메뉴 건너뛰기




Volumn 192, Issue 2, 2008, Pages 230-234

Sensitivity enhancement of the central-transition signal of half-integer spin quadrupolar nuclei in solid-state NMR: Features of multiple fast amplitude-modulated pulse transfer

Author keywords

FAM; m FAM; m SW(1 ) FAM; Quadrupolar nuclei; Sensitivity enhancement; Solid state NMR; SW(1 ) FAM

Indexed keywords

AMPLITUDE MODULATION; METAL SPINNING; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SENSITIVITY ANALYSIS; SOLID STATE REACTIONS;

EID: 43949109243     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2008.02.020     Document Type: Article
Times cited : (10)

References (31)
  • 2
    • 38749119764 scopus 로고    scopus 로고
    • 17O NMR studies of organic and biological molecules
    • 17O NMR studies of organic and biological molecules. Prog. Nucl. Magn. Reson. Spectrosc. 52 (2008) 118
    • (2008) Prog. Nucl. Magn. Reson. Spectrosc. , vol.52 , pp. 118
    • Wu, G.1
  • 3
    • 0001805442 scopus 로고
    • Triple quantum NMR on spin systems with I = 3/2 in solids
    • Vega S., and Naor Y. Triple quantum NMR on spin systems with I = 3/2 in solids. J. Chem. Phys. 75 (1981) 75
    • (1981) J. Chem. Phys. , vol.75 , pp. 75
    • Vega, S.1    Naor, Y.2
  • 4
    • 36149027989 scopus 로고
    • Nuclear quadrupole interaction in crystals
    • Pound R.V. Nuclear quadrupole interaction in crystals. Phys. Rev. 79 (1950) 685
    • (1950) Phys. Rev. , vol.79 , pp. 685
    • Pound, R.V.1
  • 5
    • 0000055192 scopus 로고
    • Sensitivity enhancement for NMR of the central transition of quadrupolar nuclei
    • Haase J., and Conradi M.S. Sensitivity enhancement for NMR of the central transition of quadrupolar nuclei. Chem. Phys. Lett. 209 (1993) 287
    • (1993) Chem. Phys. Lett. , vol.209 , pp. 287
    • Haase, J.1    Conradi, M.S.2
  • 6
    • 0001782193 scopus 로고
    • Population transfer for NMR of quadrupolar spins in solids
    • Haase J., Conradi M.S., Grey C.P., and Vega A.J. Population transfer for NMR of quadrupolar spins in solids. J. Magn. Reson. A109 (1994) 90
    • (1994) J. Magn. Reson. , vol.A109 , pp. 90
    • Haase, J.1    Conradi, M.S.2    Grey, C.P.3    Vega, A.J.4
  • 7
    • 0010131528 scopus 로고
    • Single- and double-resonance experiments of quadrupolar nuclei in solids using sensitivity enhancement of the central transition
    • Haase J., Conradi M.S., and Oldfield E. Single- and double-resonance experiments of quadrupolar nuclei in solids using sensitivity enhancement of the central transition. J. Magn. Reson. A109 (1994) 210
    • (1994) J. Magn. Reson. , vol.A109 , pp. 210
    • Haase, J.1    Conradi, M.S.2    Oldfield, E.3
  • 8
    • 0001396652 scopus 로고    scopus 로고
    • Advantages of double frequency sweeps in static, MAS and MQMAS NMR of spin I = 3/2 nuclei
    • Kentgens A.P.M., and Verhagen R. Advantages of double frequency sweeps in static, MAS and MQMAS NMR of spin I = 3/2 nuclei. Chem. Phys. Lett. 300 (1999) 435
    • (1999) Chem. Phys. Lett. , vol.300 , pp. 435
    • Kentgens, A.P.M.1    Verhagen, R.2
  • 9
    • 0034575873 scopus 로고    scopus 로고
    • Population and coherence transfer induced by double frequency sweeps in half-integer quadrupolar spin systems
    • Iuga D., Schäfer H., Verhagen R., and Kentgens A.P.M. Population and coherence transfer induced by double frequency sweeps in half-integer quadrupolar spin systems. J. Magn. Reson. 147 (2000) 192
