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Crystal data for 1: C6H24Ag 2I4N6Zn, fw, 969.02, monoclinic, P6(3, a, 9.0550(6) Å, b, 9.0550(6) Å, c, 14.4468(19) Å, γ, 120.00°, V, 1025.84(17) Å3, Z, 2, Dcalc, 3.137 g cm -5, R, 0.0422, Rw, 0.1027, reflections used 5740 with I > 2σ(I, Crystal data for 2: C6H24Ag2I4N6Ni, fw, 962.36, monoclinic, P6(3, a, 8.9969(2) Å, b, 8.9969(2) Å, c, 14.4374(7) Å, γ, 120.00°, V, 1012.06(6) Å3, Z, 2, Dcalc, 3.158 g cm-3, R, 0.0360, Rw, 0.0776, reflections used 7767 with I > 2σI, Data collection was performed on a Bruker Smart APEX II
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w = 0.0776, reflections used 7767 with I > 2σ(I). Data collection was performed on a Bruker Smart APEX II diffractometer equipped with graphite-monochromitized Mo Kα radiation (λ = 0.710 73 Å) at 293 K.
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