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3/Ag(fod) complex. See the Supporting Information for complete details. (Chemical Equation Presented)
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For an analysis of the barrier to rotation in metal-alkene complexes
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For examples of in-plane alkene coordination to d8 complexes, see: (a) Musco, A, Pontellini, R, Grassi, A, Meille, S. V, Rüegger, H, Ammann, C, Pregosin, P. S. Organometallics 1988, 7, 2130
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8 complexes, see: (a) Musco, A.; Pontellini, R.; Grassi, A.; Meille, S. V.; Rüegger, H.; Ammann, C.; Pregosin, P. S. Organometallics 1988, 7, 2130.
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Cui, Q.; Musaev, D. G.; Morokuma, K. Organometallics 1997, 16, 1355.
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Cui, Q.1
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Sakaki, S.; Satoh, H.; Shono, H.; Ujino, Y. Organometallics 1996, 15, 1713.
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34848902904
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Direct interconversion of 13 and 15 by rotation about the metal-allyl axis is generally discounted, see: Pfaltz, A.; Lautens, M. In Comprehensive Asymmetric Catalysis; Jacobsen, E. N., Pfaltz, A., Yamamoto, H., Eds.; Springer-Verlag, Berlin, 1999; 2, pp 838-839. Consistent with this, we have computed barriers of 19.4 and 29.4 kcal/mol, depending upon the direction of rotation.
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Direct interconversion of 13 and 15 by rotation about the metal-allyl axis is generally discounted, see: Pfaltz, A.; Lautens, M. In Comprehensive Asymmetric Catalysis; Jacobsen, E. N., Pfaltz, A., Yamamoto, H., Eds.; Springer-Verlag, Berlin, 1999; Vol. 2, pp 838-839. Consistent with this, we have computed barriers of 19.4 and 29.4 kcal/mol, depending upon the direction of rotation.
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91
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0001220639
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Hannson, S. H.; Norrby, P.-O.; Sjogren, M. P. T.; Åkermark, B.; Cucciolito, M. E.; Giordano, F.; Vitagliano, A. Organometallics 1993, 12, 4940.
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Hannson, S.H.1
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Giordano, F.6
Vitagliano, A.7
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