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Determined by the relative integrals of the signals due to deuterium in the vinylic (13b) and allylic (13c) positions (δ 5 6.00 and 2.59 ppm, respectively).
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Determined by the relative integrals of the signals due to deuterium in the vinylic (13b) and allylic (13c) positions (δ 5 6.00 and 2.59 ppm, respectively).
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15
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Significant migration of the double bond was observed in the absence of anisole
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Doubling of signals due to the three methyl groups was observed with a racemic sample
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Doubling of signals due to the three methyl groups was observed with a racemic sample.
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