A study of piperidinium structure-directing agents in the synthesis of silica molecular sieves under fluoride-based conditions

Journal of the American Chemical Society

Volumn 129, Issue 29, 2007, Pages 9066-9079

  Zones, Stacey I ^a   Burton, Allen W ^a   Lee, Greg S ^a,c   Olmstead, Marilyn M ^b  

^a CHEVRON ENERGY TECHNOLOGY COMPANY   (United States)

^b UNIVERSITY OF CALIFORNIA   (United States)

^c LAWRENCE LIVERMORE NATIONAL LABORATORY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CARBON; FLUORIDE MINERALS; MOLECULAR STRUCTURE; NITROGEN COMPOUNDS; SELF ASSEMBLY; SILICA;

FLUORIDE-BASED CONDITIONS; ORGANOCATIONS; PIPERIDINIUM; SILICA MOLECULAR SIEVES;

MOLECULAR DYNAMICS;

CARBON; FLUORIDE; NITROGEN; PIPERIDINE DERIVATIVE; SILICON DIOXIDE; ZEOLITE;

ARTICLE; CONFORMATION; MOLECULAR MODEL; STRUCTURE ANALYSIS; SYNTHESIS;

EID: 34547470093     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja0709122     Document Type: Article

References (51)

1. Lee, G. S.; Nakagawa, Y.; Hwang, S-J.; Davis, M. E.; Wagner, P.; Beck, L.; Zones, S. I. J. Am. Chem. Soc. 2002, 124, 7024-34.
2. Wagner, P.; Nakagawa, Y.; Lee, G. S.; Davis, M. E.; Elomari, S.; Medrud, R. C.; Zones, S. I. J. Am. Chem. Soc. 2000, 122, 263-273.
3. Zones, S. I.; Nakagawa, Y.; Yuen, L-T.; Harris, T. V. J. Am. Chem. Soc. 1996, 118, 7558-7567.
4. Wans, Z. B.; Yan, Y. Adv. Mater. 2001, 13, 1463.
5. Barrer, R. M. Zeolites and Clay Minerals as Sorbents and Molecular Sieves; Academic: New York, 1978.
6. Flanigen E. M.; Patton R. L. U.S. Patent 4 073 865, 1978.
7. Guth, J.-L.; Kessler, H.; Caullet, P.; Hazm, J.; Merrouche, A. Proc. Int. Zeolite Conf. 1993, 9, 215.
8. Camblor, M. A.; Villaescusa, L. A.; Diaz-Cabana M. J. Top. Catal. 1999, 9, 59.
9. Zones, S. I.; Hwang, S-J.; Elomari, S.; Ogino, I.; Davis, M. E.; Burton, A. W. Compt. Rend. Chim. 2005, 8, 267-282.
10. Zones, S. I.; van Nordstrand. R. A. Zeolites 1988, 8, 166.
11. Zones, S. I.; Darton, R. J.; Morris, R. E.; Hwang S-J. J. Phys Chem. B 2005, 109 652
12. Zones, S. I.; Olmstead, M. M.; Samilli, D. S. J. Am. Chem. Soc. 1992, 114, 4195.
13. Burton, A. W.; Lee, G. S.; Zones, S. I. Microporous Mesoporous Mater. 2006, 90 (1-3), 129-144.
14. Software is the Cerius2 V.2.1 product of BioSym and MSI Corp.
15. Burchart, E. d. v. Studies on Zeolites: molecular mechanics, framework stability and crystal growth. Ph.D. Thesis, 1992.
16. Rappe, A. K.; Casewit, C. J.; Colwell, K. S.; Goddard, W. A., III. J. Am. Chem. Soc. 1992, 114, 10024.
17. Lewis, D. W.; Freeman, C. M.; Catlow, C. R. A. J. Phys Chem. 1995, 99, 11194-11202.
18. Pulido, A.; Corma, A.; Sastre, G. J. Phys. Chem. B 2006; ASAP article.
19. Sastre, G.; Leiva, S.; Sabater, M. J.; Gimenez, I.; Rey, F.; Valencia, S.; Corma, A. J. Phys. Chem. B 2003, 107, 5432-5440.
20. Sastre, G. Personal communication.
21. Arranz, M.; Perez-Pariente, J.; Wright, P. A.; Slawin, A. M. Z.; Blasco, T.; Gomez-Hortiguela, L.; Cora, F. Chem. Mater. 2005, 17 (17), 4374-4385.
22. Corma, A. Proc. Int. Zeolite Conf. 2004, 14, 1.
