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Volumn 30, Issue 5, 2007, Pages 219-235

Using PGSE NMR for chemical mixture analysis: Quantitative aspects

Author keywords

Chemometrics; DECRA; Diffusion; DOSY; Mixture analysis; Pulsed gradient spin echo NMR; Quantitative analysis

Indexed keywords


EID: 34948820148     PISSN: 15466086     EISSN: 15525023     Source Type: Journal    
DOI: 10.1002/cmr.a.20093     Document Type: Article
Times cited : (41)

References (60)
  • 1
    • 0002810616 scopus 로고
    • Measurement of the self-diffusion coefficient of each component in a complex system using pulsed-gradient Fourier transform NMR
    • James TL, McDonald GG. 1973. Measurement of the self-diffusion coefficient of each component in a complex system using pulsed-gradient Fourier transform NMR. J Magn Reson 11:58-61.
    • (1973) J Magn Reson , vol.11 , pp. 58-61
    • James, T.L.1    McDonald, G.G.2
  • 2
    • 33845558390 scopus 로고
    • Molecular self-diffusion coefficients in Fourier transform nuclear magnetic resonance spectrometric analysis of complex mixtures
    • Stilbs P. 1981. Molecular self-diffusion coefficients in Fourier transform nuclear magnetic resonance spectrometric analysis of complex mixtures. Anal Chem 53:2135-2137.
    • (1981) Anal Chem , vol.53 , pp. 2135-2137
    • Stilbs, P.1
  • 3
    • 34047191652 scopus 로고
    • Fourier transform pulsed-gradient spin echo studies of molecular diffusion
    • Stilbs P. 1987. Fourier transform pulsed-gradient spin echo studies of molecular diffusion. Prog Nucl Magn Reson Spectrosc 19:1-45.
    • (1987) Prog Nucl Magn Reson Spectrosc , vol.19 , pp. 1-45
    • Stilbs, P.1
  • 4
    • 0347359145 scopus 로고    scopus 로고
    • Diffusion ordered nuclear magnetic resonance spectroscopy: Principles and applications
    • Johnson CS Jr. 1999. Diffusion ordered nuclear magnetic resonance spectroscopy: principles and applications. Prog Nucl Magn Reson Spectrosc 34:203-256.
    • (1999) Prog Nucl Magn Reson Spectrosc , vol.34 , pp. 203-256
    • Johnson Jr., C.S.1
  • 5
    • 0042372927 scopus 로고    scopus 로고
    • Diffusion ordered spectroscopy (DOSY)
    • Grant DM, Harris RK, eds, New York: Wiley. pp
    • Morris GA. 2002. Diffusion ordered spectroscopy (DOSY). In: Grant DM, Harris RK, eds. Encyclopedia of Nuclear Magnetic Resonance. New York: Wiley. pp 35-44.
    • (2002) Encyclopedia of Nuclear Magnetic Resonance , pp. 35-44
    • Morris, G.A.1
  • 6
    • 0013227077 scopus 로고    scopus 로고
    • Using pulsed gradient spin echo NMR for chemical mixture analysis: How to obtain optimum results
    • Antalek B. 2002. Using pulsed gradient spin echo NMR for chemical mixture analysis: how to obtain optimum results. Concepts Magn Reson 14:225-258.
    • (2002) Concepts Magn Reson , vol.14 , pp. 225-258
    • Antalek, B.1
  • 7
    • 33747155115 scopus 로고    scopus 로고
    • PFG NMR diffusion experiments for complex systems
    • Momot KI, Kuchel PW. 2006. PFG NMR diffusion experiments for complex systems. Concepts Magn Reson A 28:249-269.
    • (2006) Concepts Magn Reson A , vol.28 , pp. 249-269
    • Momot, K.I.1    Kuchel, P.W.2
  • 8
    • 31644450477 scopus 로고    scopus 로고
    • Real life applications of the MULVADO software package for processing DOSY NMR data
    • Huo R, Geurts C, Brandis J, Wehrens R, Buydens LMC. 2006. Real life applications of the MULVADO software package for processing DOSY NMR data. Magn Reson Chem 44:110-117.
