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2 and oxalic acid was originally intended to make mixed-metal oxalate phosphates; instead, we obtained pentamine occluded zinc phosphate only. Without them, the product tended to be an unidentified emulsion instead of crystalline compound 5.
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2 and oxalic acid was originally intended to make mixed-metal oxalate phosphates; instead, we obtained pentamine occluded zinc phosphate only. Without them, the product tended to be an unidentified emulsion instead of crystalline compound 5.
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25
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38049126943
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Hydrogen atoms of the organic groups were calculated by using a riding model
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Hydrogen atoms of the organic groups were calculated by using a riding model.
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26
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38049157318
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The quality of the crystals of 2 was always too poor to give better refinement results.
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The quality of the crystals of 2 was always too poor to give better refinement results.
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See Supporting Information Figure S9
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See Supporting Information Figure S9.
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