메뉴 건너뛰기




Volumn 14, Issue 4, 2002, Pages 225-258

Using pulsed gradient spin echo NMR for chemical mixture analysis: How to obtain optimum results

Author keywords

Chemometrics; Diffusion; Diffusion ordered spectroscopy; Direct exponential curve resolution algorithm; Mixture analysis; Pulsed gradient spin echo NMR

Indexed keywords

ANALYTIC METHOD; ARTICLE; ARTIFACT; CHEMICAL ANALYSIS; DATA ANALYSIS; DIFFUSION COEFFICIENT; INFORMATION PROCESSING; MOLECULAR SIZE; NUCLEAR MAGNETIC RESONANCE; PULSED GRADIENT SPIN ECHO NUCLEAR MAGNETIC RESONANCE; SEPARATION TECHNIQUE;

EID: 0013227077     PISSN: 15466086     EISSN: None     Source Type: Journal    
DOI: 10.1002/cmr.10026     Document Type: Article
Times cited : (287)

References (104)
  • 1
    • 84991411436 scopus 로고
    • 'Online' liquid chromatography/nuclear magnetic resonance mass spectrometry - A powerful spectroscopic tool for the analysis of mixtures of pharmaceutical interest
    • Pullen FS, Swanson AG, Newman MJ, Richards DS. 'Online' liquid chromatography/nuclear magnetic resonance mass spectrometry - A powerful spectroscopic tool for the analysis of mixtures of pharmaceutical interest. Rapid Commun Mass Spectrom 1995; 9:1003-1006.
    • (1995) Rapid Commun Mass Spectrom , vol.9 , pp. 1003-1006
    • Pullen, F.S.1    Swanson, A.G.2    Newman, M.J.3    Richards, D.S.4
  • 2
    • 0030300931 scopus 로고    scopus 로고
    • Combined HPLC, NMR spectroscopy, and ion-trap mass spectrometry with application to the detection and characterization of xenobiotic and endogenous metabolites in human urine
    • Shockcor JP, Unger SH, Wilson ID, Foxall PJD, Nicholson JK, Lindon JC. Combined HPLC, NMR spectroscopy, and ion-trap mass spectrometry with application to the detection and characterization of xenobiotic and endogenous metabolites in human urine. Anal Chem 1996; 68:4431-4435.
    • (1996) Anal Chem , vol.68 , pp. 4431-4435
    • Shockcor, J.P.1    Unger, S.H.2    Wilson, I.D.3    Foxall, P.J.D.4    Nicholson, J.K.5    Lindon, J.C.6
  • 4
    • 0035843932 scopus 로고    scopus 로고
    • Combination of matrix solid-phase dispersion extraction and direct on-line liquid chromatography-nuclear magnetic resonance spectroscopy-tandem mass spectrometry as a new efficient approach for the rapid screening of natural products: Application to the total asterosaponin fraction of the starfish Asterias rubens
    • Sandvoss M, Weltring A, Preiss A, Levsen K, Wuensch G. Combination of matrix solid-phase dispersion extraction and direct on-line liquid chromatography-nuclear magnetic resonance spectroscopy-tandem mass spectrometry as a new efficient approach for the rapid screening of natural products: Application to the total asterosaponin fraction of the starfish Asterias rubens. J Chromatogr A 2001; 917:75-86.
    • (2001) J Chromatogr A , vol.917 , pp. 75-86
    • Sandvoss, M.1    Weltring, A.2    Preiss, A.3    Levsen, K.4    Wuensch, G.5
  • 7
    • 34047191652 scopus 로고
    • Fourier transform pulsed-gradient spin-echo studies of molecular diffusion
    • Stilbs P. Fourier transform pulsed-gradient spin-echo studies of molecular diffusion. Prog NMR Spectrosc 1987; 19:1-45.
    • (1987) Prog NMR Spectrosc , vol.19 , pp. 1-45
    • Stilbs, P.1
  • 8
    • 0031498272 scopus 로고    scopus 로고
    • Pulsed-field gradient nuclear magnetic resonance as a tool for studying translational diffusion: Part I. Basic theory
    • Price WS. Pulsed-field gradient nuclear magnetic resonance as a tool for studying translational diffusion: Part I. Basic theory. Concepts Magn Reson 1997; 9:299-336.
    • (1997) Concepts Magn Reson , vol.9 , pp. 299-336
    • Price, W.S.1
  • 9
    • 0031498272 scopus 로고    scopus 로고
    • Pulsed-field gradient nuclear magnetic resonance as a tool for studying translational diffusion: Part II. Experimental aspects
    • Price WS. Pulsed-field gradient nuclear magnetic resonance as a tool for studying translational diffusion: Part II. Experimental aspects. Concepts Magn Reson 1997; 9:299-336.
    • (1997) Concepts Magn Reson , vol.9 , pp. 299-336
    • Price, W.S.1
  • 10
    • 33646376290 scopus 로고
    • Spin diffusion measurements: Spin echoes in the presence of a time-dependent field gradient
    • Stejskal EO, Tanner JE. Spin diffusion measurements: Spin echoes in the presence of a time-dependent field gradient. J Chem Phys 1965; 42:288-292.
    • (1965) J Chem Phys , vol.42 , pp. 288-292
    • Stejskal, E.O.1    Tanner, J.E.2
  • 11
    • 36849101148 scopus 로고    scopus 로고
    • The use of the stimulated echo in NMR diffusion studies
    • 190
    • Tanner JE. The use of the stimulated echo in NMR diffusion studies. J Chem Phys 190; 52:2523-2526.
