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16
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20944433734
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Andreu R., Blesa M.J., Carrasquer L., Garín J., Orduna J., Villacampa B., Alcalá R., Casado J., Ruiz-Delgado M.C., López-Navarrete J.T., and Allain M. J. Am. Chem. Soc. 127 (2005) 8835-8845
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18
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19
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34547791729
-
-
note
-
General procedure for 2a,b: To a stirred solution of the corresponding aldehyde 3a,b (0.51 mmol) and 2-amino-1,1,3-tricyanopropene (1) (0.76 mmol) in 10 mL of absolute ethanol was added one drop of piperidine/ethanol (1:1). The mixture was refluxed under argon with exclusion of light for 2.5-5 h (TLC monitoring). After cooling, the resulting solid was isolated by filtration, washed with cold ethanol and pentane and dried. Compound 2a: Purple solid (80 mg; 55%). Compound 2b: Violet solid (80 mg; 51%).
-
-
-
-
20
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-
34547820703
-
-
note
-
2, 313.0576; found, 313.0573.
-
-
-
-
21
-
-
34547753427
-
-
note
-
2/AcOEt (1:1). 65 mg (67%) of a purple solid was obtained, and identified as compound 2a.
-
-
-
-
22
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-
34250727116
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-
Andreu R., Carrasquer L., Cerdán M.A., Fernández A., Franco S., Garín J., and Orduna J. Synlett (2007) 1470-1472
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Andreu, R.1
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Franco, S.5
Garín, J.6
Orduna, J.7
-
23
-
-
34547809849
-
-
note
-
2, 339.0732; found, 339.0716.
-
-
-
-
24
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18544362812
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Metzger J., Larivé H., Dennilauler R., Baralle R., and Gaurat C. Bull. Soc. Chim. Fr. (1969) 1284-1293
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Metzger, J.1
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28
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0000882822
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Marder S.R., Perry J.W., Tiemann B.G., Gorman C.B., Gilmour S., Biddle S.L., and Bourhill G. J. Am. Chem. Soc. 115 (1993) 2524-2526
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Biddle, S.L.6
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29
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0000963221
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0030746209
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32
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0000627409
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Tarbit, B.12
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33
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0000730969
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Nguyen T.T., Sallé M., Delaunay J., Riou A., Richomme P., Raimundo J.M., Gorgues A., Ledoux I., Dhenaut C., Zyss J., Orduna J., and Garín J. J. Mater. Chem. 8 (1998) 1185-1192
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37
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0033430879
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Robinson B.H., Dalton L.R., Harper A.W., Ren A., Wang F., Zhang C., Todorova G., Lee M., Aniszfeld R., Garner S., Chen A., Steier W.H., Houbrecht S., Persoons A., Ledoux I., Zyss J., and Jen A.K.Y. Chem. Phys. 245 (1999) 35-50
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Persoons, A.14
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Zyss, J.16
Jen, A.K.Y.17
-
38
-
-
34547752329
-
-
note
-
2, 385.0787; found, 385.0780.
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-
-
|