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27844518638
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note
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ij for S, O and C atoms, x, y, z, and U fixed for H atoms). 172 variables for 1153 observations, with the resulting R = 0.073, Rw=0.078. All the calculations were performed using the XTAL 3.2 package.
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0027271335
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27844442509
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-1/2 with the resulting R = 0.048, Rw=0.062. All the calculations were performed using the MOLEN package. Full Crystallographic details, excluding structure factors, have been deposited at the Cambridge Crystallographic Data Centre (CCDC). See Information for Authors, J. Mater. Chem., 1998, Issue 1. Any request to the CCDC for this material should quote the full literature citation and the reference number 1145/91.
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