Matrix-comprehensive in-house validation and robustness check of a confirmatory method for the determination of four nitrofuran metabolites in poultry muscle and shrimp by LC-MS/MS

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 856, Issue 1-2, 2007, Pages 178-189

  Bock, Claudia ^a   Gowik, Petra ^a   Stachel, Carolin ^a  

^a Federal Office of Consumer Protection and Food Safety   (Germany)

Author keywords

LC MS MS; Matrix comprehensive in house validation; Measurement uncertainty; Metabolite; Muscle; Nitrofurans; Poultry; Residues; Robustness; Shrimps; Validation

Indexed keywords

MATRIX-COMPREHENSIVE IN-HOUSE VALIDATION; MEASUREMENT UNCERTAINTY; NITROFURANS; POULTRY;

DERIVATIVES; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; MUSCLE;

METABOLITES;

1 AMINOHYDANTOIN; 3 AMINO 2 OXAZOLIDINONE; 3 AMINO 5 METHYL MORPHOLINO 2 OXAZOLIDINONE; NITROFURAN DERIVATIVE; SEMICARBAZIDE; UNCLASSIFIED DRUG;

ANIMAL TISSUE; ARTICLE; CONTROLLED STUDY; LIQUID CHROMATOGRAPHY; MUSCLE; NONHUMAN; POULTRY; PRIORITY JOURNAL; SHRIMP; TANDEM MASS SPECTROMETRY;

ANIMALS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CRUSTACEA; MUSCLES; NITROFURANS; POULTRY; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; TANDEM MASS SPECTROMETRY; UNCERTAINTY;

DECAPODA (CRUSTACEA);

EID: 34548132379     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2007.05.044     Document Type: Article

References (24)

1. Commission Decision (EC) 2003/181/EC, Off. J. Eur. Comm., No. L71 (2003) 17.
2. Commission Decision (EC) 2002/657/EC, Off. J. Eur. Comm., No. L221 (2002) 8.
3. McCracken R.J., and Kennedy D.G. J. Chromatogr. B 691 (1997) 87
4. McCracken R.J., Blanchflower W., Rowan C., McCoy M., and Kennedy D.G. Analyst 120 (1995) 2347
5. Nouws J.F., and Laurensen J. Vet. Quart. 12 1 (1990) 56
6. Cooper K.M., Mulder P.P.J., van Rhijn J.A., Kovacsics L., McCracken R.J., Young P.B., and Kennedy D.G. Food Addit. Contam. 22 5 (2005) 406
7. Hoogenboom L., van Kammen M., Berghmans M., Koeman J., and Kuiper H. Food Chem. Toxicol. 29 5 (1991) 321
8. J.A. van Rhijn, P.P.J. Mulder, RIKILT (State Institute of Quality Control of Agricultural Products), Muscle of poultry, rabbit and aquaculture products - detection, identification and quantification of furazolidone, furaltadone, nitrofurantoin and nitrofurazone - LC-MS/MS confirmatory analysis, Meeting of the National Experts on 11 April 2002, Brussels.
9. Horne E., Cadogan A., O'Keeffe M., and Hoogenboom L.A.P. Analyst 121 (1996) 1463
10. McCracken R.J., and Kennedy D.G. Food Addit. Contam. 14 (1997) 507
11. Wüst B., Sauber C., and van Rhijn H. Quantitation of nitrofuran metabolites in shrimp and poultry by LC/MS/MS using Agilent LC/MSD Trap XCT, Agilent Application. Food (2004)
12. Jülicher B., Gowik P., and Uhlig S. Analyst 124 (1999) 537
13. Uhlig S., Gowik P., and Radeck W. Anal. Chim. Acta. 483 (2003) 351
14. Mottier P., Khong S.-P., Gremaud E., Richoz J., Delatour T., Goldmann T., and Guy P. J. Chromatogr. A 1067 (2005) 85
15. Deutsches Institut für Normung, DIN 55350, Teil 34, Beuth Verlag, Berlin (1991).
16. Deutsches Institut für Normung, DIN 32645, Beuth Verlag, Berlin (1994).
17. ISO/DIS 11843-1, International Standards Organisation, Geneva (1995).
18. Finzi J., Donato J., Sucupira M., and De Nucci G. J. Chromatogr. B 824 (2005) 30
19. Edder P., Vargas S., Ortelli D., and Corvi C. Clin. Chem. Lab. Med. 41 (2003) 1608
20. Leitner A., Zöllner P., and Lindner W. J. Chromatogr. A 939 (2001) 49
21. Uhlig (2006): Personal communications.
22. Jülicher B., Gowik P., and Uhlig S. Analyst 123 (1998) 173
23. Analytical Method Committee, Analyst 120 (1995) 2303.
24. EURACHEM, EURACHEM/CITAC Guide, 2nd edn. (2000), ISBN 0 948926 15 5.