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Volumn 9, Issue 15, 2007, Pages 2903-2906

Tetrakis(4-pyridyl)methane: Synthesis, properties, and a diamondoid network structure of its silver(I) complex

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EID: 34547215305     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol071189n     Document Type: Article
Times cited : (31)

References (34)
  • 2
    • 85183325569 scopus 로고    scopus 로고
    • Kitagawa, S.; Noro, S. In Comprehensive Coordination Chemistry II; MeCleverty, J. A., Meyer, T. J., Eds; Elsevier: Oxford, England, 2004; 7, p 231.
    • (b) Kitagawa, S.; Noro, S. In Comprehensive Coordination Chemistry II; MeCleverty, J. A., Meyer, T. J., Eds; Elsevier: Oxford, England, 2004; Vol. 7, p 231.
  • 17
    • 9444269229 scopus 로고    scopus 로고
    • Matsumoto, K.; Kannami, M.; Oda, M. Chem. Lett. 2004, 33, 1096. See also:
    • (a) Matsumoto, K.; Kannami, M.; Oda, M. Chem. Lett. 2004, 33, 1096. See also:
  • 22
    • 0034812878 scopus 로고    scopus 로고
    • Kim, J.; Chen, B.; Reineke, T. M.; Li, H.; Eddaoudi, M.; Moler, D. B.; O'Keeffe, M.; Yaghi, O. M. J. Am. Chem. Soc. 2001, 123, 8239. See also:
    • (c) Kim, J.; Chen, B.; Reineke, T. M.; Li, H.; Eddaoudi, M.; Moler, D. B.; O'Keeffe, M.; Yaghi, O. M. J. Am. Chem. Soc. 2001, 123, 8239. See also:
  • 25
    • 34547145289 scopus 로고    scopus 로고
    • Spectroscopic data for 2: mp 293-294°C; MS (EI) m/z (rel intensity) 324 (M, 60, 246, M, C5H4N, 100, 168, M, 2(C5H4N, 14, 1H NMR (270 MHz, CDCl3) δ/ppm 8.61 (dd, J, 4.6, 1.6 Hz, 8H, 7.08 (dd, J, 4.6, 1.6 Hz, 8H, 13C NMR (67.8 MHz, CDCl3) δ/ppm 150.9, 150.0, 124.9, 63.6. Anal. Calcd for C 21H16N4: C, 77.76; H, 4.97; N, 17.27. Found: C, 77.39; H, 4.97; N, 17.17
    • 4: C, 77.76; H, 4.97; N, 17.27. Found: C, 77.39; H, 4.97; N, 17.17.
  • 30
    • 34547225112 scopus 로고    scopus 로고
    • -3, T = 200 K, of the 7980 reflections which were collected, 3661 were unique used in refinement. R1 = 0.044 (2418 data, I > 2σ(I)), wR2 = 0.122 (all data), GOF = 0.90.
    • -3, T = 200 K, of the 7980 reflections which were collected, 3661 were unique used in refinement. R1 = 0.044 (2418 data, I > 2σ(I)), wR2 = 0.122 (all data), GOF = 0.90.
  • 31
    • 34547191198 scopus 로고    scopus 로고
    • We obtained a single crystal of 1, which showed the higher crystal system (tetragonal) than that reported in ref 3 after we published it. This bond length is referred to the data of the tetragonal crystal of 1.
    • We obtained a single crystal of 1, which showed the higher crystal system (tetragonal) than that reported in ref 3 after we published it. This bond length is referred to the data of the tetragonal crystal of 1.
  • 33
    • 34547235105 scopus 로고    scopus 로고
    • -3, T = 200 K, of the 31 541 reflections which were collected, 7735 were unique used in refinement. R1 = 0.132 (7735 data, I > 2σ(I)), wR2 = 0.400 (all data), GOF = 1.08.
    • -3, T = 200 K, of the 31 541 reflections which were collected, 7735 were unique used in refinement. R1 = 0.132 (7735 data, I > 2σ(I)), wR2 = 0.400 (all data), GOF = 1.08.


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