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2O): C. 20.38; H, 3.63. Found: C, 20.12; H, 3.21. Use of other template molecules instead of dioxane produced a series of crystalline compounds with the same composition for 1·1/3G, where G = THF, furan, or cyclohexane. All compounds are isostructural except for the different orientation of the guest molecules. The same reaction in the absence of organic guests yields a mixture of nonporous manganese formates including a previously known phase (Viertelhaus, M.; Henke, H.; Anson, C. E.; Powell, A. K. Eur. J. Inorg. Chem. 2003, 2283). See Supporting Information for more details.
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85039579872
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note
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2 (all data) = 0.128. GOF = 1.032.
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30
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85039563871
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note
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2 (all data) = 0.123, GOF = 1.084.
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33
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85039564985
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note
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-2 of adsorbed hydrogen.20
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35
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