Operation strategies for simulated moving bed in the presence of adsorbent ageing

Separation Science and Technology

Volumn 42, Issue 16, 2007, Pages 3555-3591

  Sá Gomes, Pedro ^a   Minceva, Mirjana ^a   Rodrigues, Alírio E ^a  

^a UNIVERSITY OF PORTO   (Portugal)

Author keywords

Adsorption; Ageing; Deactivation; Separation; Simulated moving bed; True moving bed

Indexed keywords

ADSORBENTS; MASS TRANSFER; PARAMETER ESTIMATION;

DEACTIVATION; SIMULATED MOVING BED; TRUE MOVING BED;

ADSORPTION;

ADSORBENTS; ADSORPTION; MASS TRANSFER; PARAMETER ESTIMATION;

ADSORBENCY; AGING; FLOW RATE; MASS TRANSFER; RESISTANT PROPERTY;

EID: 38149116313     PISSN: 01496395     EISSN: 15205754     Source Type: Journal    
DOI: 10.1080/01496390701710703     Document Type: Article

References (62)

1. Broughton, D.B. and Gerhold, C.G. (1961) Continuous Sorption Process Employing Fixed Bed of Sorbent and Moving Inlets and Outlets. US Patent No 2 985 589.
2. Broughton, D.B., Neuil, R.W., Pharis, J.M., and Brearley, C.S. (1970) The Parex process for recovering paraxylene. Chem. Eng. Progress, 66: 70-75.
3. Ash, G., Barth, K., Hotier, G., Mank, L., and Renard, P. (1994) ELUXYL: A new paraxylene separation process rev. Inst. Fr. Petr., 49 (05): 541-549.
4. Pavone, D. and Hotier, G. (2000) System approach modelling applied to the eluxyl process. Revue IFP., 55: 437.
5. Nicoud, R.M. (1999) The separation of optical isomers by simulated moving bed chromatography. Pharm. Tech. Europe, 11: 28-34.
6. Nicoud, R.M. (1999) The separation of optical isomers by simulated moving bed chromatography. Pharm. Tech. Europe, 11: 36-44.
7. Adam, P.R., Nicoud, R.M., Bailly, M., and Ludernann-Hombourger, O. (2000) Process and device for separation with variable-length. U.S. Patent No 6 136 198.
8. Ludemman-Hombouger, O., Nicoud, R.M., and Bailly, M. (2000) The "Varicol" Process: a new multicolumn continuous chromatographic process. Separation Science and Technology, 35 (12): 1829-1862.
9. Zhang, Z., Mazzotti, M., and Morbidelli, M. (2003) Powerfeed operation of simulated moving bed units: changing the flow-rates during the switching interval. Journal of Chromatography A, 1006: 87-99.
10. Schramm, H., Kaspereit, M., Kienle, A., and Seidel-Morgenstern, A. (2002) Improving simulated moving bed processes by cyclic modulation of the feed concentration, Chem. Eng. Tech., 25 (12): 1151-1155.
11. Schramm, H., Kaspereit, M., Kienle, A., and Seidel-Morgenstern, A. (2003) Simulated moving bed process with a cyclic modulation of the feed concentration. Journal of Chromatography A, 1006: 77-86.
12. Sá Gomes, P. and Rodrigues, A.E. (2007) Outlet Streams Swing (OSS) and MultiFeed (MF) operation of simulated moving beds. Separation Science and Technology, 42: 223-252.
13. Kim, J.K., Abunasser, N., and Wankat, P. (2005) Use of Two feeds in simulated moving beds for binary separation. Korean J. Chem. Eng., 22 (4): 619-627.
14. Hur, J.S. and Wankat, P.C. (2005) New design of simulated moving bed (SMB) for ternary separations. Ind. Eng. Chem. Res., 44: 1906-1913.
15. Hur, J.S. and Wankat, P.C. (2006) Two-zone SMB/chromatography for center-cut separation from ternary mixtures: linear isotherm sytems. Ind. Eng. Chem. Res., 45: 1426-1433.
16. Mata, V.G. and Rodrigues, A.E. (2001.) Separation of ternary mixtures by pseudo-simulated moving bed chromatography. J. Chromatography A, 939: 23-40.