    • (2006) Magn Reson Chem , vol.44 , pp. 110-117
    • Huo, R.1    Geurts, C.2    Brandis, J.3    Wehrens, R.4    Buydens, L.M.C.5
  • 9
    • 0032162451 scopus 로고    scopus 로고
    • Diffusion-separated nuclear magnetic resonance spectroscopy of polymer mixtures
    • Jerschow A, Müller N. 1998. Diffusion-separated nuclear magnetic resonance spectroscopy of polymer mixtures. Macromolecules 31:6573-6578.
    • (1998) Macromolecules , vol.31 , pp. 6573-6578
    • Jerschow, A.1    Müller, N.2
  • 11
    • 7444227835 scopus 로고    scopus 로고
    • Measuring ligand-protein binding using NMR diffusion experiments
    • Lucas LH, Larive CK. 2004. Measuring ligand-protein binding using NMR diffusion experiments. Concepts Magn Reson A 20:24-41.
    • (2004) Concepts Magn Reson A , vol.20 , pp. 24-41
    • Lucas, L.H.1    Larive, C.K.2
  • 13
    • 0029905872 scopus 로고    scopus 로고
    • Generalized rank annihilation method applied to a single multicomponent pulsed gradient spin echo NMR data set
    • Antalek B, Windig W. 1996. Generalized rank annihilation method applied to a single multicomponent pulsed gradient spin echo NMR data set. J Am Chem Soc 118:10331-10332.
    • (1996) J Am Chem Soc , vol.118 , pp. 10331-10332
    • Antalek, B.1    Windig, W.2
  • 14
    • 0030754619 scopus 로고    scopus 로고
    • Direct exponential curve resolution algorithm (DECRA): A novel application of the generalized rank annihilation method for a single spectral mixture data set with exponentially decaying contribution profiles
    • Windig W, Antalek B. 1997. Direct exponential curve resolution algorithm (DECRA): a novel application of the generalized rank annihilation method for a single spectral mixture data set with exponentially decaying contribution profiles. Chemom Intell Lab Syst 37:241-254.
    • (1997) Chemom Intell Lab Syst , vol.37 , pp. 241-254
    • Windig, W.1    Antalek, B.2
  • 15
    • 0002256081 scopus 로고    scopus 로고
    • Applications and new developments of the direct exponential curve resolution algorithm (DECRA). Examples of spectra and magnetic resonance images
    • Windig W, Antalek B, Sorriero L, Bijlsma S, Louwerse DJ, Smilde A. 1999. Applications and new developments of the direct exponential curve resolution algorithm (DECRA). Examples of spectra and magnetic resonance images. J Chemom 13:95-110.
    • (1999) J Chemom , vol.13 , pp. 95-110
    • Windig, W.1    Antalek, B.2    Sorriero, L.3    Bijlsma, S.4    Louwerse, D.J.5    Smilde, A.6
  • 16
    • 33745700267 scopus 로고    scopus 로고
    • Accounting for spin relaxation in quantitative PGSE NMR mixture analysis
    • Antalek B. 2006. Accounting for spin relaxation in quantitative PGSE NMR mixture analysis. J Am Chem Soc 128:8402-8403.
    • (2006) J Am Chem Soc , vol.128 , pp. 8402-8403
    • Antalek, B.1
  • 17
    • 34247324472 scopus 로고    scopus 로고
    • Optical molecular imaging agents for cancer diagnostics and therapeutics
    • Kumar S, Richards-Kortum R. 2006. Optical molecular imaging agents for cancer diagnostics and therapeutics. Nanomedicine 1:23-30.
    • (2006) Nanomedicine , vol.1 , pp. 23-30
    • Kumar, S.1    Richards-Kortum, R.2
  • 18
    • 0029360322 scopus 로고
    • Which polymers can make nanoparticulate drug carriers long-circulating?
    • Torchilin VP, Trubetskoy VS. 1995. Which polymers can make nanoparticulate drug carriers long-circulating? Adv Drug Delivery Rev 16:141-155.