    • (2000) J. Magn. Reson. , vol.147 , pp. 192
    • Iuga, D.1    Schäfer, H.2    Verhagen, R.3    Kentgens, A.P.M.4
  • 10
    • 0035248830 scopus 로고    scopus 로고
    • Population and coherence transfer in half-integer quadrupolar spin systems induced by simultaneous rapid passages of the satellite transitions: a static and spinning single crystal nuclear magnetic resonance study
    • Schäfer H., Iuga D., Verhagen R., and Kentgens A.P.M. Population and coherence transfer in half-integer quadrupolar spin systems induced by simultaneous rapid passages of the satellite transitions: a static and spinning single crystal nuclear magnetic resonance study. J. Chem. Phys. 114 (2001) 3073
    • (2001) J. Chem. Phys. , vol.114 , pp. 3073
    • Schäfer, H.1    Iuga, D.2    Verhagen, R.3    Kentgens, A.P.M.4
  • 11
    • 57249101755 scopus 로고    scopus 로고
    • Influencing the satellite transitions of half-integer quadrupolar nuclei for the enhancement of magic angle spinning spectra
    • Iuga D., and Kentgens A.P.M. Influencing the satellite transitions of half-integer quadrupolar nuclei for the enhancement of magic angle spinning spectra. J. Magn. Reson. 158 (2002) 65
    • (2002) J. Magn. Reson. , vol.158 , pp. 65
    • Iuga, D.1    Kentgens, A.P.M.2
  • 12
    • 0003152304 scopus 로고    scopus 로고
    • Sensitivity enhancement of the central transition NMR signal of quadrupolar nuclei under magic-angle spinning
    • Yao Z., Kwak H.T., Sakellariou D., Emsley L., and Grandinetti P.J. Sensitivity enhancement of the central transition NMR signal of quadrupolar nuclei under magic-angle spinning. Chem. Phys. Lett. 327 (2000) 85
    • (2000) Chem. Phys. Lett. , vol.327 , pp. 85
    • Yao, Z.1    Kwak, H.T.2    Sakellariou, D.3    Emsley, L.4    Grandinetti, P.J.5
  • 13
    • 0037413308 scopus 로고    scopus 로고
    • Modulation-aided signal enhancement in the magic angle spinning NMR of spin-5/2 nuclei
    • Madhu P.K., Pike K.J., Dupree R., Levitt M.H., and Smith M.E. Modulation-aided signal enhancement in the magic angle spinning NMR of spin-5/2 nuclei. Chem. Phys. Lett. 367 (2003) 150
    • (2003) Chem. Phys. Lett. , vol.367 , pp. 150
    • Madhu, P.K.1    Pike, K.J.2    Dupree, R.3    Levitt, M.H.4    Smith, M.E.5
  • 14
    • 0043031445 scopus 로고    scopus 로고
    • Application of amplitude-modulated radiofrequency fields to the magic-angle spinning NMR of spin-7/2 nuclei
    • Madhu P.K., Johannessen O.G., Pike K.J., Dupree R., Smith M.E., and Levitt M.H. Application of amplitude-modulated radiofrequency fields to the magic-angle spinning NMR of spin-7/2 nuclei. J. Magn. Reson. 163 (2003) 310
    • (2003) J. Magn. Reson. , vol.163 , pp. 310
    • Madhu, P.K.1    Johannessen, O.G.2    Pike, K.J.3    Dupree, R.4    Smith, M.E.5    Levitt, M.H.6
  • 15
    • 0037042272 scopus 로고    scopus 로고
    • A simple technique for determining nuclear quadrupole coupling constants using RAPT solid-state NMR spectroscopy
    • Prasad S., Kwak H.-T., Clark T., and Grandinetti P.J. A simple technique for determining nuclear quadrupole coupling constants using RAPT solid-state NMR spectroscopy. J. Am. Chem. Soc. 124 (2002) 4964
    • (2002) J. Am. Chem. Soc. , vol.124 , pp. 4964
    • Prasad, S.1    Kwak, H.-T.2    Clark, T.3    Grandinetti, P.J.4
  • 16
    • 1842637526 scopus 로고    scopus 로고
