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Selected details of the X-ray crystal structure analyses: 2·2thf/C6D6: space group: P1, a, 13.3350(5) Å, b, 15.8580(6) Å, c, 22.9500(9) Å, α, 102.371(3) °, β, 91.499(3) °, γ, 107.584(3) °, V, 4497.4(3) Å3, z, 2, reflections collected/unique/observed [I > 2σ(I, 58816/16943/13427, parameters, 933, R (obs, 0.0336, wR 2 (all data, 0.0825, wR2 (obs, 0.0785; 3·2C6D6 space group: P1, a, 14.2870(12) Å, b, 14.3730(10) Å, c, 16.8380(14) Å, α, 114.563(6) °, β, 93.070(6) °, γ, 109.525(6) °, V, 2888.2(4) Å3, z, 1, reflections collected/unique/observed [I > 2σ(I, 37338/10918/5889, parameters, 672, R o
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