    • J Chem Phys , vol.52 , pp. 2523-2526
    • Tanner, J.E.1
  • 12
    • 36849100445 scopus 로고
    • Restricted self-diffusion of protons in colloidal systems by the pulsed-gradient, spin-echo method
    • Tanner JE, Stejskal EO. Restricted self-diffusion of protons in colloidal systems by the pulsed-gradient, spin-echo method. J Chem Phys 1968; 49:1768-1777.
    • (1968) J Chem Phys , vol.49 , pp. 1768-1777
    • Tanner, J.E.1    Stejskal, E.O.2
  • 13
    • 49649143174 scopus 로고
    • Pulsed NMR studies of restricted diffusion
    • Packer KJ, Rees C. Pulsed NMR studies of restricted diffusion. J Colloid Interface Sci 1972; 40:206-218.
    • (1972) J Colloid Interface Sci , vol.40 , pp. 206-218
    • Packer, K.J.1    Rees, C.2
  • 14
    • 33845558390 scopus 로고
    • Molecular self-diffusion coefficients in Fourier transform nuclear magnetic resonance spectrometric analysis of complex mixtures
    • Stilbs P. Molecular self-diffusion coefficients in Fourier transform nuclear magnetic resonance spectrometric analysis of complex mixtures. Anal Chem 1981; 53:2135-2137.
    • (1981) Anal Chem , vol.53 , pp. 2135-2137
    • Stilbs, P.1
  • 15
    • 0347359145 scopus 로고    scopus 로고
    • Diffusion ordered nuclear magnetic resonance spectroscopy: Principles, applications
    • Johnson CS Jr. Diffusion ordered nuclear magnetic resonance spectroscopy: principles, applications. Prog NMR Spectrosc 1999; 34:203-256.
    • (1999) Prog NMR Spectrosc , vol.34 , pp. 203-256
    • Johnson Jr., C.S.1
  • 16
    • 0001098519 scopus 로고
    • Diffusion-ordered two-dimensional nuclear magnetic resonance spectroscopy
    • Morris KF, Johnson CS Jr. Diffusion-ordered two-dimensional nuclear magnetic resonance spectroscopy. J Am Chem Soc 1992; 114:3139-3141.
    • (1992) J Am Chem Soc , vol.114 , pp. 3139-3141
    • Morris, K.F.1    Johnson Jr., C.S.2
  • 17
    • 0000673856 scopus 로고
    • Resolution of discrete, continuous molecular size distribution by means of diffusion-ordered 2D NMR
    • Morris KF, Johnson CS Jr. Resolution of discrete, continuous molecular size distribution by means of diffusion-ordered 2D NMR. J Am Chem Soc 1993; 115:4291-4299.
    • (1993) J Am Chem Soc , vol.115 , pp. 4291-4299
    • Morris, K.F.1    Johnson Jr., C.S.2
  • 18
    • 0029905872 scopus 로고    scopus 로고
    • Generalized rank annihilation method applied to a single multicomponent pulsed gradient spin echo NMR data set
    • Antalek B, Windig W. Generalized rank annihilation method applied to a single multicomponent pulsed gradient spin echo NMR data set. J Am Chem Soc 1996; 118:10331-10332.
    • (1996) J Am Chem Soc , vol.118 , pp. 10331-10332
    • Antalek, B.1    Windig, W.2
  • 19
    • 0030754619 scopus 로고    scopus 로고
    • Direct exponential curve resolution algorithm (DECRA): A novel application of the generalized rank annihilation method for a single spectral mixture data set with exponentially decaying contribution profiles
    • Windig W, Antalek B. Direct exponential curve resolution algorithm (DECRA): A novel application of the generalized rank annihilation method for a single spectral mixture data set with exponentially decaying contribution profiles. Chemom Intell Lab Syst 1997; 37:241-254.
    • (1997) Chemom Intell Lab Syst , vol.37 , pp. 241-254
    • Windig, W.1    Antalek, B.2
  • 20
    • 0033560017 scopus 로고    scopus 로고
    • Resolving nuclear magnetic resonance data of complex mixtures by three-way methods: Examples of chemical solutions and the human brain
    • Windig W, Antalek B. Resolving nuclear magnetic resonance data of complex mixtures by three-way methods: Examples of chemical solutions and the human brain. Chemom Intell Lab Syst 1999; 46:207-219.
    • (1999) Chemom Intell Lab Syst , vol.46 , pp. 207-219
    • Windig, W.1    Antalek, B.2
  • 21
    • 0030134645 scopus 로고    scopus 로고
    • Global least-squares analysis of large, correlated spectral data sets: Application to component-resolved FT-PGSE NMR spectroscopy
    • Stilbs P, Paulsen K, Griffiths PC. Global least-squares analysis of large, correlated spectral data sets: Application to component-resolved FT-PGSE NMR spectroscopy. J Phys Chem 1996; 100:8180-8189.
    • (1996) J Phys Chem , vol.100 , pp. 8180-8189
    • Stilbs, P.1    Paulsen, K.2    Griffiths, P.C.3
  • 22
    • 0031555733 scopus 로고    scopus 로고
    • FT-PGSE NMR study of mixed micellization of an anionic and a sugar-based nonionic surfactant
    • Griffiths PC, Stilbs P, Paulsen K, Howe AM, Pitt AR. FT-PGSE NMR study of mixed micellization of an anionic and a sugar-based nonionic surfactant. J Phys Chem B 1997; 101:915-918.