17. Borges da Silva, E.A. and Rodrigues, A.E. (2006) Continuous chromatographic separation of multicomponent mixtures using JO technology. AIChE Journal, 52: 3794-3812.
18. Silva, V.M.T.M. and Rodrigues, A.E. (2005) Novel process for diethylacetal synthesis. AIChE Journal, 51: 2752-2768.
19. Rodrigues, A.E. and Silva, V.M.T.M. (2004). Processo Industrial de Produção de Acetais num Reactor Adsorptivo de Leito Móvel Simulado. Patent no. PT 103123. also published as (2005) Industrial Process for Acetals Production in a Simulated Moving Bed Reactor Patent No. WO113476 A1.
20. Bartholomew, C.H. (2001) Mechanisms of catalyst deactivation. Applied Catalysis: General, 212: 17-60.
21. Denny, P.J. and Twigg, M.V. (1980) In Catalyst Deactivation 1980 Stud. Surf. Sci. Catal.; Delmon, B. and Froment, G.F. (eds.); Elsevier: Amsterdam, Vol. 6, p. 577.
22. Bartholomew, C.H. (1984) Catalyst deactivation. Chem. Eng., 91 (23): 96-112.
23. Butt, J.B. (1984) In Catalysis, Science and Technology; Anderson, J.R. and Boudart, M. (eds.); Springer: New York, p.1.
24. Farrauto, R.J. and Bartholomew, C.H. (1997) Fundamentals of Industrial Catalytic Processes; Chapman & Hall, Kluver Academic Publishers: London, Chapter 5.
25. Figueiredo, J.L. (ed.), (1982) Progress in catalyst deactivation, NATO Advanced Study Institute Series E, Marunus Nijhoff: Boston.
26. Hughes, R. (1984) Deactivation of Catalysts; Academic Press: London, Chapter 8.
27. Oudar, J. and Wise, H. (1985) Deactivation and Poisoning of Catalysts; Marcel Dekker: New York.
28. Butt, J.B. and Peterson, E.E. (1988) Activation, Deactivation and Poisoning of Catalysts; Academic Press: San Diego.
29. Delmon, B. and Forment, G.F. (1980) Catalyst Deactivation, Stud. Surf. Sci. Catal.; Elsevier: Amsterdam, Vol. 6.
30. Delmon, B. and Forment, G.F. (1987) Catalyst Deactivation; Stud. Surf. Sci. Catal.; Elsevier: Amsterdam, Vol. 34.
31. Delmon, B. and Forment, G.F. (1994) Catalyst Deactivation; Stud. Surf. Sci. Catal.; Elsevier: Amsterdam, Vol. 88.
32. Delmon, B. and and Forment, G.F. (1999) Catalyst Deactivation Stud. Surf. Sci. Catal.: Elsevier: Amsterdam, Vol. 126.
33. Bartholomew, C.H. and Butt, J.B. (1991) Catalyst Deactivation, Stud. Surf. Sci. Catal.; Elsevier: Amsterdam., Vol. 68.
34. Bartholomew, C.H. and Fuentes, G.A. (1997) Catalyst Deactivation, Stud. Surf. Sci. Catal.; Elsevier: Amsterdam., Vol. 111.
35. Sá Gomes, P., Minceva, M., and Rodrigues, A.E. (2006) Operation of Simulated Moving Bed in Presence of Adsorbent Ageing, 2006 AIChE Annual Meeting; paper 148c.
36. Minceva, M. and Rodrigues, A.E. (2002) Modelling and simulation of a simulated moving bed for the separation of p-Xylene. Ind. Eng. Chem. Res., 41: 3454-3461.
37. Kohl, A. and Nielsen, R. (1997) Gas Purification; Gulf Publishing Company: Houston, Chap. 12, p. 1070.
38. Natarajan, S. and Lee, J.H. (2000) Repetitive model predictive control applied to a simulated moving bed chromatography systems. Computers & Chemical Engineering, 24: 1127-1133.
39. Abel, S., Erdem, G., Mazzotti, M., Morari, M., and Morbidelli, M. (2004) Optimizing control of simulated moving beds - linear isotherm. Journal of Chromatography A, 1033: 229-239.
40. Toumi, A. and Engell, A. (2004) Optimization based control of a reactive simulated moving bed process for glucose isomerization. Chemical Engineering Science, 59: 3777-3792.
