메뉴 건너뛰기




Volumn 178, Issue 2, 2006, Pages 212-219

New opportunities for double rotation NMR of half-integer quadrupolar nuclei

Author keywords

DOR; Homonuclear correlation; MQDOR; Quadrupolar nuclei; Repetitive DFS

Indexed keywords

DIPOLE ANTENNAS; LATTICE CONSTANTS; METAL SPINNING; MINERALS; PULSE AMPLIFIERS; ROTATION; ROTORS;

EID: 30844447647     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2005.09.014     Document Type: Article
Times cited : (47)

References (45)
  • 2
    • 84891567947 scopus 로고
    • High-resolution solid-state NMR averaging of 2nd-order effects by means of a double-rotor
    • A. Samoson, E. Lippmaa, and A. Pines High-resolution solid-state NMR averaging of 2nd-order effects by means of a double-rotor Mol. Phys. 65 1988 1013
    • (1988) Mol. Phys. , vol.65 , pp. 1013
    • Samoson, A.1    Lippmaa, E.2    Pines, A.3
  • 4
    • 0001421829 scopus 로고
    • Isotropic spectra of half-integer quadrupolar spins from bidimensional magic-angle-spinning NMR
    • L. Frydman, and J.S. Harwood Isotropic spectra of half-integer quadrupolar spins from bidimensional magic-angle-spinning NMR J. Am. Chem. Soc. 117 1995 5367
    • (1995) J. Am. Chem. Soc. , vol.117 , pp. 5367
    • Frydman, L.1    Harwood, J.S.2
  • 5
    • 0034607375 scopus 로고    scopus 로고
    • Isotropic NMR spectra of half-integer quadrupolar nuclei using satellite transitions and magic-angle spinning
    • Z.H. Gan Isotropic NMR spectra of half-integer quadrupolar nuclei using satellite transitions and magic-angle spinning J. Am. Chem. Soc. 122 2000 3242
    • (2000) J. Am. Chem. Soc. , vol.122 , pp. 3242
    • Gan, Z.H.1
  • 6
    • 0001805442 scopus 로고
    • Triple quantum NMR on spin systems with i = 3/2 in solids
    • S. Vega, and Y. Naor Triple quantum NMR on spin systems with I = 3/2 in solids J. Chem. Phys. 75 1981 75
    • (1981) J. Chem. Phys. , vol.75 , pp. 75
    • Vega, S.1    Naor, Y.2
  • 7
    • 0000055192 scopus 로고
    • Sensitivity enhancement for NMR of the central transition of quadrupolar nuclei
    • J. Haase, and M.S. Conradi Sensitivity enhancement for NMR of the central transition of quadrupolar nuclei Chem. Phys. Lett. 209 1993 287
    • (1993) Chem. Phys. Lett. , vol.209 , pp. 287
    • Haase, J.1    Conradi, M.S.2
  • 8
    • 0001396652 scopus 로고    scopus 로고
    • Advantages of double frequency sweeps in static, MAS and MQMAS NMR of spin i = 3/2 nuclei
    • A.P.M. Kentgens, and R. Verhagen Advantages of double frequency sweeps in static, MAS and MQMAS NMR of spin I = 3/2 nuclei Chem. Phys. Lett. 300 1999 435
    • (1999) Chem. Phys. Lett. , vol.300 , pp. 435
    • Kentgens, A.P.M.1    Verhagen, R.2
  • 9
    • 0035248830 scopus 로고    scopus 로고
    • Population and coherence transfer in half-integer quadrupolar spin systems induced by simultaneous rapid passages of the satellite transitions: A static and spinning single crystal nuclear magnetic resonance study
    • H. Schäfer, D. Iuga, R. Verhagen, and A.P.M. Kentgens Population and coherence transfer in half-integer quadrupolar spin systems induced by simultaneous rapid passages of the satellite transitions: a static and spinning single crystal nuclear magnetic resonance study J. Chem. Phys. 114 2001 3073
    • (2001) J. Chem. Phys. , vol.114 , pp. 3073
    • Schäfer, H.1    Iuga, D.2    Verhagen, R.3    Kentgens, A.P.M.4
  • 10
    • 0002099140 scopus 로고    scopus 로고
    • Sensitivity enhancements of the MQMAS experiment by fast amplitude modulation of the pulses
    • P.K. Madhu, A. Goldbourt, L. Frydman, and S. Vega Sensitivity enhancements of the MQMAS experiment by fast amplitude modulation of the pulses Chem. Phys. Lett. 307 1999 41