    • (1997) J Phys Chem B , vol.101 , pp. 915-918
    • Griffiths, P.C.1    Stilbs, P.2    Paulsen, K.3    Howe, A.M.4    Pitt, A.R.5
  • 23
    • 0030402985 scopus 로고    scopus 로고
    • Global least-squares analysis of large, correlated spectral data sets. Application to chemical kinetics and time-resolved fluorescence
    • Stilbs P, Paulsen K. Global least-squares analysis of large, correlated spectral data sets. Application to chemical kinetics and time-resolved fluorescence. Rev Sci Instrum 1996; 67:4380-4386.
    • (1996) Rev Sci Instrum , vol.67 , pp. 4380-4386
    • Stilbs, P.1    Paulsen, K.2
  • 24
    • 0001225297 scopus 로고    scopus 로고
    • Analysis of DOSY and GPC-NMR experiments on polymers by multivariate curve resolution
    • Van Gorkom LCM, Hancewicz TM. Analysis of DOSY and GPC-NMR experiments on polymers by multivariate curve resolution. J Magn Reson 1998; 130:125-130.
    • (1998) J Magn Reson , vol.130 , pp. 125-130
    • Van Gorkom, L.C.M.1    Hancewicz, T.M.2
  • 25
    • 0033353595 scopus 로고    scopus 로고
    • Use of PFG-NMR for mixture analysis: Measurement of diffusion coefficients of cis and trans isomers of proline-containing peptides
    • Derrick TS, Larive CK. Use of PFG-NMR for mixture analysis: Measurement of diffusion coefficients of cis and trans isomers of proline-containing peptides. Appl Spectrosc 1999; 53:1595-1600.
    • (1999) Appl Spectrosc , vol.53 , pp. 1595-1600
    • Derrick, T.S.1    Larive, C.K.2
  • 26
    • 0032351694 scopus 로고    scopus 로고
    • Polymer additives mixture analysis using pulsed-field gradient NMR spectroscopy
    • Jayawickrama AD, Larive CK, McCord EF, Roe CD. Polymer additives mixture analysis using pulsed-field gradient NMR spectroscopy. Magn Reson Chem 1998; 36:755-760.
    • (1998) Magn Reson Chem , vol.36 , pp. 755-760
    • Jayawickrama, A.D.1    Larive, C.K.2    McCord, E.F.3    Roe, C.D.4
  • 27
    • 0033702584 scopus 로고    scopus 로고
    • Analysis of hydrocarbon mixtures by diffusion-ordered NMR spectroscopy
    • Kapur GS, Findeisen M, Berger S. Analysis of hydrocarbon mixtures by diffusion-ordered NMR spectroscopy. Fuel 2000; 79:1347-1351.
    • (2000) Fuel , vol.79 , pp. 1347-1351
    • Kapur, G.S.1    Findeisen, M.2    Berger, S.3
  • 29
    • 0001002874 scopus 로고
    • High-resolution diffusion-ordered 2D spectroscopy (HR-DOSY) - A new tool for the analysis of complex mixtures
    • Barjat H, Morris GA, Smart S, Swanson AG, Wiliams SCR. High-resolution diffusion-ordered 2D spectroscopy (HR-DOSY) - A new tool for the analysis of complex mixtures. J Magn Reson Ser B 1995; 108:170-172.
    • (1995) J Magn Reson Ser B , vol.108 , pp. 170-172
    • Barjat, H.1    Morris, G.A.2    Smart, S.3    Swanson, A.G.4    Wiliams, S.C.R.5
  • 30
    • 0028327522 scopus 로고
    • Analysis of mixtures based on molecular size, hydrophobicity by means of diffusion-ordered 2D NMR
    • Morris KF, Stilbs P, Johnson CS Jr. Analysis of mixtures based on molecular size, hydrophobicity by means of diffusion-ordered 2D NMR. Anal Chem 1994; 66:211-215.
    • (1994) Anal Chem , vol.66 , pp. 211-215
    • Morris, K.F.1    Stilbs, P.2    Johnson Jr., C.S.3
  • 31
    • 0032162451 scopus 로고    scopus 로고
    • Diffusion-separated nuclear magnetic resonance spectroscopy of polymer mixtures
    • Jerschow A, Müller N. Diffusion-separated nuclear magnetic resonance spectroscopy of polymer mixtures. Macromolecules 1998; 31:6573-6578.
    • (1998) Macromolecules , vol.31 , pp. 6573-6578
    • Jerschow, A.1    Müller, N.2
  • 32
    • 0034514817 scopus 로고    scopus 로고
    • Micellization of sodium dodecyl sulfate with a series of nonionic n-alkyl malono-bis-N-methylglucamides in the presence and absence of gelatin
    • Griffiths PC, Roe JA, Jenkins RL, Reeve J, Cheung AYF, Hall DG, Pitt AR, Howe AM. Micellization of sodium dodecyl sulfate with a series of nonionic n-alkyl malono-bis-N-methylglucamides in the presence and absence of gelatin. Langmuir 2000; 16:9983-9990.
    • (2000) Langmuir , vol.16 , pp. 9983-9990
    • Griffiths, P.C.1    Roe, J.A.2    Jenkins, R.L.3    Reeve, J.4    Cheung, A.Y.F.5    Hall, D.G.6    Pitt, A.R.7    Howe, A.M.8
  • 33
    • 0002256081 scopus 로고    scopus 로고
    • Applications and new developments of the direct exponential curve resolution algorithm (DECRA). Examples of spectra and magnetic resonance images
    • Windig W, Antalek B, Sorriero L, Bijlsma S, Louwerse DJ, Smilde A. Applications and new developments of the direct exponential curve resolution algorithm (DECRA). Examples of spectra and magnetic resonance images. J Chemom 1999; 13:95-110.