41. Engell, S. (2007) Feedback control for optimal process operation. Journal of Process Control, article in Press.
42. Aida, T. and Silveston, P.L. (2005) Cyclic Separating Reactors; Blackwell Publishing: Oxford, Chap. 8, p. 162.
43. Pilliod, D.L., Randall, K.C., and Harding, E.M. (2006) A process for hydrocarbon conversion with on-line solid particulate material removal. WO Patent No 118739 A2.
44. Pilliod, D.L., Randall, K.C., and Harding, E.M. (2006). An adsorption process with on-line adsorbent removal. WO Patent No 118740 A1.
45. Frey, S.J., Sechrist, P.A., and Kauff, D.A. (2006) Fluid distribution apparatus. WO Patent No 055222 A1.
46. Minceva, M. and Rodrigues, A.E. (2005) Two-level optimization of an existing SMB for p-xylene separation. Computers & Chemical Engineering, 29: 2215-2228.
47. Storti, G., Mazzotti, M., Morbidelli, M., and Carra, S. (1993) Robust design of binary counter-current adsorption separation processes. AIChE Journal, 39: 471-492.
48. DeVault, D. (1943) The Theory of chromatography. J. Am. Chem. Soc., 65: 532-540.
49. Klein, G., Tondeur, D., and Vermeulen, T. (1967) multicomponent ion exchange in fixed beds: general proprieties of equilibrium systems. Ind Eng. Chem. Fundamentals, 6 (3): 339-351.
50. Tondeur, D. and Klein, G. (1967) Constant-Separation-Factor equilibrium. Ind. Eng. Chem. Fundamentals, 6 (3): 351-361.
51. Helfferich, F.G. (1967) Multicomponent ion exchange in fixed beds: generalized equilibrium theory for systems with constant separation factors. Ind. Eng. Chem. Fundamentals, 6 (3): 362-364.
52. Helfferich, F. and Klein, G. (1970) Multicomponent Chromatography; Marcel Dekker: New York.
53. Rhee, H.-K., Aris, R., and Amundson, N.R. (1970) On the theory of multicomponent chromatography. Phil. Trans. Roy. Soc. London A, 267: 419-455.
54. Mazzotti, M., Storti, G., and Morbidelli, M. (1997) Optimal operation of simulated moving bed units for nonlinear chromatographic separations. J. Chromatography A, 769: 3-24.
55. Migliorini, C., Mazzotti, M., and Morbidelli, M. (2000) Design of simulated moving bed multicomponent separations: Langmuir systems. Sep. and Pur. Tech., 20: 79-96.
56. Leão, C.P. and Rodrigues, A.E. (2004) Computers and Chemical Engineering, 28: 1725-1741.
57. Sá Gomes, P., Leão, C.P., and Rodrigues, A.E. (2007) Simulation of true moving bed adsorptive reactor: detailed particle model and linear driving force approximations. Chemical Engineering Science, 62: 1026-1041.
58. Glueckauf, E. (1955) Theory of chromatography part 10: Formula for diffusion into spheres and their application to chromatography. Trans. Faraday Soc., 51: 1540-1551.
59. Ruthven, D.M. (1984) Principles of Adsorption and Adsorption Processes; John Wiley & Sons Inc.: New York, p. 243.
60. Rodrigues, A.E. and Pais, L.S. (2004) Design of SMB chiral separations units using concept of separation volume. Sep. Sci. and Tech., 39: 245-270.
61. Azevedo, D.C. and Rodrigues, A.E. (1999) Design of a simulated moving bed in the presence of mass-transfer resistances. AIChE Journal, 45: 956-966.
62. Pais, L.S. and Rodrigues, A.E. (2003) Design of simulated moving bed and varicol processes for preparative separations with a low number of columns. J. of Chromatography A, 1006: 33-44.