    • (1999) Chem. Phys. Lett. , vol.307 , pp. 41
    • Madhu, P.K.1    Goldbourt, A.2    Frydman, L.3    Vega, S.4
  • 11
    • 0003152304 scopus 로고    scopus 로고
    • Sensitivity enhancement of the central transition NMR signal of quadrupolar nuclei under magic-angle spinning
    • Z. Yao, H.T. Kwak, D. Sakellariou, L. Emsley, and P.J. Grandinetti Sensitivity enhancement of the central transition NMR signal of quadrupolar nuclei under magic-angle spinning Chem. Phys. Lett. 327 2000 85
    • (2000) Chem. Phys. Lett. , vol.327 , pp. 85
    • Yao, Z.1    Kwak, H.T.2    Sakellariou, D.3    Emsley, L.4    Grandinetti, P.J.5
  • 12
    • 24144463839 scopus 로고    scopus 로고
    • Sensitivity enhancement of NMR spectra of half-integer quadrupolar nuclei in the solid-state via population transfer
    • R. Siegel, T.T. Nakashima, and R.E. Wasylishen Sensitivity enhancement of NMR spectra of half-integer quadrupolar nuclei in the solid-state via population transfer Conc. Magn. Reson. 26A 2005 47
    • (2005) Conc. Magn. Reson. , vol.26 , pp. 47
    • Siegel, R.1    Nakashima, T.T.2    Wasylishen, R.E.3
  • 13
    • 57249101755 scopus 로고    scopus 로고
    • Influencing the satellite transitions of half-integer quadrupolar nuclei for the enhancement of magic-angle spinning spectra
    • D. Iuga, and A.P.M. Kentgens Influencing the satellite transitions of half-integer quadrupolar nuclei for the enhancement of magic-angle spinning spectra J. Magn. Reson. 56 2002 65
    • (2002) J. Magn. Reson. , vol.56 , pp. 65
    • Iuga, D.1    Kentgens, A.P.M.2
  • 14
    • 0034575873 scopus 로고    scopus 로고
    • Population and coherence transfer induced by double frequency sweeps in half-integer quadrupolar spin systems
    • D. Iuga, H. Schäfer, R. Verhagen, and A.P.M. Kentgens Population and coherence transfer induced by double frequency sweeps in half-integer quadrupolar spin systems J. Magn. Reson. 147 2000 192
    • (2000) J. Magn. Reson. , vol.147 , pp. 192
    • Iuga, D.1    Schäfer, H.2    Verhagen, R.3    Kentgens, A.P.M.4
  • 15
    • 0000715865 scopus 로고
    • High-resolution solid-state sodium-23, aluminum-27 and silicon-29 nuclear magnetic resonance reconnaissance of alkali and plagioclase feldspars
    • R.J. Kirkpatrick, R.A. Kinsey, K.A. Smith, D.M. Henderson, and E. Oldfield High-resolution solid-state sodium-23, aluminum-27 and silicon-29 nuclear magnetic resonance reconnaissance of alkali and plagioclase feldspars Am. Mineral 70 1985 106
    • (1985) Am. Mineral , vol.70 , pp. 106
    • Kirkpatrick, R.J.1    Kinsey, R.A.2    Smith, K.A.3    Henderson, D.M.4    Oldfield, E.5
  • 16
    • 0042890463 scopus 로고    scopus 로고
    • Enhancing sensitivity of quadrupolar nuclei in solid-state NMR with multiple rotor assisted population transfers
    • H.-T. Kwak, S. Prasad, T. Clark, and P.J. Grandinetti Enhancing sensitivity of quadrupolar nuclei in solid-state NMR with multiple rotor assisted population transfers Solid State Nucl. Magn. Reson. 24 2003 71
    • (2003) Solid State Nucl. Magn. Reson. , vol.24 , pp. 71
    • Kwak, H.-T.1    Prasad, S.2    Clark, T.3    Grandinetti, P.J.4
  • 17
    • 0030567890 scopus 로고    scopus 로고
    • An Al-27 MQMAS and off-resonance nutation NMR investigation of Mo-P/γ-Al2O3 hydrotreating catalyst precursors
    • H. Kraus, R. Prins, and A.P.M. Kentgens An Al-27 MQMAS and off-resonance nutation NMR investigation of Mo-P/γ-Al2O3 hydrotreating catalyst precursors J. Phys. Chem. 100 1996 16337
    • (1996) J. Phys. Chem. , vol.100 , pp. 16337