    • (1995) Adv Drug Delivery Rev , vol.16 , pp. 141-155
    • Torchilin, V.P.1    Trubetskoy, V.S.2
  • 21
    • 33646376290 scopus 로고
    • Spin diffusion measurements: Spin echoes in the presence of a time-dependent field gradient
    • Stejskal EO, Tanner JE. 1965. Spin diffusion measurements: spin echoes in the presence of a time-dependent field gradient. J Chem Phys 42:288-292.
    • (1965) J Chem Phys , vol.42 , pp. 288-292
    • Stejskal, E.O.1    Tanner, J.E.2
  • 22
    • 33749622370 scopus 로고
    • Spin echoes
    • Hahn EL. 1950. Spin echoes. Phys Rev 80:580-594.
    • (1950) Phys Rev , vol.80 , pp. 580-594
    • Hahn, E.L.1
  • 23
    • 33847534249 scopus 로고
    • Effects of diffusion on free precession in nuclear magnetic resonance experiments
    • Carr HY, Purcell EM. 1954. Effects of diffusion on free precession in nuclear magnetic resonance experiments. Phys Rev 94:630-638.
    • (1954) Phys Rev , vol.94 , pp. 630-638
    • Carr, H.Y.1    Purcell, E.M.2
  • 24
    • 0031498272 scopus 로고    scopus 로고
    • Pulsed-field gradient nuclear magnetic resonance as a tool for studying translational diffusion. II. Experimental aspects
    • Price WS. 1997. Pulsed-field gradient nuclear magnetic resonance as a tool for studying translational diffusion. II. Experimental aspects. Concepts Magn Reson 9:299-336.
    • (1997) Concepts Magn Reson , vol.9 , pp. 299-336
    • Price, W.S.1
  • 25
    • 36849101148 scopus 로고
    • The use of the stimulated echo in NMR diffusion studies
    • Tanner JE. 1970. The use of the stimulated echo in NMR diffusion studies. J Chem Phys 52:2523-2526.
    • (1970) J Chem Phys , vol.52 , pp. 2523-2526
    • Tanner, J.E.1
  • 27
    • 28044451282 scopus 로고    scopus 로고
    • Improving pulse sequences for 3D DOSY: Convection compensation
    • Nilsson M, Morris GA. 2005. Improving pulse sequences for 3D DOSY: convection compensation. J Magn Reson 177:203-211.
    • (2005) J Magn Reson , vol.177 , pp. 203-211
    • Nilsson, M.1    Morris, G.A.2
  • 28
    • 33746276198 scopus 로고    scopus 로고
    • An improved method for suppressing protein background in PEG NMR experiments to determine ligand coefficients in the presence of receptor
    • Becker BA, Morris KF, Larive CK. 2006. An improved method for suppressing protein background in PEG NMR experiments to determine ligand coefficients in the presence of receptor. J Magn Reson 181:327-330.
    • (2006) J Magn Reson , vol.181 , pp. 327-330
    • Becker, B.A.1    Morris, K.F.2    Larive, C.K.3
  • 29
  • 30
    • 58149362694 scopus 로고
    • An improved diffusion-ordered spectroscopy experiment incorporating bipolar gradient pulses
    • Wu D, Chen A, Johnson CS Jr. 1995. An improved diffusion-ordered spectroscopy experiment incorporating bipolar gradient pulses. J Magn Reson Ser A 115:260-264.
    • (1995) J Magn Reson Ser A , vol.115 , pp. 260-264
    • Wu, D.1    Chen, A.2    Johnson Jr., C.S.3
  • 31
    • 0000657454 scopus 로고    scopus 로고
    • Cross-relaxation effects in stimulated echo-type PGSE NMR experiments by bipolar and monopolar gradient pulses
    • Dvinskikh SV, Furó I. 2000. Cross-relaxation effects in stimulated echo-type PGSE NMR experiments by bipolar and monopolar gradient pulses. J Magn Reson 146:283-289.
