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The diene 4 employed for our reactions was prepared according to ref. 3a GC-MS analysis of the reaction mixture at different reaction times revealed the presence of a second product with molecular mass corresponding to that of 7a with an hydrogen atom substituted by a trimethylsilyl group. This compound, subsequently identified as 2-methyl-3-trimethylsilyl-5-phenyl furan 6a, was not isolated as it was converted into 7a during work-up and chromatographic purification on silica gel column (see below and ESI)
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