Sensitivity enhancement of solid-state NMR spectra of half-integer spin quadrupolar nuclei using hyperbolic secant pulses: Applications to spin-5/2 nuclei

Chemical Physics Letters

Volumn 421, Issue 4-6, 2006, Pages 529-533

  Siegel, Renée ^a   Nakashima, Thomas T ^a   Wasylishen, Roderick E ^a  

^a UNIVERSITY OF ALBERTA   (Canada)

Author keywords

[No Author keywords available]

Indexed keywords

ALUMINA; ELECTRON ENERGY LEVELS; NUCLEAR ENERGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SOLIDS;

DOUBLE-FREQUENCY SWEEP METHOD; HYPERBOLIC SECANT; QUADRUPOLAR NUCLEI;

NUCLEIC ACIDS;

EID: 33645870424     PISSN: 00092614     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.cplett.2006.01.107     Document Type: Article

References (32)

1. Siegel R., Nakashima T.T., and Wasylishen R.E. Chem. Phys. Lett. 388 (2004) 441
2. Silver M.S., Joseph R.I., Chen C.N., Sank V.J., and Hoult D.I. Nature 310 (1984) 681
3. Silver M.S., Joseph R.I., and Hoult D.I. J. Magn. Reson. 59 (1984) 347
4. Silver M.S., Joseph R.I., and Hoult D.I. Magn. Reson. Med. 1 (1984) 294
5. Silver M.S., Joseph R.I., and Hoult D.I. Phys. Rev. A 31 (1985) 2753
6. Bendall M.R. J. Magn. Reson. A 116 (1995) 46
7. Kupče E., and Freeman R. J. Magn. Reson. A 118 (1996) 299
8. Tannus A., and Garwood M. NMR Biomed. 10 (1997) 423
9. Rosenfeld D., and Zur Y. J. Magn. Reson. 132 (1998) 102
10. Tesiram Y.A., and Bendall M.R. J. Magn. Reson. 156 (2002) 26
11. Hahn E.L. Phys. Rev. 80 (1950) 580
12. Carr H.Y., and Purcell E.M. Phys. Rev. 94 (1954) 630
13. Meiboom S., and Gill D. Rev. Sci. Instrum. 29 (1958) 688
14. Larsen F.H., Jakobsen H.J., Ellis P.D., and Nielsen N.C. J. Phys. Chem. A 101 (1997) 8597
15. Yao Z., Kwak H.T., Sakellariou D., Emsley L., and Grandinetti P.J. Chem. Phys. Lett. 327 (2000) 85
16. Kentgens A.P.M., and Verhagen R. Chem. Phys. Lett. 300 (1999) 435
17. Iuga D., Schafer H., Verhagen R., and Kentgens A.P.M. J. Magn. Reson. 147 (2000) 192
18. Iuga D., and Kentgens A.P.M. J. Magn. Reson. 158 (2002) 65
19. Siegel R., Nakashima T.T., and Wasylishen R.E. Chem. Phys. Lett. 403 (2005) 353
20. Frydman L., and Harwood J.S. J. Am. Chem. Soc. 117 (1995) 5367
21. Medek A., Harwood J.S., and Frydman L. J. Am. Chem. Soc. 117 (1995) 12779
22. Madhu P.K., Goldbourt A., Frydman L., and Vega S. Chem. Phys. Lett. 307 (1999) 41
23. Wu G., Rovnyak D., and Griffin R.G. J. Am. Chem. Soc. 118 (1996) 9326
24. Haase J., and Conradi M.S. Chem. Phys. Lett. 209 (1993) 287
25. Haase J., Conradi M.S., Grey C.P., and Vega A.J. J. Magn. Reson. A 109 (1994) 90
26. Schurko R.W., Wasylishen R.E., and Foerster H. J. Phys. Chem. A 102 (1998) 9750
27. Bak M., Rasmussen J.T., and Nielsen N.C. J. Magn. Reson. 147 (2000) 296
28. Segel S.L. J. Chem. Phys. 51 (1969) 848
29. Mooberry E.S., Spiess H.W., and Sheline R.K. J. Chem. Phys. 57 (1972) 813
30. Wi S., and Frydman L. J. Chem. Phys. 112 (2000) 3248
31. Kwak H.T., Prasad S., Clark T., and Grandinetti P.J. Solid State Nucl. Magn. Reson. 24 (2003) 71
32. Kentgens A.P.M., van Eck E.R.H., Ajithkumar T.G., Anupöld T., Past J., Reinhold A., and Samoson A. J. Magn. Reson. 178 (2006) 212