    • Kraus, H.1    Prins, R.2    Kentgens, A.P.M.3
  • 18
    • 0009931448 scopus 로고    scopus 로고
    • Two-dimensional isotropic NMR of quadrupole nuclei in solids
    • A. Samoson Two-dimensional isotropic NMR of quadrupole nuclei in solids J. Magn. Reson. A 121 1996 209
    • (1996) J. Magn. Reson. A , vol.121 , pp. 209
    • Samoson, A.1
  • 20
    • 84994930785 scopus 로고
    • High-resolution solid-state 23Na NMR of anhydrous sodium sulfite
    • W.P. Power High-resolution solid-state 23Na NMR of anhydrous sodium sulfite Magn. Reson. Chem. 33 1995 220
    • (1995) Magn. Reson. Chem. , vol.33 , pp. 220
    • Power, W.P.1
  • 21
    • 0036923874 scopus 로고    scopus 로고
    • Multiple-quantum magic-angle spinning: High-resolution solid state NMR spectroscopy of half-integer quadrupolar nuclei
    • A. Goldbourt, and P.K. Madhu Multiple-quantum magic-angle spinning: high-resolution solid state NMR spectroscopy of half-integer quadrupolar nuclei Monatsh. Chem. 133 2002 1497
    • (2002) Monatsh. Chem. , vol.133 , pp. 1497
    • Goldbourt, A.1    Madhu, P.K.2
  • 22
    • 0000012749 scopus 로고    scopus 로고
    • Triple-quantum excitation enhancement in MQMAS experiments on spin i = 5/2 systems
    • D. Iuga, and A.P.M. Kentgens Triple-quantum excitation enhancement in MQMAS experiments on spin I = 5/2 systems Chem. Phys. Lett. 343 2001 556
    • (2001) Chem. Phys. Lett. , vol.343 , pp. 556
    • Iuga, D.1    Kentgens, A.P.M.2
  • 23
    • 13444310556 scopus 로고    scopus 로고
    • Sensitivity enhancement of MQMAS NMR spectra of spin 3/2 nuclei using hyperbolic secant pulses
    • R. Siegel, T.T. Nakashima, and R.E. Wasylishen Sensitivity enhancement of MQMAS NMR spectra of spin 3/2 nuclei using hyperbolic secant pulses Chem. Phys. Lett. 403 2005 353
    • (2005) Chem. Phys. Lett. , vol.403 , pp. 353
    • Siegel, R.1    Nakashima, T.T.2    Wasylishen, R.E.3
  • 24
    • 0347064094 scopus 로고    scopus 로고
    • Homonuclear NMR correlations between half-integer quadrupolar nuclei undergoing magic-angle spinning
    • M. Edén, and L. Frydman Homonuclear NMR correlations between half-integer quadrupolar nuclei undergoing magic-angle spinning J. Phys. Chem. B 107 2003 14598
    • (2003) J. Phys. Chem. B , vol.107 , pp. 14598
    • Edén, M.1    Frydman, L.2
  • 25
    • 0031551536 scopus 로고    scopus 로고
    • Determination of structural data from multiple-quantum magic-angle spinning NMR experiments
    • M.J. Duer Determination of structural data from multiple-quantum magic-angle spinning NMR experiments Chem. Phys. Lett. 277 1997 167
    • (1997) Chem. Phys. Lett. , vol.277 , pp. 167
    • Duer, M.J.1
  • 26
    • 0000467220 scopus 로고    scopus 로고
    • Deuterium polarization transfer in rotating solids and its application in structural investigation
    • Z. Gan, and P. Robyr Deuterium polarization transfer in rotating solids and its application in structural investigation Mol. Phys. 1998 1143
    • (1998) Mol. Phys. , pp. 1143
    • Gan, Z.1    Robyr, P.2
  • 27
    • 0034161770 scopus 로고    scopus 로고
    • H-2 MAS NMR of strongly dipolar coupled deuterium pairs in transition metal dihydrides: Extracting dipolar coupling and quadrupolar tensor orientations from the lineshape of spinning sidebands
    • G. Facey, D. Gusev, R.H. Morris, S. Macholl, and G. Buntkowsky H-2 MAS NMR of strongly dipolar coupled deuterium pairs in transition metal dihydrides: extracting dipolar coupling and quadrupolar tensor orientations from the lineshape of spinning sidebands Phys. Chem. Chem. Phys. 2 2000 935
    • (2000) Phys. Chem. Chem. Phys. , vol.2 , pp. 935
