Multivariate optimization of a derivatisation procedure for the simultaneous determination of nine anabolic steroids by gas chromatography coupled with mass spectrometry

Journal of Chromatography A

Volumn 1190, Issue 1-2, 2008, Pages 278-285

  Hadef, Y ^a   Kaloustian, J ^b,c   Portugal, H ^b,c   Nicolay, A ^b,c  

^a BADJI MOKHTAR UNIVERSITY   (Algeria)

^b AIX MARSEILLE UNIVERSITY   (France)

^c INSERM   (France)

Author keywords

Anabolic steroids; Derivatisation; Desirability; Doelhert design; Experimental design; Optimization

Indexed keywords

ANABOLIC STEROIDS; DERIVATIZATION; DESIRABILITY; DOELHERT DESIGN;

DESIGN OF EXPERIMENTS; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; PARAMETER ESTIMATION;

OPTIMIZATION;

ACETAMIDE DERIVATIVE; ALPHA CHOLESTANE; AMMONIUM DERIVATIVE; AMMONIUM IODIDE; ANABOLIC AGENT; ANDROSTERONE; BOLDENONE; CHOLESTANE DERIVATIVE; DYDROGESTERONE; EPITESTOSTERONE; ESTRADIOL; MERCAPTOETHANOL; N METHYL N TRIMETHYLSILYLTRIFLUOROACETAMIDE; NANDROLONE; NANDROLONE 17 PROPIONATE; TESTOSTERONE; TESTOSTERONE PROPIONATE; TRIMETHYLSILYL DERIVATIVE; UNCLASSIFIED DRUG;

ANALYTICAL PARAMETERS; ARTICLE; CORRELATION COEFFICIENT; DERIVATIZATION; LINEAR SYSTEM; MASS FRAGMENTOGRAPHY; MULTIVARIATE ANALYSIS; PREDICTION; PRIORITY JOURNAL; REACTION ANALYSIS; REGRESSION ANALYSIS; SILYLATION; STEROID ANALYSIS; TEMPERATURE DEPENDENCE; THEORETICAL MODEL; VALIDATION STUDY;

ANABOLIC AGENTS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; MULTIVARIATE ANALYSIS; REFERENCE STANDARDS; STEROIDS;

EID: 42149127180     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2008.02.100     Document Type: Article

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