    • (1999) J Chemom , vol.13 , pp. 95-110
    • Windig, W.1    Antalek, B.2    Sorriero, L.3    Bijlsma, S.4    Louwerse, D.J.5    Smilde, A.6
  • 34
    • 0001174635 scopus 로고    scopus 로고
    • Diffusion-edited NMR - Affinity NMR for direct observation of molecular interactions
    • Lin M, Shapiro MJ, Wareing JR. Diffusion-edited NMR - Affinity NMR for direct observation of molecular interactions. J Am Chem Soc 1997; 119:5249-5250.
    • (1997) J Am Chem Soc , vol.119 , pp. 5249-5250
    • Lin, M.1    Shapiro, M.J.2    Wareing, J.R.3
  • 35
    • 0033214588 scopus 로고    scopus 로고
    • Affinity NMR - A new drug-screening tool that probes ligand-receptor interactions
    • Chen A, Shapiro MJ. Affinity NMR - A new drug-screening tool that probes ligand-receptor interactions. Anal Chem 1999; 71:669-675.
    • (1999) Anal Chem , vol.71 , pp. 669-675
    • Chen, A.1    Shapiro, M.J.2
  • 36
    • 0035819596 scopus 로고    scopus 로고
    • A novel NMR method for screening soluble compound libraries
    • Hodge P, Monvisade P, Morris GA, Preece I. A novel NMR method for screening soluble compound libraries. Chem Commun 2001; 3:239-240.
    • (2001) Chem Commun , vol.3 , pp. 239-240
    • Hodge, P.1    Monvisade, P.2    Morris, G.A.3    Preece, I.4
  • 37
    • 0001448626 scopus 로고    scopus 로고
    • Mixture analysis in combinatorial chemistry. Application of diffusion-resolved NMR spectroscopy
    • Lin M, Shapiro MJ. Mixture analysis in combinatorial chemistry. Application of diffusion-resolved NMR spectroscopy. J Org Chem 1996; 61:7617-7619.
    • (1996) J Org Chem , vol.61 , pp. 7617-7619
    • Lin, M.1    Shapiro, M.J.2
  • 38
    • 0001364796 scopus 로고    scopus 로고
    • Screening mixtures by affinity NMR
    • Lin M, Shapiro MJ, Wareing JR. Screening mixtures by affinity NMR. J Org Chem 1997; 62:8930-8931.
    • (1997) J Org Chem , vol.62 , pp. 8930-8931
    • Lin, M.1    Shapiro, M.J.2    Wareing, J.R.3
  • 40
    • 0033469788 scopus 로고    scopus 로고
    • Spatial coherence phenomena arising from translational spin motion in gradient spin echo experiments
    • Callaghan PT, Codd SL, Seymour JD. Spatial coherence phenomena arising from translational spin motion in gradient spin echo experiments. Concepts Magn Reson 1999; 11:181-202.
    • (1999) Concepts Magn Reson , vol.11 , pp. 181-202
    • Callaghan, P.T.1    Codd, S.L.2    Seymour, J.D.3
  • 41
    • 33749622370 scopus 로고
    • Spin echoes
    • Hahn EL. Spin echoes. Phys Rev 1950; 80:580-594.
    • (1950) Phys Rev , vol.80 , pp. 580-594
    • Hahn, E.L.1
  • 42
    • 33847534249 scopus 로고
    • Effects of diffusion on free precession in nuclear magnetic resonance experiments
    • Carr HY, Purcell EM. Effects of diffusion on free precession in nuclear magnetic resonance experiments. Phys Rev 1954; 94:630-638.
    • (1954) Phys Rev , vol.94 , pp. 630-638
    • Carr, H.Y.1    Purcell, E.M.2
  • 44
    • 0007804677 scopus 로고
    • NMR and the structure of D-glucose
    • Gurst JE. NMR and the structure of D-glucose. J Chem Ed 1991; 68:1003-1004.
    • (1991) J Chem Ed , vol.68 , pp. 1003-1004
    • Gurst, J.E.1
  • 45
    • 0001426032 scopus 로고
    • Analytical method for the compensation of eddy-current effects induced by pulsed magnetic field gradients in NMR systems
    • Jehenson P, Westphal M, Schuff N. Analytical method for the compensation of eddy-current effects induced by pulsed magnetic field gradients in NMR systems. J Magn Reson 1990; 90:264-278.
    • (1990) J Magn Reson , vol.90 , pp. 264-278
    • Jehenson, P.1    Westphal, M.2    Schuff, N.3
  • 46
    • 0003161755 scopus 로고
    • Effect of nonrectangular field gradient pulses in the Stejskal and Tanner (diffusion) pulse sequence
    • Price WS, Kuchel PW. Effect of nonrectangular field gradient pulses in the Stejskal and Tanner (diffusion) pulse sequence. J Magn Reson 1991; 94:133-139.
    • (1991) J Magn Reson , vol.94 , pp. 133-139
    • Price, W.S.1    Kuchel, P.W.2
  • 47
    • 43949164076 scopus 로고
    • NMR diffusion measurements using a composite gradient PGSE sequence
    • Merrill MR. NMR diffusion measurements using a composite gradient PGSE sequence. J Magn Reson Ser A 1993; 103:223-225.
    • (1993) J Magn Reson Ser A , vol.103 , pp. 223-225
    • Merrill, M.R.1
  • 48
    • 43949151247 scopus 로고
    • Self-compensating pulsed magnetic-field gradients for short recovery times
    • Wider G, Dötsch V, Wüthrich K. Self-compensating pulsed magnetic-field gradients for short recovery times. J Magn Reson Ser A 1994; 108:255-258.
