Preparative isolation and purification of three rotenoids and one isoflavone from the seeds of Millettia pachycarpa Benth by high-speed counter-current chromatography

Journal of Chromatography A

Volumn 1178, Issue 1-2, 2008, Pages 101-107

  Ye, Haoyu ^a   Chen, Lijuan ^a   Li, Yanfang ^b   Peng, Aihua ^a   Fu, Afu ^a   Song, Hang ^b   Tang, Minghai ^a   Luo, Houding ^a   Luo, Youfu ^a   Xu, Yongbin ^a   Shi, Jianyou ^a   Wei, Yuquan ^a  

^a SICHUAN UNIVERSITY   (China)

^b SICHUAN UNIVERSITY   (China)

Author keywords

4 ,5 Dimethoxy 6,6 dimethylpyranoisoflavone; 6a,12a Dehydrodeguelin; Deguelin; HSCCC; Millettia pachycarpa Benth; Tephrosin

Indexed keywords

COUNTER-CURRENT CHROMATOGRAPHY; DEGUELIN; HSCCC; MILLETTIA PACHYCARPA BENTH; TEPHROSIN;

AROMATIC POLYMERS; BIOACTIVITY; CHROMATOGRAPHY; NUCLEAR MAGNETIC RESONANCE; PURIFICATION;

PLANTS (BOTANY);

4',5' DIMETHOXY 6,6 DIMETHYLPYRANOISOFLAVONE; ACETIC ACID ETHYL ESTER; DEGUELIN; DEHYDRODEGUELIN; HEXANE; ISOFLAVONE; METHANOL; ROTENOID; TEPHROSIN; UNCLASSIFIED DRUG; WATER;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; COUNTER CURRENT CHROMATOGRAPHY; DRUG ISOLATION; DRUG PURIFICATION; DRUG STRUCTURE; ELECTROSPRAY MASS SPECTROMETRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MILLETTIA; MILLETTIA PACHYCARPA; NONHUMAN; PLANT SEED; PRIORITY JOURNAL; PROTON NUCLEAR MAGNETIC RESONANCE;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CHROMONES; COUNTERCURRENT DISTRIBUTION; ISOFLAVONES; MAGNETIC RESONANCE SPECTROSCOPY; MILLETTIA; PYRANS; ROTENONE; SEEDS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION;

MILLETTIA;

EID: 37549033426     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2007.11.060     Document Type: Article

References (25)

1. Jiangsu New Medical School, Zhongyao Dacidian, Shanghai Science Technology Press, Shanghai, 1997, p. 1300.
2. Kang J., Chen R.Y., and Yu D.Q. Chin. Trad. Herb. Drugs 34 (2003) 209
3. Gerhäuser C., Mar W., Lee S.K., Suh N., Luo Y., and Kosmeder J. Nat. Med. 1 (1995) 260
4. Fang N., and Casida J.E. Proc. Natl. Acad. Sci. 95 (1998) 3380
5. Murilloa G., Saltia G.I., Kosmeder J.W., Pezzutob J.M., and Mehtaa R.G. Eur. J. Cancer 38 (2002) 2446
6. Peng X.H., Karna P., O'Regan R.M., Liu X.J., Naithani R., Moriarty R.M., Wood W.C., Lee H.Y., and Yang L.l. Mol. Pharmacol. 71 (2007) 101
7. Singhal A.K., Barua N.C., Sharma R.P., and Baruah J.N. Photochemistry 22 (1983) 1005
8. Ito Y. J. Chromatogr. 214 (1981) 122
9. In: Berthod A. (Ed). Countercurrent Chromatography, the Support-free Liquid Stationary Phase, Comprehensive Analytical Chemistry vol. 38 (2002), Elsevier, Amsterdam
10. Chen L.J., Zhang Q., Yang G.L., Fan L.Y., Tang J., Garrard I., Ignatova S.N., Fisher D., and Sutherland I.A. J. Chromatogr. A 1142 (2007) 115
11. Janaway L., Hawes D., Ignatova S.N., Wood P., and Sutherland I.A. J. Liq. Chromatogr. Relat. Technol. 26 (2003) 1345
12. Chen L., Song H., Lan X.Q., Games D.E., and Sutherland I.A. J. Chromatogr. A 1063 (2005) 241
13. Chen L., Han Y.S., Yang F.Q., and Zhang T.Y. J. Chromatogr. A 907 (2001) 343
14. Denis G., Philippe J., Andrée D., Alain B., Bernard F., Yves M., Yves B., and Sylvie B. J. Chromatogr. A 1059 (2004) 73
15. Pan Y., Lu Y., and Liq J. Chromatogr. Relat. Technol. 30 (2007) 649
16. Gu M., Wang X., Su Z., and Ouyang F. J. Chromatogr. A 1140 (2007) 107
17. Zhou T., Zhu Z., Wang C., Fan G., Peng J., Chai Y., and Wu Y. J. Pharm. Biomed. Anal. 44 (2007) 96
18. Ito Y. J. Chromatogr. A 1065 (2005) 145
19. Ma C.J., Li G.S., Zhang D.L., Liu K., and Fan X. J. Chromatogr. A 1078 (2005) 188
20. Peng J.Y., Yang G.J., Fan G.R., and Wu Y.T. J. Chromatogr. A 1092 (2005) 235
21. Peng J.Y., Fan G.R., and Wu Y.T. J. Chromatogr. A 1115 (2006) 103
22. Terada H. Chem. Pharm. Bull. 41 (1993) 187
23. Ashok K.S., Ram P.S., and Jogendra N.B. Phytochemistry 21 (1982) 949
24. Murthy M.S., Rao E.V., and Ward R.S. Magn. Reson. Chem. 24 (1986) 225
25. Somleva T., and Ognyanov I. Planta Med. 43 (1985) 219