    • (2000) J Magn Reson , vol.146 , pp. 283-289
    • Dvinskikh, S.V.1    Furó, I.2
  • 32
    • 0000082309 scopus 로고    scopus 로고
    • Cross-relaxation in pulsed-field-gradient stimulated echo measurements on water in a macromolecular matrix
    • Pescher LJC, Bouwstra JA, de Bleyser J, Junginger HE, Leyte JC. 1996. Cross-relaxation in pulsed-field-gradient stimulated echo measurements on water in a macromolecular matrix. J Magn Reson Ser B 110:150-157.
    • (1996) J Magn Reson Ser B , vol.110 , pp. 150-157
    • Pescher, L.J.C.1    Bouwstra, J.A.2    de Bleyser, J.3    Junginger, H.E.4    Leyte, J.C.5
  • 33
    • 0033538276 scopus 로고    scopus 로고
    • Nuclear overhauser effect on diffusion measurements
    • Chen A, Shapiro MJ. 1999. Nuclear overhauser effect on diffusion measurements. J Am Chem Soc 121: 5338-5339.
    • (1999) J Am Chem Soc , vol.121 , pp. 5338-5339
    • Chen, A.1    Shapiro, M.J.2
  • 36
    • 0037554150 scopus 로고
    • Relaxation of AB systems in stimulated echo spectroscopy
    • Straubinger K, Schick F, Lutz O. 1995. Relaxation of AB systems in stimulated echo spectroscopy. J Magn Reson Ser B 109:251-258.
    • (1995) J Magn Reson Ser B , vol.109 , pp. 251-258
    • Straubinger, K.1    Schick, F.2    Lutz, O.3
  • 38
    • 0025186604 scopus 로고
    • A new method for the analysis of correlated data using Procrustes rotation which is suitable for spectral analysis
    • Kubista M. 1990. A new method for the analysis of correlated data using Procrustes rotation which is suitable for spectral analysis. Chemom Intell Lab Syst 7:273-279.
    • (1990) Chemom Intell Lab Syst , vol.7 , pp. 273-279
    • Kubista, M.1
  • 39
    • 0001635164 scopus 로고
    • Analysis of correlated spectral data
    • Scarminio I, Kubista M. 1993. Analysis of correlated spectral data. Anal Chem 65:409-416.
    • (1993) Anal Chem , vol.65 , pp. 409-416
    • Scarminio, I.1    Kubista, M.2
  • 40
    • 84984336824 scopus 로고
    • Comments on data analysis (datan) algorithm and rank annihilation factor analysis for the analysis of correlated spectral data
    • Booksh KS, Kowalski BR. 1994. Comments on data analysis (datan) algorithm and rank annihilation factor analysis for the analysis of correlated spectral data. J Chemom 8:287-292.
    • (1994) J Chemom , vol.8 , pp. 287-292
    • Booksh, K.S.1    Kowalski, B.R.2
  • 41
    • 26444570774 scopus 로고
    • Generalized rank annihilation factor analysis
    • Sanchez E, Kowalski BR. 1986. Generalized rank annihilation factor analysis. Anal Chem 58:496-499.
    • (1986) Anal Chem , vol.58 , pp. 496-499
    • Sanchez, E.1    Kowalski, B.R.2
  • 42
    • 0000904076 scopus 로고
    • An improved algorithm for the generalized rank annihilation method
    • Wilson BE, Sanchez E, Kowalski BR. 1989. An improved algorithm for the generalized rank annihilation method. J Chemom 3:493-498.
    • (1989) J Chemom , vol.3 , pp. 493-498
    • Wilson, B.E.1    Sanchez, E.2    Kowalski, B.R.3
  • 43
    • 43949173362 scopus 로고
    • Analysis of multicomponent FT-PGSE experiments by multivariate statistical methods applied to the complete bandshapes
    • Schulze D, Stilbs P. 1993. Analysis of multicomponent FT-PGSE experiments by multivariate statistical methods applied to the complete bandshapes. J Magn Reson Ser A 105:54-58.
