Powder X-ray thermodiffraction study of mirabilite and epsomite dehydration. Effects of direct IR-irradiation on samples

Analytical Chemistry

Volumn 79, Issue 12, 2007, Pages 4455-4462

  Cardell, Carolina ^a   Sánchez Navas, Antonio ^a   Olmo Reyes, F José ^a   Martín Ramos, J Daniel ^a  

^a UNIVERSITY OF GRANADA   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

EPSOMITE; IRRADIATION SENSITIVE; ISOTHERMAL DEHYDRATION; PHOTODEHYDRATION; POWDER X-RAY THERMODIFFRACTION; RADIATION STABILITY; X-RAY DIFFRACTOMETER PROTOTYPE;

AMORPHOUS MATERIALS; CHEMICAL BONDS; DEHYDRATION; DIFFRACTOMETERS; IRRADIATION; POROUS MATERIALS; RADIATION DAMAGE; REACTION KINETICS; X RAY POWDER DIFFRACTION;

SULFUR COMPOUNDS;

EPSOMITE; MAGNESIUM SULFATE; MIRABILITE; SODIUM CHLORIDE; SODIUM SULFATE; UNCLASSIFIED DRUG;

ARTICLE; COMPUTER PROGRAM; CULTURAL ANTHROPOLOGY; DESICCATION; DESTRUCTION; DEVICE; FILTER; HEATING; INFRARED RADIATION; KINETICS; POROSITY; POWDER X RAY THERMODIFFRACTION; RADIATION EXPOSURE; TEMPERATURE DEPENDENCE; WEATHERING; X RAY POWDER DIFFRACTION;

DEHYDRATION; INFRARED RAYS; KINETICS; MAGNESIUM SULFATE; SULFATES; TEMPERATURE; X-RAY DIFFRACTION;

EID: 34347263406     PISSN: 00032700     EISSN: None     Source Type: Journal    
DOI: 10.1021/ac062412h     Document Type: Article

References (50)