    • (1994) J Magn Reson Ser A , vol.108 , pp. 255-258
    • Wider, G.1    Dötsch, V.2    Wüthrich, K.3
  • 49
    • 0032615708 scopus 로고    scopus 로고
    • Composite pulsed gradients with refocused chemical shifts and short recovery time
    • Haitao H, Shaka AJ. Composite pulsed gradients with refocused chemical shifts and short recovery time. J Magn Reson 1999; 136:54-62.
    • (1999) J Magn Reson , vol.136 , pp. 54-62
    • Haitao, H.1    Shaka, A.J.2
  • 50
    • 0032396789 scopus 로고    scopus 로고
    • Two-dimensional HSQC NMR spectra obtained using a self-compensating double pulsed field gradient and processed using the filter diagonalization method
    • Mandelshtam VA, Haitao H, Shaka AJ. Two-dimensional HSQC NMR spectra obtained using a self-compensating double pulsed field gradient and processed using the filter diagonalization method. Magn Reson Chem 1998; 36:S17-S28.
    • (1998) Magn Reson Chem , vol.36
    • Mandelshtam, V.A.1    Haitao, H.2    Shaka, A.J.3
  • 51
    • 0346677079 scopus 로고    scopus 로고
    • The influence of a nonconstant magnetic-field gradient on PFG NMR diffusion experiments. A Brownian-dynamics computer simulation study
    • Håkansson B, Jönsson B, Linse P, Söderman O. The influence of a nonconstant magnetic-field gradient on PFG NMR diffusion experiments. A Brownian-dynamics computer simulation study. J Magn Reson 1997; 124:343-351.
    • (1997) J Magn Reson , vol.124 , pp. 343-351
    • Håkansson, B.1    Jönsson, B.2    Linse, P.3    Söderman, O.4
  • 52
    • 0003052693 scopus 로고    scopus 로고
    • Shaped radiofrequency pulses in high resolution NMR
    • Freeman R. Shaped radiofrequency pulses in high resolution NMR. Prog Nucl Magn Reson Spectrosc 1998; 32:59-106.
    • (1998) Prog Nucl Magn Reson Spectrosc , vol.32 , pp. 59-106
    • Freeman, R.1
  • 53
    • 0001522444 scopus 로고
    • The impact of Rayleigh-Benard convection on NMR pulsed-field-gradient diffusion measurements
    • Goux WJ, Verkruyse LA, Salter SJ. The impact of Rayleigh-Benard convection on NMR pulsed-field-gradient diffusion measurements. J Magn Reson 1990; 88:609-614.
    • (1990) J Magn Reson , vol.88 , pp. 609-614
    • Goux, W.J.1    Verkruyse, L.A.2    Salter, S.J.3
  • 54
    • 0035743083 scopus 로고    scopus 로고
    • Diffusion-broadened velocity spectra of convection in variable-temperature BP-LED experiments
    • Mau X-A, Kohlmann O. Diffusion-broadened velocity spectra of convection in variable-temperature BP-LED experiments. J Magn Reson 2001; 150:35-38.
    • (2001) J Magn Reson , vol.150 , pp. 35-38
    • Mau, X.-A.1    Kohlmann, O.2
  • 57
    • 0000293290 scopus 로고
    • Velocity and diffusion imaging in dynamic NMR microscopy
    • Callaghan PT, Xia Y. Velocity and diffusion imaging in dynamic NMR microscopy. J Magn Reson 1991; 91:326-352.
    • (1991) J Magn Reson , vol.91 , pp. 326-352
    • Callaghan, P.T.1    Xia, Y.2
  • 58
    • 0000664854 scopus 로고    scopus 로고
    • Electrophoretic NMR
    • Grand DM, Harris RK, editors. New York: Wiley
    • Johnson CS Jr. Electrophoretic NMR. In: Grand DM, Harris RK, editors. Encyclopedia of NMR; New York: Wiley; 1996. Vol. 2. p 1886-1895.
    • (1996) Encyclopedia of NMR , vol.2 , pp. 1886-1895
    • Johnson Jr., C.S.1
  • 59
    • 0000468681 scopus 로고    scopus 로고
    • Thermal convection currents in NMR: Flow profiles and implications for coherence pathway selection
    • Jerschow A. Thermal convection currents in NMR: Flow profiles and implications for coherence pathway selection. J Magn Reson 2000; 145:121-131.
    • (2000) J Magn Reson , vol.145 , pp. 121-131
    • Jerschow, A.1
  • 60
    • 0033170437 scopus 로고    scopus 로고
    • Measurement of convection and temperature profiles in liquid samples
    • Loening NM, Keeler J. Measurement of convection and temperature profiles in liquid samples. J Magn Reson 1999; 139:334-341.
    • (1999) J Magn Reson , vol.139 , pp. 334-341
    • Loening, N.M.1    Keeler, J.2
  • 62
    • 0000871046 scopus 로고    scopus 로고
    • 1H NMR and suppression of convection in NMR probes
    • 1H NMR and suppression of convection in NMR probes. J Magn Reson 1998; 131:126-130.
    • (1998) J Magn Reson , vol.131 , pp. 126-130
    • Hedin, N.1    Furó, I.2
  • 64
    • 0002077129 scopus 로고    scopus 로고
    • Effects of thermal convection on NMR and their elimination by sample rotation
    • Lounila J, Oikarinen K, Ingman P, Jokisaari J. Effects of thermal convection on NMR and their elimination by sample rotation. J Magn Reson Ser A 1996; 118:50-54.