23. Nakagawa, Y.; Lee, G. S.; Harris, T. V.; Yuen, L-T.; Zones, S. I. Microporous Mesoporous Mater. 1998, 22, 69-85.
24. Gies, H.; Marler, B. Zeolites 1992, 12, 42-49.
25. Zones, S. I. Microporous Mater. 1992, 2, 281-287.
26. Zones, S. I.; Nakagawa, Y.; Lee, G. S.; Chen, C. Y.; Yuen, L-T. Microporous Mesoporous Mater. 1998, 21, 199-211.
27. Caullet, P.; Guth, J. L.; Hazm, J.; Lamblin, J. M.; Gies, H. Eur. J. Solid State Inorg. Chem. 1991, 28, 345-361.
28. Brunner, G. O.; Meier, W. M. Nature 1989, 337, 146-147.
29. Cheetham, A.; Fjellvag, H.; Gier, T. E.; Kongshaug, K. O.; Lillerud, K. P.; Stucky, G. D. Stud. Surf. Sci. Catal. 2001, 63 (135), 788-795.
30. Annen, M. J.; Davis, M. E. Microporous Mater. 1993, 1, 1.
31. Rohrig, C.; Gies, H. Angew. Chem., Int. Ed. 1995, 34, 63-65.
32. Sastre, G.; Vidal-Moya, J. A.; Blasco, T.; Ruis, J.; Lorda, J. L.; Navarro, M. T.; Rey, F.; Corma, A. Angew. Chem., Int. Ed. 2002, 41, 4722-26.
33. Corma, A.; Diaz-Cabanas, M. J.; Jorda, J. L.; Martinez, C.; Moliner, M. Nature 2006 443, 842-845.
34. Ohsuna, T.; Terasaki, O.; Nakagawa, Y.; Zones, S. I.; Hiraga, K. J. Phys. Chem. B 1997, 101, 9881-85.
35. Njo, S. L.; Koegler, J. H.; von Koningsveld, H.; van De Graaf, B. Microporous Mater. 1997, 8, 223.
36. Wagner, P.; Zones, S. I.; Medrud, R. C.; Davis, M. E. Angew. Chem., Int. Ed. 1999, 38, 1269.
37. Nakagawa, Y. U.S. Patent 5 268 161, 1993, and refs 2 and 23 herein.
38. Zones, S. I.; Hwang, S-J. Microporous Mesoporous Mater. 2003, 58, 263-27.
39. Corma, A.; Diaz-Cabanas, M. J.; Fornes, V. Angew. Chem., Int. Ed. 2000, 39, 2346-49.
40. (a) Sastre, G.; Cantin, A.; Diaz-Cabanas, M. J.; Corma, A. Chem. Mater. 2005, 17 (3), 545-552.
41. (b) Villaescusa, L. A.; Barrett, P. A.; Camblor, M. A. Angew. Chem., Int Ed. 1999, 38, 1997.
42. Camblor, M. A.; Diaz-Cabanas, M. J.; Perez-Pariente, J.; Teat, S. J.; Clegg, W.; Shannon, I. J.; Lightfoot, P.; Wright, P. A.; Morris, R. E. Angew. Chem., Int. Ed. 1998, 37, 2122.
43. Attfield, M. P.; Catlow, C. R. A.; Sokol, A. A. Chem. Mater. 2001, 13, 4708.
44. Fyfe, C. A.; Brouwer, D. H.; Lewis, A. R.; Villaescusa, L. A.; Morris, R. E. J. Am. Chem. Soc. 2002, 124, 7770-7778.
45. Harbuzaru, B.; Roux, M.; Paillaud, J. L.; Porcher, F.; Marichal, C.; Chezeau, J. M.; Patarin, J. Chem. Lett. 2002, 616-617.
46. Tamao, K.; Hayashi, T.; Ito, Y.; Shiro, M. Organometallics 1992, 11, 2099.
47. Burton, A. W.; Darton R. J.; Davis M. E.; Morris, R. E.; Ogino, I.; Zones, S. I. J. Phys. Chem. B 2006, 110, 5273-78.
48. Fyfe, C. A.; Brouwer, D. H.; Lewis, A. R.; Villaescusa, L. A.; Morris, R. E. J. Am. Chem. Soc. 2002, 124, 7770.
49. Lobo, R. F.; Tsapatsis, M.; Freyhardt, C. C.; Chan, I. Y.; Chen, C. Y.; Zones, S. I.; Davis, M. E. J. Am. Chem. Soc. 1997, 119, 3732.
50. Piccione, P. M.; Yang, S.; Navrotsky, A.; Davis, M. E. J. Phys. Chem. B 2002, 106, 3629-38.
51. Burton, A. W. In Introduction to Zeolite Science and Practice; van Bekkum, H., Cejka, J., Corma, A., Schuth, F., Eds.; Studies in Surface Science and Catalysis Series; in press, 2007.