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4 gave low yields of the coupling product.
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note
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We thank Dr André DeCian for his assistance with the analysis of the crystal structure (Service commun Rayons X, 4 rue Blaise Pascal 67070 Strasbourg cedex e-mail: sercomrx@chimie.u-strasbg.fr).
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note
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Crystallographic data (excluding structure factors) for structure 2b in this paper have been deposited with the Cambridge Crystallographic Data Centre (CCDC) as supplementary publication number CCDC 650915. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 lEZ, UK [fax: +44 1223 336033 or e-mail: deposit@ccdc.cam.ac.uk].
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