    • (1993) J Magn Reson Ser A , vol.105 , pp. 54-58
    • Schulze, D.1    Stilbs, P.2
  • 44
    • 1042268190 scopus 로고    scopus 로고
    • Effect of non-exponential and multi-exponential decay behavior on the performance of the direct exponential curve resolution algorithm (DECRA) in NMR investigations
    • Alam TM, Alam MK. 2003. Effect of non-exponential and multi-exponential decay behavior on the performance of the direct exponential curve resolution algorithm (DECRA) in NMR investigations. J Chemom 17:583-593.
    • (2003) J Chemom , vol.17 , pp. 583-593
    • Alam, T.M.1    Alam, M.K.2
  • 45
    • 0001494550 scopus 로고    scopus 로고
    • Multivariate image analysis of magnetic resonance images with the direct exponential curve resolution algorithm (DECRA). I. Algorithm and model study
    • Windig W, Hornak JP, Antalek B. 1998. Multivariate image analysis of magnetic resonance images with the direct exponential curve resolution algorithm (DECRA). I. Algorithm and model study. J Magn Reson 132:298-306.
    • (1998) J Magn Reson , vol.132 , pp. 298-306
    • Windig, W.1    Hornak, J.P.2    Antalek, B.3
  • 46
    • 0032087380 scopus 로고    scopus 로고
    • Multivariate image analysis of magnetic resonance images with the direct exponential curve resolution algorithm (DECRA). II. Application to human brain images
    • Antalek B, Hornak JP, Windig W. 1998. Multivariate image analysis of magnetic resonance images with the direct exponential curve resolution algorithm (DECRA). II. Application to human brain images. J Magn Reson 132:307-315.
    • (1998) J Magn Reson , vol.132 , pp. 307-315
    • Antalek, B.1    Hornak, J.P.2    Windig, W.3
  • 47
    • 0033652458 scopus 로고    scopus 로고
    • Applications of the direct exponential curve resolution algorithm (DECRA) to solid state nuclear magnetic resonance and mid-infrared spectra
    • Windig W, Antalek B, Robbins MJ, Zumbulyadis N, Heckler CE. 2000. Applications of the direct exponential curve resolution algorithm (DECRA) to solid state nuclear magnetic resonance and mid-infrared spectra. J Chemom 14:213-227.
    • (2000) J Chemom , vol.14 , pp. 213-227
    • Windig, W.1    Antalek, B.2    Robbins, M.J.3    Zumbulyadis, N.4    Heckler, C.E.5
  • 48
    • 0033573127 scopus 로고    scopus 로고
    • Elucidation of polymorph mixtures using solid-state 13C CP/MAS NMR spectroscopy and direct exponential curve resolution algorithm
    • Zumbulyadis N, Antalek B, Windig W, Scaringe RP, Lanzafame AM, Blanton T, et al. 1999. Elucidation of polymorph mixtures using solid-state 13C CP/MAS NMR spectroscopy and direct exponential curve resolution algorithm. J Am Chem Soc 121:11554-11557.
    • (1999) J Am Chem Soc , vol.121 , pp. 11554-11557
    • Zumbulyadis, N.1    Antalek, B.2    Windig, W.3    Scaringe, R.P.4    Lanzafame, A.M.5    Blanton, T.6
  • 49
    • 0042143259 scopus 로고    scopus 로고
    • PGSE-WATERGATE, a new tool for NMR diffusion-based studies of ligand-macrmolecule binding
    • Price WS, Elwinger F, Vigoureux C, Stilbs P. 2002. PGSE-WATERGATE, a new tool for NMR diffusion-based studies of ligand-macrmolecule binding. Magn Reson Chem 40:391-395.
    • (2002) Magn Reson Chem , vol.40 , pp. 391-395
    • Price, W.S.1    Elwinger, F.2    Vigoureux, C.3    Stilbs, P.4
  • 50
    • 2942525657 scopus 로고    scopus 로고
    • Convection-compensating PGSE experiment incorporating excitation-sculpting water suppression (CONVEX)
    • Momot KI, Kuchel PW. 2004. Convection-compensating PGSE experiment incorporating excitation-sculpting water suppression (CONVEX). J Magn Reson 169:92-101.