    • (1996) J Magn Reson Ser A , vol.118 , pp. 50-54
    • Lounila, J.1    Oikarinen, K.2    Ingman, P.3    Jokisaari, J.4
  • 65
    • 0032708818 scopus 로고    scopus 로고
    • Investigation of the diffusion measurement using PFG and test of robustness against experimental conditions and parameters
    • Augé S, Amblard-Blondel B, Delsuc M-A. Investigation of the diffusion measurement using PFG and test of robustness against experimental conditions and parameters. J Chim Phys 1999; 96:1559-1565.
    • (1999) J Chim Phys , vol.96 , pp. 1559-1565
    • Augé, S.1    Amblard-Blondel, B.2    Delsuc, M.-A.3
  • 66
    • 0001467456 scopus 로고
    • Asymmetric modes and the transition to vortex structures in rotating Rayleigh-Bénard convection
    • Zhong F, Ecke R, Steinberg V. Asymmetric modes and the transition to vortex structures in rotating Rayleigh-Bénard convection. Phys Rev Lett 1991; 67:2473-2476.
    • (1991) Phys Rev Lett , vol.67 , pp. 2473-2476
    • Zhong, F.1    Ecke, R.2    Steinberg, V.3
  • 67
    • 0001522444 scopus 로고
    • The impact of Rayleigh-Bernard convection on NMR pulsed-field-gradient diffusion measurements
    • Goux WJ, Verkruyse LA, Salter SJ. The impact of Rayleigh-Bernard convection on NMR pulsed-field-gradient diffusion measurements. J Magn Reson 1990; 88:609-614.
    • (1990) J Magn Reson , vol.88 , pp. 609-614
    • Goux, W.J.1    Verkruyse, L.A.2    Salter, S.J.3
  • 68
    • 0001424822 scopus 로고    scopus 로고
    • Suppression of convection artifacts in stimulated-echo diffusion experiments. Double-stimulated-echo experiments
    • Jerschow A, Müller N. Suppression of convection artifacts in stimulated-echo diffusion experiments. Double-stimulated-echo experiments. J Magn Reson 1997; 125:372-375.
    • (1997) J Magn Reson , vol.125 , pp. 372-375
    • Jerschow, A.1    Müller, N.2
  • 69
    • 0002258765 scopus 로고    scopus 로고
    • Convection compensation in gradient enhanced nuclear magnetic resonance spectroscopy
    • Jerschow A, Müller N. Convection compensation in gradient enhanced nuclear magnetic resonance spectroscopy. J Magn Reson 1998; 132:13-18.
    • (1998) J Magn Reson , vol.132 , pp. 13-18
    • Jerschow, A.1    Müller, N.2
  • 70
    • 0000466944 scopus 로고    scopus 로고
    • Improved convection compensating pulsed field gradient spin-echo and stimulated echo methods
    • Sørland GH, Seland JG, Krane J, Anthonsen HK. Improved convection compensating pulsed field gradient spin-echo and stimulated echo methods. J Magn Reson 2000; 142:323-325.
    • (2000) J Magn Reson , vol.142 , pp. 323-325
    • Sørland, G.H.1    Seland, J.G.2    Krane, J.3    Anthonsen, H.K.4
  • 71
    • 58149362694 scopus 로고
    • An improved diffusion-ordered spectroscopy experiment incorporating bipolar gradient pulses
    • Wu D, Chen A, Johnson CS Jr. An improved diffusion-ordered spectroscopy experiment incorporating bipolar gradient pulses. J Magn Reson Ser A 1995; 115:260-264.
    • (1995) J Magn Reson Ser A , vol.115 , pp. 260-264
    • Wu, D.1    Chen, A.2    Johnson Jr., C.S.3
  • 72
    • 0032134648 scopus 로고    scopus 로고
    • Practical aspects of the measurement of the diffusion of proteins in aqueous solution
    • Tillet ML, Lu-Yun L, Norwood TJ. Practical aspects of the measurement of the diffusion of proteins in aqueous solution. J Magn Reson 1998; 133:379-384.
    • (1998) J Magn Reson , vol.133 , pp. 379-384
    • Tillet, M.L.1    Lu-Yun, L.2    Norwood, T.J.3
  • 73
  • 74
    • 0028857598 scopus 로고
    • Association of biomolecular systems via pulsed field gradient NMR self-diffusion measurements
    • Altieri AS, Hinton DP, Byrd RA. Association of biomolecular systems via pulsed field gradient NMR self-diffusion measurements. J Am Chem Soc 1995; 117:7566-7567.
    • (1995) J Am Chem Soc , vol.117 , pp. 7566-7567
    • Altieri, A.S.1    Hinton, D.P.2    Byrd, R.A.3
  • 75
    • 0033170441 scopus 로고    scopus 로고
    • Strategies for diagnosing and alleviating artifactual attenuation associated with large gradient pulses in PGSE NMR diffusion measurements
    • Price WS, Hayamizu K, Ide H, Arata Y. Strategies for diagnosing and alleviating artifactual attenuation associated with large gradient pulses in PGSE NMR diffusion measurements. J Magn Reson 1999; 139:205-212.
    • (1999) J Magn Reson , vol.139 , pp. 205-212
    • Price, W.S.1    Hayamizu, K.2    Ide, H.3    Arata, Y.4
  • 76
    • 0000082309 scopus 로고    scopus 로고
    • Cross-relaxation in pulsed-field-gradient stimulated-echo measurements on water in a macromolecular matrix
    • Pescher LJC, Bouwstra JA, de Bleyser J, Junginger HE, Leyte JC. Cross-relaxation in pulsed-field-gradient stimulated-echo measurements on water in a macromolecular matrix. J Magn Reson Ser B 1996; 110:150-157.