    • Signal enhancement of NMR spectra of half-integer quadrupolar nuclei in solids using hyperbolic secant pulses
    • Siegel R., Nakashima T.T., and Wasylishen R.E. Signal enhancement of NMR spectra of half-integer quadrupolar nuclei in solids using hyperbolic secant pulses. Chem. Phys. Lett. 388 (2004) 441
    • (2004) Chem. Phys. Lett. , vol.388 , pp. 441
    • Siegel, R.1    Nakashima, T.T.2    Wasylishen, R.E.3
  • 17
    • 24144463839 scopus 로고    scopus 로고
    • Sensitivity enhancement of NMR spectra of half-integer quadrupolar nuclei in the solid state via population transfer
    • Siegel R., Nakashima T.T., and Wasylishen R.E. Sensitivity enhancement of NMR spectra of half-integer quadrupolar nuclei in the solid state via population transfer. Conc. Magn. Reson. 26A (2005) 47
    • (2005) Conc. Magn. Reson. , vol.26 A , pp. 47
    • Siegel, R.1    Nakashima, T.T.2    Wasylishen, R.E.3
  • 18
    • 33645870424 scopus 로고    scopus 로고
    • Sensitivity enhancement of solid-state NMR spectra of half-integer spin quadrupolar nuclei using hyperbolic secant pulses: applications to spin-5/2 nuclei
    • Siegel R., Nakashima T.T., and Wasylishen R.E. Sensitivity enhancement of solid-state NMR spectra of half-integer spin quadrupolar nuclei using hyperbolic secant pulses: applications to spin-5/2 nuclei. Chem. Phys. Lett. 421 (2006) 529
    • (2006) Chem. Phys. Lett. , vol.421 , pp. 529
    • Siegel, R.1    Nakashima, T.T.2    Wasylishen, R.E.3
  • 19
    • 33846001010 scopus 로고    scopus 로고
    • Sensitivity enhancement of NMR spectra of half-integer spin quadrupolar nuclei in solids using hyperbolic secant pulses
    • Siegel R., Nakashima T.T., and Wasylishen R.E. Sensitivity enhancement of NMR spectra of half-integer spin quadrupolar nuclei in solids using hyperbolic secant pulses. J. Magn. Reson. 184 (2007) 85
    • (2007) J. Magn. Reson. , vol.184 , pp. 85
    • Siegel, R.1    Nakashima, T.T.2    Wasylishen, R.E.3
  • 20
    • 0000769739 scopus 로고
    • Multiple-quantum magic-angle spinning NMR: a new method for the study of quadrupolar nuclei in solids
    • Frydman L., and Harwood J.S. Multiple-quantum magic-angle spinning NMR: a new method for the study of quadrupolar nuclei in solids. J. Am. Chem. Soc. 117 (1995) 5367
    • (1995) J. Am. Chem. Soc. , vol.117 , pp. 5367
    • Frydman, L.1    Harwood, J.S.2
  • 21
    • 0002099140 scopus 로고    scopus 로고
    • Fast radio-frequency amplitude modulation in multiple-quantum magic-angle-spinning nuclear magnetic resonance: Theory and experiments
    • Madhu P.K., Goldbourt A., Frydman L., and Vega S. Fast radio-frequency amplitude modulation in multiple-quantum magic-angle-spinning nuclear magnetic resonance: Theory and experiments. Chem. Phys. Lett. 307 (1999) 41
    • (1999) Chem. Phys. Lett. , vol.307 , pp. 41
    • Madhu, P.K.1    Goldbourt, A.2    Frydman, L.3    Vega, S.4
  • 22
    • 0036923874 scopus 로고    scopus 로고
    • Multiple-quantum magic-angle spinning: High-resolution solid state NMR spectroscopy of half-integer quadrupolar nuclei
    • Goldbourt A., and Madhu P.K. Multiple-quantum magic-angle spinning: High-resolution solid state NMR spectroscopy of half-integer quadrupolar nuclei. Monatsh. Chem. 133 (2002) 1497
    • (2002) Monatsh. Chem. , vol.133 , pp. 1497
    • Goldbourt, A.1    Madhu, P.K.2
  • 23
