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41649099146
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2O and DMF) and temperatures (rt, -20°C and -78°C) did not give satisfactory results.
-
2O and DMF) and temperatures (rt, -20°C and -78°C) did not give satisfactory results.
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24
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41649105365
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Other synthetic protocols attempted included (i) the reaction of 1 with acyl chloride in the presence of Mg and (ii) the reaction of 3 with Grignard reagents. Both procedures resulted in no reaction or complex mixtures.
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Other synthetic protocols attempted included (i) the reaction of 1 with acyl chloride in the presence of Mg and (ii) the reaction of 3 with Grignard reagents. Both procedures resulted in no reaction or complex mixtures.
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33645544948
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and literature cited therein. For tandem RCM-isomerization reactions, see
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For tandem RCM-isomerization reactions, see: Fustero, S.; Sánchez-Roselló, M.; Jiménez, D.; Sanz-Cervera, J. F.; del Pozo, C.; Aceña, J. L. J. Org. Chem. 2006, 71, 2706-2714 and literature cited therein.
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36
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41649109683
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The other isomers of 14a and 14b were isolated in 8% and 20% yield, respectively.
-
The other isomers of 14a and 14b were isolated in 8% and 20% yield, respectively.
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41649107903
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