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Volumn 111, Issue 35, 2007, Pages 10386-10396

Synthesis and photophysical properties of nonbenzoid ended fluorophores

Author keywords

[No Author keywords available]

Indexed keywords

ENERGY GAP; EXCITED STATES; GROUND STATE; MOLECULAR STRUCTURE; PHOTOLUMINESCENCE; SYNTHESIS (CHEMICAL);

EID: 34548829650     PISSN: 15206106     EISSN: None     Source Type: Journal    
DOI: 10.1021/jp073767n     Document Type: Article
Times cited : (12)

References (42)
  • 6
    • 0041586517 scopus 로고
    • Cambridge University Press: Cambridge, UK
    • Rost, F. W. D. Fluorescence Microscopy; Cambridge University Press: Cambridge, UK, 1992; Vol. 1, p 28.
    • (1992) Fluorescence Microscopy , vol.1 , pp. 28
    • Rost, F.W.D.1
  • 32
    • 84906413952 scopus 로고    scopus 로고
    • X-ray measurements of 11 and 17 were carried out on CCD area detector diffractometer by using graphite-monochromated Mo Kα radiation (λ, 0.71073 Å) at 293 K. Crystal parameters of 11: C40H30, MW 510.64, monoclinic, space group P2(1)/c, a, 9.282(12) Å, b, 14.607(19) Å c, 10.4436(14) Å, α, 90°, ß, 92.662(3)°, γ, 90°, V, 1414.4(3) A°3, Z, 2, Dc, 1.199 mg/cm3, crystal size 0.476 mm × 0.287 mm × 0.150 mm, μ, 0.068 mm-1, 8226 reflections were collected giving 3068 independent reflections from which 1525 with I > 2σ(I) were available for calculation. wR2, 0.0891(all data, GOF, 0.797. Crystal parameters of 17: C65H50, MW 831.05, triclinic, space group P1, a, 9.053(1) A°, b, 16.397(2, c, 16.8932
    • -1, 12978 reflections were collected giving 9077 independent reflections from which 3377 with I > 2σ(I) were available for calculation. The structure was solved and refined with the SHELX 97 package. The hydrogen atoms were placed in calculated positions at a bond distance of 0.93 Å to aryl C and 0.97 Å to alkyl C. Finally, refinements of the structure (579 variables) led to R = 0.0870, wR2 = 0.290, GOF = 0.88.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.