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-1): 3568 (m), 3474 (w, br), 1676 (vs), 1641 (vs), 1600 (s), 1427 (s), 1384 (s), 1321(m), 1193 (w), 1083 (w), 801 (w), 739 (m), 665 (m).
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26
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note
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2 = 0.0557 [I > 2σ(I)]. Structural data for 1 and 2 were collected on a Bruker Smart Apex CCD with graphite-monochromated Mo Kα radiation (λ = 0.71073 Å) at 293 K. Their structures were solved by direct methods and refined with the full-matrix least-squares technique using the SHELXS-97 and SHELXL-97 programs [10].
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