, unpublished results.
12. S.S. Yang, I. Smetena, A.I. Goldsmith, J. Chromatogr. 746 (1996) 131.
13. R.F. Severson, K.L. McDuffie, R.F. Arrendale, G.R. Gwynn, J.F. Chaplin, A.W. Johnson, J. Chromatogr. 211 (1981) 111.
14. R.A. Andersen, P.D. Fleming, H.R. Burton, T.R. Hamilton-Kemp, D.F. Hildebrand, T.G. Sutton, Tobacco Science 34 (1990) 50.
15. F. Saitoh, M. Noma, N. Kawashima, Phytochemistry 24 (1985) 477.
16. V.A. Sisson, R.F. Severson, Beitrage zur Tabakforschung International 14 (1990) 327.
17. L.P. Bush, C. Grunwald, D.L. Davis, J. Agric. Food Chem. 20 (1972) 676.
18. H.R. Burton, R.A. Andersen, P.D. Fleming, L.R. Walton, J. Agric. Food Chem. 36 (1988) 579.
19. G.P. Morie, Tobacco Science 16 (1972) 167.
20. I. Yamamoto, in: R.L. Metcalf (Ed.), Advances in Pest Control Research, Interscience Publishers, New York, 1965, p. 231.
21. L.A. Ciolino, D.B. Fraser, T.Y. Yi, J.A. Turner, D.Y. Barnett, H.A. McCauley, J. Agric. Food Chem., submitted for publication.
22. P.G. Haines, A. Eisner, J. Am. Chem. Soc. 72 (1950) 1719.