    • (1996) J Magn Reson Ser B , vol.110 , pp. 150-157
    • Pescher, L.J.C.1    Bouwstra, J.A.2    De Bleyser, J.3    Junginger, H.E.4    Leyte, J.C.5
  • 77
    • 0033538276 scopus 로고    scopus 로고
    • Nuclear Overhauser effect on diffusion measurements
    • Chen A, Shapiro MJ. Nuclear Overhauser effect on diffusion measurements. J Am Chem Soc 1999; 121:5338-5339.
    • (1999) J Am Chem Soc , vol.121 , pp. 5338-5339
    • Chen, A.1    Shapiro, M.J.2
  • 79
    • 33947473108 scopus 로고
    • The mutual diffusion of light and heavy water
    • Longsworth LG. The mutual diffusion of light and heavy water. J Phys Chem 1960; 64:1914-1917.
    • (1960) J Phys Chem , vol.64 , pp. 1914-1917
    • Longsworth, L.G.1
  • 81
    • 0000552707 scopus 로고
    • Diffusion and scaling behavior of polymer-surfactant aggregates
    • Chari K, Antalek B, Minter J. Diffusion and scaling behavior of polymer-surfactant aggregates. Phys Rev Lett 1995; 74:3624-3627.
    • (1995) Phys Rev Lett , vol.74 , pp. 3624-3627
    • Chari, K.1    Antalek, B.2    Minter, J.3
  • 82
    • 0010322441 scopus 로고
    • Influence of multiple length scales on the behavior of polymer self-diffusion in the semidilute regime
    • Callaghan PT, Pinder DN. Influence of multiple length scales on the behavior of polymer self-diffusion in the semidilute regime. Macromolecules 1984; 17:431-437.
    • (1984) Macromolecules , vol.17 , pp. 431-437
    • Callaghan, P.T.1    Pinder, D.N.2
  • 83
    • 0001300409 scopus 로고
    • Role of hydrogen-bond cooperativity and free-volume fluctuations in the non-Arrhenius behavior of water self-diffusion: A continuity-of-states model
    • Lamanna R, Delmelle M, Cannistraro S. Role of hydrogen-bond cooperativity and free-volume fluctuations in the non-Arrhenius behavior of water self-diffusion: A continuity-of-states model. Phys Rev E 1994; 49:2841-2850.
    • (1994) Phys Rev E , vol.49 , pp. 2841-2850
    • Lamanna, R.1    Delmelle, M.2    Cannistraro, S.3
  • 84
    • 0042936805 scopus 로고
    • Self-diffusion in normal and heavy water in the range 1-45 degrees
    • Mills R. Self-diffusion in normal and heavy water in the range 1-45 degrees. J Phys Chem 1973; 77:685-688.
    • (1973) J Phys Chem , vol.77 , pp. 685-688
    • Mills, R.1
  • 85
    • 0029289354 scopus 로고
    • Diffusion in aqueous solutions of poly(ethylene glycol) at low concentrations
    • Waggoner RA, Blum FD, Lang JC. Diffusion in aqueous solutions of poly(ethylene glycol) at low concentrations. Macromolecules 1995; 28:2658-2664.
    • (1995) Macromolecules , vol.28 , pp. 2658-2664
    • Waggoner, R.A.1    Blum, F.D.2    Lang, J.C.3
  • 86
    • 0035744178 scopus 로고    scopus 로고
    • Accurate measurement of translational diffusion coefficients: A practical method to account for nonlinear gradients
    • Damberg P, Jarvet J, Gräslund A. Accurate measurement of translational diffusion coefficients: A practical method to account for nonlinear gradients. J Magn Reson 2001; 148:343-348.
    • (2001) J Magn Reson , vol.148 , pp. 343-348
    • Damberg, P.1    Jarvet, J.2    Gräslund, A.3
  • 87
    • 0001531472 scopus 로고    scopus 로고
    • Exponential analysis in physical phenomena
    • Istratov AA, Vyvenko OF. Exponential analysis in physical phenomena. Rev Sci Instrum 1999; 70:1233-1257.
    • (1999) Rev Sci Instrum , vol.70 , pp. 1233-1257
    • Istratov, A.A.1    Vyvenko, O.F.2
  • 88
    • 36749107621 scopus 로고
    • An eigenfunction expansion method for the analysis of exponential decay curves
    • Provencher SW. An eigenfunction expansion method for the analysis of exponential decay curves. J Chem Phys 1976; 64:2772-2777.
    • (1976) J Chem Phys , vol.64 , pp. 2772-2777
    • Provencher, S.W.1
  • 89
    • 0020330142 scopus 로고
    • Double beam fluorescence spectrometer with subnanosecond resolution: Application to aqueous tryptophan
    • Wijnaendts van Resandt RW, Vogel RH, Provencher SW. Double beam fluorescence spectrometer with subnanosecond resolution: Application to aqueous tryptophan. Rev Sci Instrum 1982; 53:1392-1397.
    • (1982) Rev Sci Instrum , vol.53 , pp. 1392-1397
    • Wijnaendts Van Resandt, R.W.1    Vogel, R.H.2    Provencher, S.W.3
  • 90
    • 0020176708 scopus 로고
    • CONTIN: A general purpose constrained regularization program for inverting noisy linear algebraic and integral equations
    • Provencher SW. CONTIN: A general purpose constrained regularization program for inverting noisy linear algebraic and integral equations. Comput Phys Commun 1982; 27:229-242.
