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Volumn 5, Issue 1, 2008, Pages 65-68

Solvent-free mechanochemical reaction of [60]fullerene with phenylhydrazine hydrochlorides

Author keywords

60 Fullerene; Mechanochemistry; Phenylhydrazine hydrochlorides; Solvent free

Indexed keywords


EID: 38949178890     PISSN: 15701786     EISSN: None     Source Type: Journal    
DOI: 10.2174/157017808783330153     Document Type: Article
Times cited : (6)

References (42)
  • 30
    • 0037296385 scopus 로고    scopus 로고
    • Allard, E.; Cheng, R; Chopin. S.; Delaunay, J.; Rondeau, D.; Cousseau, J. New J. Chem., 2003, 27, 188.
    • (c) Allard, E.; Cheng, R; Chopin. S.; Delaunay, J.; Rondeau, D.; Cousseau, J. New J. Chem., 2003, 27, 188.
  • 38
    • 38949182244 scopus 로고    scopus 로고
    • 60 due to their low polarity.
    • 60 due to their low polarity.
  • 39
    • 38949090989 scopus 로고    scopus 로고
    • Spectral data for product 2e: 1H NMR (300 MHz, CS2-CDCl3) δ 8.67 (d, J, 8.8 Hz, 2H, δ 8.62 (d, J, 8.8 Hz, 2H, 6.67 (s, 1H, 13C NMR (75 MHz, CS2-CDCl3 with Cr(acac)3 as relaxation agent all 2C unless indicated) δ 153.54 (1C, aryl C, 150.85, 150.63, 146.68 (1C, 146.58 (1C, 146.30 (1C, 145.57, 145.47 (4C, 145.29 (4C, 144.78, 144.68, 144.61, 144.50, 144.42, 144.33, 143.68, 143.43, 142.35, 141.70 (4C, 141.20, 141.06 (4C, 140.76, 140.71 (4C, 139.57, 139.28, 135.12, 135.02, 127.85 (aryl C, 124.29 (aryl C, 66.53 (1C, sp3-C of C60, 62.52 (1C2 sp3-C of C60, FT-IR (KBr) υ max (cm-1) 2922,2852, 1603, 1516, 1427, 1345, 1185, 1111, 853, 731, 583, 527; MS (MALDI-TOF) m/z 842 (M-1, UV-vis CHCl3, λmax nm log ε
    • max nm (log ε) 256 (5.16), 309 (4.71), 431 (3.64), 698 (2.70).
  • 40
    • 38949213300 scopus 로고    scopus 로고
    • 2).
    • 2).
  • 41
    • 38949213986 scopus 로고    scopus 로고
    • Spectral data for product 4: 1H NMR (300 MHz, CS2-CDCl3) δ 7.47 (d, J, 8.7 Hz, 2H, 6.88 (d, J, 8.7 Hz, 2H, 3.80 (s, 3H, OCH3, 13C NMR (75 MHz, CS2-CDCl3 with Cr(acac)3 as relaxation agent all 2C unless indicated) δ 154.52 (1C, aryl C, 146.51, 143.55, 143.50, 143.40, 143.18, 143.13, 143.06 (3C, 143.02, 142.82 (3C, 142.55, 142.33 (4C, 142.16 (4C, 142.11, 141.92, 141.89 141.76, 141.68, 140.61, 140.20 (3C, 139.23 (1C, 139.64, 139.52, 137.55, 136.77 (1C, aryl C, 136.65, 136.27, 135.75, 133.87, 116.52 (aryl C, 113.63 (aryl C, 54.57 (1C, OCH3, FT-IR (KBr) υmax (cm-1) 2922, 2826, 1556, 1506, 1460, 1437, 1395, 1344, 1285, 1243, 1179, 1036, 821, 619, 525; MS (MALDI-TOF) m/z 841 (M, UV-vis (CHCl3) λmax nm (log ε) 260 (5.20, 329 (4.57, 502 (3.42, 544 3.36
    • max nm (log ε) 260 (5.20), 329 (4.57), 502 (3.42), 544 (3.36).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.