Characterization of the extra-large-pore zeolite UTD-1

Journal of the American Chemical Society

Volumn 119, Issue 36, 1997, Pages 8474-8484

  Lobo, Raul F ^c   Tsapatsis, Michael ^d   Freyhardt, Clemens C ^e,f   Khodabandeh, Shervin ^e   Wagner, Paul ^e   Chen, Cong Yan ^a   Balkus Jr , Kenneth J ^b   Zones, Stacey I ^a   Davis, Mark E ^c,e  

^a CHEVRON ENERGY TECHNOLOGY COMPANY   (United States)

^b UNIVERSITY OF TEXAS AT DALLAS   (United States)

^c University of Delaware   (United States)

^d University of Massachusetts   (United States)

^e California Institute of Technology   (United States)

^f UNIVERSITY OF KONSTANZ   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

CHARACTERIZATION; ELECTRON DIFFRACTION; ISOMERIZATION; MOLECULAR SIEVES; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SCANNING ELECTRON MICROSCOPY; THERMODYNAMIC STABILITY; TRANSMISSION ELECTRON MICROSCOPY; X RAY DIFFRACTION;

EXTRA LARGE PORE ZEOLITE; HIGH SILICA ZEOLITE; HYDROTHERMAL STABILITY;

ZEOLITES;

ZEOLITE;

ARTICLE; DRUG STRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; TRANSMISSION ELECTRON MICROSCOPY; X RAY DIFFRACTION;

EID: 1842369100     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja9708528     Document Type: Article

References (54)