    • (2004) J Magn Reson , vol.169 , pp. 92-101
    • Momot, K.I.1    Kuchel, P.W.2
  • 51
    • 0032134648 scopus 로고    scopus 로고
    • Practical aspects of the measurement of the diffusion of proteins in aqueous solution
    • Tillet ML, Lu-Yun L, Norwood TJ. 1998. Practical aspects of the measurement of the diffusion of proteins in aqueous solution. J Magn Reson 133:379-384.
    • (1998) J Magn Reson , vol.133 , pp. 379-384
    • Tillet, M.L.1    Lu-Yun, L.2    Norwood, T.J.3
  • 52
    • 58149365344 scopus 로고
    • Wet solvent suppression and its applications to LC NMR and high-resolution NMR spectroscopy
    • Smallcombe SH, Patt SL, Keifer PA. 1995. Wet solvent suppression and its applications to LC NMR and high-resolution NMR spectroscopy. J Magn Reson Ser A 117:295-303.
    • (1995) J Magn Reson Ser A , vol.117 , pp. 295-303
    • Smallcombe, S.H.1    Patt, S.L.2    Keifer, P.A.3
  • 53
    • 0030134645 scopus 로고    scopus 로고
    • Global least-squares analysis of large, correlated spectral data sets: Application to component-resolved FT-PGSE NMR spectroscopy
    • Stilbs P, Paulsen K, Griffiths PC. 1996. Global least-squares analysis of large, correlated spectral data sets: application to component-resolved FT-PGSE NMR spectroscopy. J Phys Chem 100:8180-8189.
    • (1996) J Phys Chem , vol.100 , pp. 8180-8189
    • Stilbs, P.1    Paulsen, K.2    Griffiths, P.C.3
  • 54
    • 0001225297 scopus 로고    scopus 로고
    • Analysis of DOSY and GPC-NMR experiments on polymers by multivariate curve resolution
    • Van Gorkom LCM, Hancewicz TM. 1998. Analysis of DOSY and GPC-NMR experiments on polymers by multivariate curve resolution. J Magn Reson 130:125-130.
    • (1998) J Magn Reson , vol.130 , pp. 125-130
    • Van Gorkom, L.C.M.1    Hancewicz, T.M.2
  • 57
    • 24444473406 scopus 로고
    • Suppression of J-modulation effects for resonance editing by NMR spin-echo experiments
    • Mahi L, Duplan JC, Fenet B. 1993. Suppression of J-modulation effects for resonance editing by NMR spin-echo experiments. Chem Phys Lett 211:27-30.
    • (1993) Chem Phys Lett , vol.211 , pp. 27-30
    • Mahi, L.1    Duplan, J.C.2    Fenet, B.3
  • 58
    • 25144444206 scopus 로고    scopus 로고
    • Acquisition of pure-phase diffusion spectra using oscillating-gradient spin echo
    • Momot KI, Kuchel PW, Chapman BE. Acquisition of pure-phase diffusion spectra using oscillating-gradient spin echo. J Magn Reson 176:151-159.
    • J Magn Reson , vol.176 , pp. 151-159
    • Momot, K.I.1    Kuchel, P.W.2    Chapman, B.E.3
  • 59
    • 0033876007 scopus 로고    scopus 로고
    • Self-assembled monolayers of alkanoic acids: A solid-state NMR study
    • Pawsey S, Yach K, Halla J, Reven L. 2000. Self-assembled monolayers of alkanoic acids: a solid-state NMR study. Langmuir 16:3294-3303.
    • (2000) Langmuir , vol.16 , pp. 3294-3303
    • Pawsey, S.1    Yach, K.2    Halla, J.3    Reven, L.4
  • 60
    • 0037455836 scopus 로고    scopus 로고
    • Formation of silica/poly(p-dioxanone) microspheres by surface-initiated polymerization
    • Yoon KR, Koh Y-J, Choi IS. 2003. Formation of silica/poly(p-dioxanone) microspheres by surface-initiated polymerization. Macromol Rapid Commun 24:207-210.
    • (2003) Macromol Rapid Commun , vol.24 , pp. 207-210
    • Yoon, K.R.1    Koh, Y.-J.2    Choi, I.S.3


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