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19
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note
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2 = 0.1031, GOF = 1.023, max/min residual electron densities -0.194/0.402 e Å. The data were collected at 293 K using a SMART APEX II-CCD single crystal X-ray diffractometer (graphite monochromated Mo Kα radiation, λ = 0.71073 Å). A multi-scan absorption correction was applied using the SADABS program. The structures were solved by direct methods and refined by full-matrix least-squares method implemented in SHELXTL-97 [21]. All the non-hydrogen atoms were refined anisotropically. Hydrogen atoms were added theoretically.
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