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Volumn 37, Issue 1, 2008, Pages 10-11

A proline-based macrocyclic amide with S4 symmetry

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[No Author keywords available]

Indexed keywords


EID: 38949187929     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.2008.10     Document Type: Article
Times cited : (8)

References (21)
  • 16
    • 0035857549 scopus 로고    scopus 로고
    • For cyclic amides with an alternating sequence of L- and D-α-amino acids, see: D. T. Bong, T. D. Clark, J. R. Granja, M. R. Ghadiri, Angew. Chem., Int. Ed. 2001, 40, 988.
    • For cyclic amides with an alternating sequence of L- and D-α-amino acids, see: D. T. Bong, T. D. Clark, J. R. Granja, M. R. Ghadiri, Angew. Chem., Int. Ed. 2001, 40, 988.
  • 17
    • 38949202528 scopus 로고    scopus 로고
    • Spartan'06 (Wavefunction, Inc.) was used for the calculations. A Monte Carlo conformation search was performed using the MMFF force field to find the lowest energy conformation, which was then used as an initial structure for the geometry optimization using the semiempirical AMI model.
    • Spartan'06 (Wavefunction, Inc.) was used for the calculations. A Monte Carlo conformation search was performed using the MMFF force field to find the lowest energy conformation, which was then used as an initial structure for the geometry optimization using the semiempirical AMI model.
  • 20
    • 38949135845 scopus 로고    scopus 로고
    • Spectral data of macrocycle 1: 1HNMR (400 MHz, DMSO-d 6) δ 10.08 (s, 4H, 7.90 (d, 4J, 2.6Hz, 4H, 7.62 (dd, 3J, 9.3Hz, 4J, 2.6Hz, 4H, 6.94 (d, 3J, 9.3Hz, 4H, 4.38-4.41 (m, 4H, 3.38-3.42 (m, 4H, 3.07-3.11 (m, 4H, 2.38-2.42 (m, 4H, 1.84-2.01 (m, 12H, 13CNMR (100MHz, DMSCW6) δ 167.0, 137.4, 136.6, 128.8, 125.1, 117.9, 115.7, 62.8, 51.5, 31.6, 24.3; HRMS (FAB) m/z: [M, H, calcd for C44H45NnO12, 933.3280; found 933.3276
    • 12, 933.3280; found 933.3276.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.