1. Davis, M. E. Chem. Ind. 1992, 137.
2. Shannon, M. D.; Casci, J. L.; Cox, P. A.; Andrews, S. J. Nature 1991, 353, 417-420.
3. Nakagawa, Y. Stud. Surf. Sci. Catal. 1994, 84, 323-330.
4. Zones, S. I.; Olmstead, M. M.; Santilli, D. S. J. Am. Chem. Soc. 1992, 114,4195-4201.
5. Lobo, R. F.; Davis, M. E. J. Am. Chem. Soc. 1995, 117, 3764-3779.
6. (a) Leonowicz, M. E.; Lawton, J. A.; Lawton, S. L.; Rubin, M. K. Science 1994, 264, 1910-1913.
7. (b) Chan, I. Y.; Labun, P. A.; Pan, M.; Zones, S. I. Microporous Mater. 1995, 3, 409-418.
8. Rasband, W., NIH Image, Nat. Inst. Health: Bethesda, MD 1996: version 1.60.
9. Adair, B.; Chen, C. Y.; Wan, K. T.; Davis, M. E. Microporous Mater. 1996, 7,261-270.
10. Balkus, K. J.; Gabrielov, A. G.; Sandler, N. Mater. Res. Soc. Symp. Proc. 1995, 368, 369-375.
11. Balkus, K. J.; Khanmamedova, A.; Gabrierlov, A. G.; Zones, S. I. Stud. Surf. Sci. Catal. 1996, 101, 1341-1348.
12. Balkus, K. J.; Gabrielov, A. G. Synthesis of novel molecular sieves using a metal complex as template. U.S., 5,489,424, 1996.
13. Freyhardt, C. C.; Tsapatsis, M.; Lobo, R. F.; Balkus, K. J.; Davis, M. E. Nature 1996, 381, 295-298.
14. Meier, W. M.; Olson, D. H.; Baerlocher, C. Atlas of Zeolite Structure Types, 4th ed.; Elsevier: London, 1996.
15. Davis, M. E.; Saldarriaga, C.; Montes, C.; Garces, J.; Crowder, C. Nature 1988, 331, 698-699.
16. Dessau, R. M.; Schlenker, J. L.; Higgins, J. B. Zeolites 1990, 10, 522-524.
17. Estermann, M.; McCusker, L. B.; Baerlocher, C.; Merrouch, A.; Kassier, H. Nature 1991, 352, 320-323.
18. Jones, R. H.; Thomas, J. M.; Chen, J. S.; Xu, R. R.; Huo, Q. S.; Li, S. G.; Ma, Z. J. Solid State Chem. 1993, 102, 202-208.
19. Loiseau, T.; Ferey, G. J. Solid State Chem. 1994, 111, 403-415.
20. Loiseau, T.; Ferey, G. J. Mater. Chem. 1996, 6, 1073-1074.
21. Khan, M. I.; Meyer, L. M.; Haushalter, R. C. Chem. Mater. 1996, 8, 43-53.
22. Schindler, M.; Joswig, W.; Baur, W. H. Z. Anorg. Allg. Chem. 1997, 623,45-54.
23. Balkus, K. J.; Gabrielov, A. G.; Zones, S. I.; Chan, I. Y. In Synthesis of Microporous Materials, Zeolites, Clays and Nanocomposites; Kessler, H., Occelli, M., Eds.; Marcel Dekker: New York, 1996.
24. Zones, S. I.; Nakagawa, Y. Microporous Mater. 1994, 2, 543-555.
25. Breck, D. W. Zeolite Molecular Sieves: Structure, Chemistry and Use; Wiley: New York, 1974.
26. Rappe, A. K.; Casewit, C. J.; Colwell, K. S.; Goddard, W. A.; Skiff, W. M. J. Am, Chem. Soc. 1992, 114, 10024-10035.
27. (a) Dessau, R. M.; Schmitt, K. D.; Kerr, G. T.; Woolery, G. L.; Alemany, L. B. J. Catal. 1987, 104, 484-489.
28. (b) Boxhoorn, G., Kortbeek, A. G. T. G., Hays, G. R., Alma, N. C. M. Zeolites 1984, 4, 15-21.
29. Woolery, G. L.; Alemany, L. B.; Dessau, R. M.; Chester, A. W. Zeolites 1986, 6, 14-16.
30. Hunger, M.; Karger, J.; Pfeifer, H.; Caro, J.; Zibrowius, B.; Bulow, M.; Mostowicz, R. J. Chem. Soc., Faraday Trans. I 1987, 83, 3459.
31. Engelhardt, G.; Michel, D. High-Resolution Solid-State NMR of Silicates and Zeolites; Wiley: New York, 1987.
32. Koller, H.; Lobo, R. F.; Burkett, S. L.; Davis, M. E. J. Phys. Chem. 1995, 99, 12588-12596.
33. Lobo, R. F.; Zones, S. I.; Davis, M, E. J. Inclusion Phenom. 1995, 21, 47-78.
34. Bialek, R.; Meier, W, M.; Davis, M. E.; Annen, M. J. Zeolites 1991, 11, 438-442.
35. Richardson, J, W.; Smith, J. V.; Han, S. X. J. Chem. Soc., Faraday Trans. 1990, 86, 2341.
36. Davis, M. E.; Montes, C.; Hathaway, P. E.; Arhancet, J. P.; Hasha, D. L.; Garces, G. J. Am. Chem. Soc. 1989, 111, 3919.
37. Balkus, K. J.; Biscotto, M.; Gabrielov, A. G. Stud. Surf. Sci. Catal. 1997, 105, 415-423.
38. Pan, M. Micron 1996, 27, 219-238.
39. Terasaki, O.; Ohsuna, T. Catal. Today 1995, 23, 201-218.
40. Terasaki, O.; Ohsuna, T.; Sakuma, H.; Watanabe, D.; Nakagawa, Y.; Medrud, R. Chem. Mater. 1996, 8, 463-468.
41. Schlenker, J. L.; Rohrbaugh, W. J.; Chu, P.; Valyocsik, E. W.; Kokotailo, G. T. Zeolites 1985, 5, 355-358.
42. Higgins, J. B. High-Silica Zeolites. In Silica: Physical Behavior, Geochemistry and Materials Applications; Heaney, P. J., Prewitt, C. T., Gibbs, G. V., Eds.; Mineralogical Society of America: Washington, 1994.
43. Lobo, R. F.; Tsapatsis, M.; Freyhardt, C. C.; Chan, I. Y.; Chen, C. Y.; Zones, S. I.; Davis, M. E. J. Am. Chem. Soc. 1997, 119, 3732-3744.
44. Treacy, M. M. J.; Newsam, J. M.; Deem, M. W. Proc. R. Soc. London A 1991, 433, 499-520.
45. Treacy, M. M. J.; Vaughan, D. E. W.; Strohmaier, K. G.; Newsam, J. M. Proc. R. Soc. London A 1996, 452, 813-840.
46. Baerlocher, C.; Hepp, A.; Meier, W. M. DLS-76: A Fortran Program for the Simulation of Crystal Structures by Geometric Refinement; Institut fuer Kristallographie, ETH: Zurich, 1977.
47. Farneth, W. E.; Gorte, R. J. Chem. Rev. 1995, 95, 615-635.
48. Unlike Gorte et al. (see ref 45) we carry out the desorption of the amine from the zeolite in flowing He gas at 1 bar. Gorte et al. carry out their desorption experiments in vacuum and this may be the reason for the polymerization of the propene in the zeolite pores in our experiment.
49. Perez-Pariente, J.; Sastre, E.; Fornes, V.; Martens, J. A.; Jacobs, P. A.; Corma, A. Appl. Catal 1991, 69, 125-137.
50. Martens, J. A.; Perez-Pariente, J.; Sastre, E.; Corma, A.; Jacobs, P. A. Appl. Catal. 1988, 45, 85-101.
51. Weitkamp, J.; Ernst, S. Catal. Today 1994, 19, 107-150.
52. Khodabandeh, S.; Davis, M. E. Manuscript in preparation, 1997.
53. Shen, V.; Bell, A. T. Microporous Mater. 1996, 7, 187-199.
54. Lewis, D. W.; Freeman, C. M.; Catlow, C.R. A. J. Phys Chem. 1995,99, 11194-11202