    • (1982) Comput Phys Commun , vol.27 , pp. 229-242
    • Provencher, S.W.1
  • 91
    • 0001409990 scopus 로고    scopus 로고
    • Maximum entropy processing of DOSY NMR spectra
    • Delsuc MA, Malliavin, TE. Maximum entropy processing of DOSY NMR spectra. Anal Chem 1998; 70:2146-2148.
    • (1998) Anal Chem , vol.70 , pp. 2146-2148
    • Delsuc, M.A.1    Malliavin, T.E.2
  • 93
    • 0025186604 scopus 로고
    • A new method for the analysis of correlated data using Procrustes rotation which is suitable for spectral analysis
    • Kubista M. A new method for the analysis of correlated data using Procrustes rotation which is suitable for spectral analysis. Chemom Intell Lab Syst 1990; 7:273-279.
    • (1990) Chemom Intell Lab Syst , vol.7 , pp. 273-279
    • Kubista, M.1
  • 94
    • 0001635164 scopus 로고
    • Analysis of correlated spectral data
    • Scarminio I, Kubista M. Analysis of correlated spectral data. Anal Chem 1993; 65:409-416.
    • (1993) Anal Chem , vol.65 , pp. 409-416
    • Scarminio, I.1    Kubista, M.2
  • 95
    • 84984336824 scopus 로고
    • Comments on data analysis (datan) algorithm and rank annihilation factor analysis for the analysis of correlated spectral data
    • Booksh KS, Kowalski BR. Comments on data analysis (datan) algorithm and rank annihilation factor analysis for the analysis of correlated spectral data. J Chemom 1994; 8:287-292.
    • (1994) J Chemom , vol.8 , pp. 287-292
    • Booksh, K.S.1    Kowalski, B.R.2
  • 96
    • 26444570774 scopus 로고
    • Generalized rank annihilation factor analysis
    • Sanchez E, Kowalski BR. Generalized rank annihilation factor analysis. Anal Chem 1986; 58:496-499.
    • (1986) Anal Chem , vol.58 , pp. 496-499
    • Sanchez, E.1    Kowalski, B.R.2
  • 97
    • 0000904076 scopus 로고
    • An improved algorithm for the generalized rank annihilation method
    • Wilson BE, Sanchez E, Kowalski BR. An improved algorithm for the generalized rank annihilation method. J Chemom 1989; 3:493-498.
    • (1989) J Chemom , vol.3 , pp. 493-498
    • Wilson, B.E.1    Sanchez, E.2    Kowalski, B.R.3
  • 98
    • 43949173362 scopus 로고
    • Analysis of multicomponent FT-PGSE experiments by multivariate statistical methods applied to the complete bandshapes
    • Schulze D, Stilbs P. Analysis of multicomponent FT-PGSE experiments by multivariate statistical methods applied to the complete bandshapes. J Magn Reson Ser A 1993; 105:54-58.
    • (1993) J Magn Reson Ser A , vol.105 , pp. 54-58
    • Schulze, D.1    Stilbs, P.2
  • 99
    • 0001494550 scopus 로고    scopus 로고
    • Multivariate image analysis of magnetic resonance images with the direct exponential curve resolution algorithm (DECRA). Part 1: Algorithm and model study
    • Windig W, Hornak JP, Antalek B. Multivariate image analysis of magnetic resonance images with the direct exponential curve resolution algorithm (DECRA). Part 1: Algorithm and model study. J Magn Reson 1998; 132:298-306.
    • (1998) J Magn Reson , vol.132 , pp. 298-306
    • Windig, W.1    Hornak, J.P.2    Antalek, B.3
  • 100
    • 0032087380 scopus 로고    scopus 로고
    • Multivariate image analysis of magnetic resonance images with the direct exponential curve resolution algorithm (DECRA). Part 2: Application to human brain images
    • Antalek B, Hornak JP, Windig W. Multivariate image analysis of magnetic resonance images with the direct exponential curve resolution algorithm (DECRA). Part 2: Application to human brain images. J Magn Reson 1998; 132:307-315.
    • (1998) J Magn Reson , vol.132 , pp. 307-315
    • Antalek, B.1    Hornak, J.P.2    Windig, W.3
  • 101
    • 0033652458 scopus 로고    scopus 로고
    • Applications of the direct exponential curve resolution algorithm (DECRA) to solid state nuclear magnetic resonance and mid-infrared spectra
    • Windig W, Antalek B, Robbins MJ, Zumbulyadis N, Heckler CE. Applications of the direct exponential curve resolution algorithm (DECRA) to solid state nuclear magnetic resonance and mid-infrared spectra. J Chemom 2000; 14:213-227.
    • (2000) J Chemom , vol.14 , pp. 213-227
    • Windig, W.1    Antalek, B.2    Robbins, M.J.3    Zumbulyadis, N.4    Heckler, C.E.5
  • 103
    • 0032209514 scopus 로고    scopus 로고
    • Component separation in NMR imaging and multidimensional spectroscopy through global least-squares analysis, based on prior knowledge
    • Stilbs P. Component separation in NMR imaging and multidimensional spectroscopy through global least-squares analysis, based on prior knowledge. J Magn Reson 1998; 241:236-241.
    • (1998) J Magn Reson , vol.241 , pp. 236-241
    • Stilbs, P.1
  • 104
    • 0027292957 scopus 로고
    • Multivariate curve resolution applied to liquid chromatography-diode array detection
    • Tauler R, Barcelo D. Multivariate curve resolution applied to liquid chromatography-diode array detection. Trends Anal Chem 1993; 12:319-327.
    • (1993) Trends Anal Chem , vol.12 , pp. 319-327
    • Tauler, R.1    Barcelo, D.2


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.