    • Facey, G.1    Gusev, D.2    Morris, R.H.3    MacHoll, S.4    Buntkowsky, G.5
  • 28
    • 0035280646 scopus 로고    scopus 로고
    • Quadrupolar-driven recoupling of homonuclear dipolar interactions in nuclear magnetic resonance of rotating solids
    • M. Edén, and L. Frydman Quadrupolar-driven recoupling of homonuclear dipolar interactions in nuclear magnetic resonance of rotating solids J. Chem. Phys. 114 2001 4116
    • (2001) J. Chem. Phys. , vol.114 , pp. 4116
    • Edén, M.1    Frydman, L.2
  • 29
    • 0037039405 scopus 로고    scopus 로고
    • Double-quantum-filtered nuclear magnetic resonance spectroscopy applied to quadrupolar nuclei in solids
    • A.J. Painter, and M.J. Duer Double-quantum-filtered nuclear magnetic resonance spectroscopy applied to quadrupolar nuclei in solids J. Chem. Phys. 116 2002 710
    • (2002) J. Chem. Phys. , vol.116 , pp. 710
    • Painter, A.J.1    Duer, M.J.2
  • 30
    • 84946636929 scopus 로고
    • Spectral spin-diffusion of a spin-3/2 system in rotating solids
    • S. Ding, and C.A. McDowell Spectral spin-diffusion of a spin-3/2 system in rotating solids Mol. Phys. 85 1995 283
    • (1995) Mol. Phys. , vol.85 , pp. 283
    • Ding, S.1    McDowell, C.A.2
  • 31
    • 0037126441 scopus 로고    scopus 로고
    • Relative orientation of quadrupole tensors from high-resolution NMR of powdered solids
    • N.G. Dowell, S.E. Ashbrook, and S. Wimperis Relative orientation of quadrupole tensors from high-resolution NMR of powdered solids J. Phys. Chem. B 106 2002 9470
    • (2002) J. Phys. Chem. B , vol.106 , pp. 9470
    • Dowell, N.G.1    Ashbrook, S.E.2    Wimperis, S.3
  • 32
    • 30844471064 scopus 로고    scopus 로고
    • J. Phys. Chem. B 106 2002 12412
    • (2002) J. Phys. Chem. B , vol.106 , pp. 12412
  • 33
    • 0037151661 scopus 로고    scopus 로고
    • High resolution 3D exchange NMR spectroscopy and the mapping of connectivities between half-integer quadrupolar nuclei
    • M. Edén, J. Grinshtein, and L. Frydman High resolution 3D exchange NMR spectroscopy and the mapping of connectivities between half-integer quadrupolar nuclei J. Am. Chem. Soc. 124 2002 9708
    • (2002) J. Am. Chem. Soc. , vol.124 , pp. 9708
    • Edén, M.1    Grinshtein, J.2    Frydman, L.3
  • 34
    • 0037063503 scopus 로고    scopus 로고
    • Reintroducing anisotropic interactions in magic-angle-spinning nmr of half-integer quadrupolar nuclei: 3D MQMAS
    • S. Wi, H. Heise, and A. Pines Reintroducing anisotropic interactions in magic-angle-spinning nmr of half-integer quadrupolar nuclei: 3D MQMAS J. Am. Chem. Soc. 124 2002 10653
    • (2002) J. Am. Chem. Soc. , vol.124 , pp. 10653
    • Wi, S.1    Heise, H.2    Pines, A.3
  • 35
    • 0033121292 scopus 로고    scopus 로고
    • Off-angle correlation spectroscopy applied to spin-1/2 and quadrupolar nuclei
    • P. Hartmann, C. Jäger, and J.W. Zwanziger Off-angle correlation spectroscopy applied to spin-1/2 and quadrupolar nuclei Solid State NMR 13 1999 245
    • (1999) Solid State NMR , vol.13 , pp. 245
    • Hartmann, P.1    Jäger, C.2    Zwanziger, J.W.3
  • 36
    • 0037420327 scopus 로고    scopus 로고
    • Homonuclear correlation experiments of half-integer quadrupolar nuclei using multiple-quantum techniques spinning at a P-4 magic angle
    • T.G. Ajithkumar, and A.P.M. Kentgens Homonuclear correlation experiments of half-integer quadrupolar nuclei using multiple-quantum techniques spinning at a P-4 magic angle J. Am. Chem. Soc. 125 2003 2398
    • (2003) J. Am. Chem. Soc. , vol.125 , pp. 2398
    • Ajithkumar, T.G.1    Kentgens, A.P.M.2