    • 14844359910 scopus 로고    scopus 로고
    • Multiple-quantum magic-angle spinning: high-resolution solid-state NMR of half-integer spin quadrupolar nuclei
    • Goldbourt A., and Madhu P.K. Multiple-quantum magic-angle spinning: high-resolution solid-state NMR of half-integer spin quadrupolar nuclei. Annu. Rep. NMR Spectrosc. 54 (2005) 81
    • (2005) Annu. Rep. NMR Spectrosc. , vol.54 , pp. 81
    • Goldbourt, A.1    Madhu, P.K.2
  • 24
    • 1642493879 scopus 로고    scopus 로고
    • Enhancement of the central-transition signal in static and magic-angle-spinning NMR of quadrupolar nuclei by frequency-swept fast amplitude-modulated pulses
    • Bräuniger T., Ramaswamy K., and Madhu P.K. Enhancement of the central-transition signal in static and magic-angle-spinning NMR of quadrupolar nuclei by frequency-swept fast amplitude-modulated pulses. Chem. Phys. Lett. 383 (2004) 403
    • (2004) Chem. Phys. Lett. , vol.383 , pp. 403
    • Bräuniger, T.1    Ramaswamy, K.2    Madhu, P.K.3
  • 26
    • 33744995202 scopus 로고    scopus 로고
    • Fast amplitude-modulated pulse trains with frequency sweep (SW-FAM) in static NMR of half-integer spin quadrupolar nuclei
    • Bräuniger T., Hempel G., and Madhu P.K. Fast amplitude-modulated pulse trains with frequency sweep (SW-FAM) in static NMR of half-integer spin quadrupolar nuclei. J. Magn. Reson. 181 (2006) 68
    • (2006) J. Magn. Reson. , vol.181 , pp. 68
    • Bräuniger, T.1    Hempel, G.2    Madhu, P.K.3
  • 27
    • 0042890463 scopus 로고    scopus 로고
    • Enhancing sensitivity of quadrupolar nuclei in solid-state NMR with multiple rotor assisted population transfers
    • Kwak H.-T., Prasad S., Clark T., and Grandinetti P.J. Enhancing sensitivity of quadrupolar nuclei in solid-state NMR with multiple rotor assisted population transfers. Solid State Nucl. Magn. Reson. 24 (2003) 71
    • (2003) Solid State Nucl. Magn. Reson. , vol.24 , pp. 71
    • Kwak, H.-T.1    Prasad, S.2    Clark, T.3    Grandinetti, P.J.4
  • 29
    • 0034238161 scopus 로고    scopus 로고
    • The influence of the radiofrequency excitation and conversion pulses on the lineshapes and intensities of the triple-quantum MAS NMR spectra of I = 3/2 Nuclei
    • Goldbourt A., Madhu P.K., Kababya S., and Vega S. The influence of the radiofrequency excitation and conversion pulses on the lineshapes and intensities of the triple-quantum MAS NMR spectra of I = 3/2 Nuclei. Solid State Nucl. Magn. Reson. 18 (2000) 1
    • (2000) Solid State Nucl. Magn. Reson. , vol.18 , pp. 1
    • Goldbourt, A.1    Madhu, P.K.2    Kababya, S.3    Vega, S.4
  • 30
    • 0001412426 scopus 로고
    • 27Al nuclear magnetic resonance spectroscopy
    • 27Al nuclear magnetic resonance spectroscopy. Am. Mineral. 74 (1989) 203
    • (1989) Am. Mineral. , vol.74 , pp. 203
    • Woessner, D.E.1
  • 31
    • 0042494541 scopus 로고    scopus 로고
    • Efficient 5QMAS NMR of spin-5/2 nuclei: Use of fast amplitude-modulated radio-frequency pulses and cogwheel phase cycling
    • Bräuniger T., Pike K.J., Harris R.K., and Madhu P.K. Efficient 5QMAS NMR of spin-5/2 nuclei: Use of fast amplitude-modulated radio-frequency pulses and cogwheel phase cycling. J. Magn. Reson. 163 (2003) 64
    • (2003) J. Magn. Reson. , vol.163 , pp. 64
    • Bräuniger, T.1    Pike, K.J.2    Harris, R.K.3    Madhu, P.K.4


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.