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Volumn 5, Issue 1, 2008, Pages 51-54

A convenient, solvent free and high yielding synthesis of bicyclo-heterocyclic compounds

Author keywords

Amines; Bicyclo heterocyclic; Dicarboxlic acids; Microwave

Indexed keywords

EID: 38949113346 PISSN: 15701786 EISSN: None Source Type: Journal
DOI: 10.2174/157017808783330180 Document Type: Article

Times cited : (12)

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24
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- 1HNMR data is reported by following the numbering as mentioned for compound 2a. A figure is presented, 2a)m.p. 105°C; IR(KBr) cm-11662, CO-N-CO, 1561 & 1484 (Ar, 1HNMR (500 MHzDMSO- d6) 1.40-1.41(d, 2H, C6′, 1.52-1.56 (m, 4H, C5′ C7′, 2.55-2.65 (m, 6H, C1′, C8′, C2′, 2.94-2.96 (t, 2H, CH2,C1′, 7.54-7.56 (q, 2H, Ar, 8.06-8.09 (t, 2H, Ar, GCMS m/z 258(M+4.52, 2b) m.p. 113°C; IR(KBr) cm-1 1771, CO-N-CO, 1612,1560 (Ar),1′HNMR (500 MHz DMSO-d6, 4.76 (s, 2H, CH2),6.36-6.37(d, 1H, furan, 6.38-6.39 (q, 1H, furan, 7.55-7.56 (d, 1H, furan, 7.83-7.91(m, 4H, Ar, GCMS m/z 227 (M+ 100, 2c) m.p. 110°C, IR(KBr) cm-1 1625, CO-N-CO, 1559,1451 (Ar, 1HNMR (590 MHz, DMSO-d6, 1.38-1.39d, 2H, C
- 6′)

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