  • 37
    • 4544293924 scopus 로고    scopus 로고
    • Homonuclear correlation experiments for quadrupolar nuclei, spinning away from the magic angle
    • T.G. Ajithkumar, E.R.H. van Eck, and A.P.M. Kentgens Homonuclear correlation experiments for quadrupolar nuclei, spinning away from the magic angle Solid State Nucl. Magn. Reson. 26 2004 180
    • (2004) Solid State Nucl. Magn. Reson. , vol.26 , pp. 180
    • Ajithkumar, T.G.1    Van Eck, E.R.H.2    Kentgens, A.P.M.3
  • 38
    • 0034628599 scopus 로고    scopus 로고
    • Rotational-resonance NMR experiments in half-integer quadrupolar spin systems
    • M. Nijman, M. Ernst, A.P.M. Kentgens, and B.H. Meier Rotational-resonance NMR experiments in half-integer quadrupolar spin systems Mol. Phys. 98 2000 161
    • (2000) Mol. Phys. , vol.98 , pp. 161
    • Nijman, M.1    Ernst, M.2    Kentgens, A.P.M.3    Meier, B.H.4
  • 39
    • 0001018555 scopus 로고    scopus 로고
    • Radio-frequency-mediated dipolar recoupling among half-integer quadrupolar spins
    • M. Baldus, D. Rovnyak, and R.G. Griffin Radio-frequency-mediated dipolar recoupling among half-integer quadrupolar spins J. Chem. Phys. 112 2000 5902
    • (2000) J. Chem. Phys. , vol.112 , pp. 5902
    • Baldus, M.1    Rovnyak, D.2    Griffin, R.G.3
  • 40
    • 0037109606 scopus 로고    scopus 로고
    • Rotary resonance recoupling for half-integer quadrupolar nuclei in solid-state nuclear magnetic resonance spectroscopy
    • S.S. Wi, J.W. Logan, D. Sakellariou, J.D. Walls, and A. Pines Rotary resonance recoupling for half-integer quadrupolar nuclei in solid-state nuclear magnetic resonance spectroscopy J. Chem. Phys. 117 2002 7024
    • (2002) J. Chem. Phys. , vol.117 , pp. 7024
    • Wi, S.S.1    Logan, J.W.2    Sakellariou, D.3    Walls, J.D.4    Pines, A.5
  • 41
    • 1542636177 scopus 로고    scopus 로고
    • Double-quantum homonuclear correlation magic angle sample spinning nuclear magnetic resonance spectroscopy of dipolar-coupled quadrupolar nuclei
    • G. Mali, G. Fink, and F. Taulelle Double-quantum homonuclear correlation magic angle sample spinning nuclear magnetic resonance spectroscopy of dipolar-coupled quadrupolar nuclei J. Chem. Phys. 120 2004 2835
    • (2004) J. Chem. Phys. , vol.120 , pp. 2835
    • Mali, G.1    Fink, G.2    Taulelle, F.3
  • 42
    • 20444496119 scopus 로고    scopus 로고
    • Pulse-assisted homonuclear dipolar recoupling of half-integer quadrupolar spins in magic-angle spinning NMR
    • M. Edén, H. Annersten, and A. Zazzi Pulse-assisted homonuclear dipolar recoupling of half-integer quadrupolar spins in magic-angle spinning NMR Chem. Phys. Lett. 410 2005 24
    • (2005) Chem. Phys. Lett. , vol.410 , pp. 24
    • Edén, M.1    Annersten, H.2    Zazzi, A.3
  • 43
    • 0011352041 scopus 로고    scopus 로고
    • Encyclopedia of NMR
    • D.M. Grant R.K. Harris Wiley Chichester, England
    • M.H. Levitt Encyclopedia of NMR D.M. Grant R.K. Harris Advances in NMR vol. 9 2002 Wiley Chichester, England 165 196
    • (2002) Advances in NMR , vol.9 , pp. 165-196
    • Levitt, M.H.1
  • 44
    • 4043060016 scopus 로고
    • Synchronized double-rotation NMR spectroscopy
    • A. Samoson, and E. Lippmaa Synchronized double-rotation NMR spectroscopy J. Magn. Reson. 84 1989 410
    • (1989) J. Magn. Reson. , vol.84 , pp. 410
    • Samoson, A.1    Lippmaa, E.2
  • 45
    • 30844446622 scopus 로고    scopus 로고
    • J. van Beek, MatNMR is a toolbox for processing NMR/EPR data under MATLAB and can be freely downloaded at 〈http://matnmr.sourceforge.net〉.
    • Van Beek, J.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.