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Volumn 7, Issue 12, 2007, Pages 2376-2379

Bimetallic clusters of pyridine-appended ethylenediaminetetraacetic acid (EDTA)-amides in designing ID and 2D coordination frameworks

(2) Rajput, Lalit a Biradha, Kumar a

a INDIAN INSTITUTE OF TECHNOLOGY (India)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 37549003941 PISSN: 15287483 EISSN: None Source Type: Journal
DOI: 10.1021/cg070289x Document Type: Article

Times cited : (15)

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31
- 37548998767
- Several derivatives of 1 (R = 4-pyridyl and substututed phenyl) were prepared in our laboratory. Their crystal structures, cocrystals, coordination polymers, and other properties are under study.
- Several derivatives of 1 (R = 4-pyridyl and substututed phenyl) were prepared in our laboratory. Their crystal structures, cocrystals, coordination polymers, and other properties are under study.

32
- 37549062381
- II were obtained. Slow evaporation of these solutions at room temperature resulted in crystals suitable for single-crystal X-ray diffraction. Further, the usage of excess metal salt (M/L = 6:1) in the reaction also resulted in similar crystals, implying that the complex formation/composition has no dependency on the metal/ligand ratios present in the reaction.
- II were obtained. Slow evaporation of these solutions at room temperature resulted in crystals suitable for single-crystal X-ray diffraction. Further, the usage of excess metal salt (M/L = 6:1) in the reaction also resulted in similar crystals, implying that the complex formation/composition has no dependency on the metal/ligand ratios present in the reaction.

33
- 37549069093
- The X-ray diffraction data were collected on a Bruker SMART Apex diffractometer with CCD detectors, and structures were solved using SHELXTL software. Crystal data 2: triclinic, P1, a= 13.453(3) Å, b, 14.200(3) Å, c, 14.372(3) Å, α, 102.34(3)°, β, 91.96(3)°, γ, 116.04(3)°, V, 2118.9(15) Å3, Z, 1, Dc, 1.426 g cm-3, 4720 reflections of 7074 unique reflections with I > 2σ(I, 1.76° < θ < 28.35°, final R factors R1, 0.0515, wR2, 0.1625. Elemental analysis: C, 39.68, H, 5.40, N, 15.34, caled: C, 39.60, H, 5.50, N, 15.40, yield: 70, Crystal data 3: triclinic, P1, a, 13.269(3) Å, b, 13.674(3) Å, c= 14.545(3) Aring;, a, 92.93(1)°, β= 108.24(1)°, γ, 118.68(1)°, V, 2133.9(15) Å3, Z= 1, Dc, 1.956 g cm-3, 4643 reflections of 10 442 unique reflections with I > 2σI, 1
- 2 = 0.2127. The peaks corresponding to half PFD ion and water molecules exhibited high thermal motions and disorder. Therefore, the Platon squeeze optionwas applied for the final refinement. Elemental analysis: C, 29.75%; H, 3.65%; N, 12.09%; caled: C, 30.07%; H, 4.59%; N, 11.69%, yield: 91%.

34
- 0003992309
- Utrecht University: Utrecht, The Netherlands
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- Spek, A.L.¹

35
- 37549046197
- 2 = 0.2470. In structures 4-6, the peaks corresponding to anions and free water molecules exhibited high thermal motions and heavy disorder. Therefore, the Platon squeeze option was applied to refine the final structures. Elemental analysis: C, 32.37%; H, 5.16%; N, 16.26%; caled: C, 33.13%; H, 5.15%; N, 16.75%, yield: 82%.
- 2 = 0.2470. In structures 4-6, the peaks corresponding to anions and free water molecules exhibited high thermal motions and heavy disorder. Therefore, the Platon squeeze option was applied to refine the final structures. Elemental analysis: C, 32.37%; H, 5.16%; N, 16.26%; caled: C, 33.13%; H, 5.15%; N, 16.75%, yield: 82%.

36
- 33749999987
- Biradha, K.; Sarkar, M.; Rajput, L. Chem. Commun., 2006, 4169.
- (2006) Chem. Commun , pp. 4169
- Biradha, K.¹ Sarkar, M.² Rajput, L.³

37
- 37549057144
- Crystal data 5: monoclinic, C2/c, a, 27.096(3) Å, b, 12.639(1) Å, c, 26.681(2) Å, β= 92.178(2)°, V, 9131.2(15) Å3, Z, 4, Dc, 1.543 g cm-3, 5346 reflections of 7779 unique reflections with I > 2σ(I, 1.50° < θ < 25.00°, final R factors R1, 0.0354, wR2, 0.1417. Elemental analysis: C, 34.72, H, 4.24, N, 17.21, caled: C, 34.61, H, 5.00, N, 17.50, yield: 86, Crystal data 6: monolinic, P2/n, a, 12.733(3) A, b, 12.197(1) Å, c, 32.286(7) Å, β= 96.62(2)°, V, 4980.4(17) Å3, Z, 2, Dc, 1.565 g cm-3, 3874 reflections of 8766 unique reflections with I > 2σI, 1.27° < θ < 25.00°, final R factors R1, 0.0874, wR2, 0.1976. Elemental analysis: C, 30.28, H, 4.32, N, 11.53, caled: C, 30.70, H, 4.43, N, 11.94, yield: 84
- 2 = 0.1976. Elemental analysis: C, 30.28%, H, 4.32%, N, 11.53%; caled: C, 30.70%; H, 4.43%; N, 11.94%, yield: 84%.

38
- 37549034057
- The distances between metal atoms of the two sides of a rectangle were considered as dimensions of SBU
- The distances between metal atoms of the two sides of a rectangle were considered as dimensions of SBU.

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