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X-ray crystallography for 4c: Empirical formula C 18H11FN2O, Fw, 290.29, T, 173(2) K, monoclinic, space group p 21/c, a, 8.705 (2) Å, b, 7.9408(18) Å, c, 20462(5) Å, α, 90°, β, 97.309(5)°, γ, 90°, V, 14029(6) Å3, Z, 4, Dcalcd, 1.374 Mg/m 3, λ (MoKα, 0.71070 Å, μ, 0.096 mm -1, F000, 600. 3.26°< θ <25.34°, R, 0.0624, wR, 0.1373. s, 1.173. largest diff. peak and hole: 0.207 and -0.218 e. Å3
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