1. Nordhoff, S.; Ulrich, J. J. Therm. Anal. Calorim. 1999, 57, 181-192.
2. García-Guinea, J.; Abella, R.; Sánchez-Moral, S.; Benito, R.; Martín-Ramos, D. J. Sediment. Res. 2000, 70-4, 964-967.
3. Bataille, T.; Auffredis, J. P.; Louër, D. J. Mater. Chem. 2000, 10, 1707-1711.
4. Correcher, V.; García-Guinea, J.; López-Arce, P.; Gómez-Ros, J. M. Spectrochim. Acta, A 2004, 60, 1431-1438.
5. Isnard, O. J. Optoelectron. Adv. Mater. 2006. 8-2, 411-417.
6. Vaniman, D. T.; Bish, D. L.; Chipera, S. J.; Fialips, C. I.; Carey, J. W.; Feldman, W. C. Nature 2004, 43, 663-665.
7. Linnow, K.; Zeunert, A.; Steiger, M. Anal. Chem. 2006, 78, 4683-4689.
8. Wang, A.; Freeman, J. F.; Jolliff, B. L.; Arvidson, R. E. Lunar Planet. Sci. 2006, XXXVII, 2168-2169.
9. Charola, A. E. J. Am. Inst. Conserv. 2000, 39, 327-343.
10. Doehne, E. Geol. Soc. Spec. Publ. 2002, 205, 51-64.
11. Fortes, A. D. Axis 2005, 1-9, 1-28.
12. Martínez-Frias, J.; Amaral, G.; Vázquez, L. Rev. Environ. Sci. Biotechnol. 2006, 5, 219-231.
13. Mustoe, G. E. Geol. Soc. Am. Bull. 1982, 93, 108-115.
14. Smith, B. J. In Geomorphology of Desert Environments; Abrahams, A. D., Parsons, A. J., Eds.; Routledge Chapman & Hall: London, 1994.
15. McBride, E. F.; Picard, M. D. Earth Surf. Processes Landforms 2000, 25-8, 869-879.
16. Schwarz, H. J.; Roesch, H. Stud. Conserv. 1993, 38, 224-230.
17. Colston, B. J.; Watt, D. S.; Munro, H. L. J. Cultural Heritage 2001, 4, 297-307.
18. Cardell, C.; Delalieux, F.; Roumpopoulos, K.; Moropoulou, A.; Auger, F.; Van Grieken, R. Constr. Build. Mater. 2003, 17, 165-179.
19. Thaulow, N.; Sahu, S. Mater. Charact. 2004, 53, 123-127.
20. Cardell, C. Salt crystallization in calcarenites: application to the monastery of Sant Gerome, Granada (Spain); Granada University Press: Granada, 2003 (in Spanish).
21. ASTM C 88-90, Standard test method for soundness of aggregate by use of sodium sulfate or magnesium sulfate. In Annual Book of ASTM Standards 4.2; ASTM International: West Conshohocken, PA 1997; pp 37-42.
22. RILEM PEM/25. Mater. Constr. 1980, 17, 216-220.
23. Hamad, S. El D. Thermochim. Acta 1975, 13, 409-418.
24. Hamad, S. El D. Thermochim. Acta 1976, 17, 85-96.
25. Arnold, A.; Zehnder, K. In Atti 1° Simposio Intenationale La conservazione dei monumenti nel bacino del Mediterraneo; influenza dell'ambiente costiero e dello spray marino sulla pietra calcarea e sul marmo; Zezza, F., Ed.; Bari, 1989; pp 31-58.
26. López-Arce, P.; Doehne, E. In Proceeding of Heritage, Weathering and Conservation; Fort, R., Alvarez de Buergo, M., Gómez-Heras, M., Vazquez-Calvo, C. Eds.; Madrid, 2006; pp 285-291.
27. Siedel, H. In Proceeding of the 6th International Congress on Applied Mineralogy; Heimann, R. B.: Göttingen, 2000; Vol. 2, pp 1035-1038.
28. Price, C. A.; Brimblecombe, P. In Preventive Conservation: Practice, Theory and Research; Roy, A., Smith, P., Eds.; International Institute for Conservation of Historic and Artistic Works: London, 1994
29. Price, C. A. An expert chemical model for determining the environmental conditions needed to prevent salt damage in porous materials. European Commission Research Report 11, Protection and Conservation of European Cultural Heritage: London, 2000.
30. McCord, T. B.; Orlando, T. M.; Teeter, G.; Hansen, G. B.; Sieger, M. T.; Oetrik, N. G.; Van Keulen, L. J. Geophys. Res. 2001, 106-E2, 3311-3319.
31. Swann, J. Guidelines for Costume; ICOM Costume Committee, 1998; http:dept.kent.edu/museum/link/icom.html.
32. Brimblecombe, P. In Cultural Heritage Conservation and Environmental Impact Assesment by non-destructive testing and micro-analysis; Van Grieken, R., Janssens, K., Eds.; Balkema, A. A. Publishers: Leiden, 2005; pp 11-18.
33. Martín-Ramos, J. D. Using XPowder: A software package for Powder X-Ray diffraction analysis. www.xpowder.com D.L.; 2004 (GR 1001/04.ISBN 84-609-1497-6).
34. Winkler, E. M. Stone: Properties, durability in man's environment, 3rd ed.; Springer-Verlag: Berlin, 1997.
35. Naruse, H.; Tanak, K.; Morikawa, H.; Marumo, F. Acta Crystallogr., B 1987, 43, 143-146.
36. Rasmussen, S. E.; Jørgense, J. E.; Lundtoft, B. J. Appl. Cryst. 1996, 29, 42-47.
37. Winkler, E. M.; Singer, P. C. Geol. Soc. Am. Bull. 1972, 83, 3509-3514.
38. Sperling, C. B.; Cooke, R. V. Earth Surf. Processes Landforms 1985, 10, 541-555.
39. Charola, A. E.; Weber, J. In Proceedings of the 7th International Congress on Deterioration and Conservation of Stone; Delgado Rodríguez, J., Henriquez, F., Jeremias, J. T., Eds.; Laboratorio Nacional de Engenharia Civil: Lisbon, 1992; Vol. 2, pp 581-590.
40. Benavente, D.; García del Cura, M. A.; García-Guinea, J.; Sánchez-Moral, S.; Ordóñez, S. J. Cryst. Growth 2004, 260, 532-544.
41. Huguenin, R.; Prim, R. G.; Maderazzo, M. Icarus 1977, 32, 270-298.
42. Yen, A. S.; Gellert, R.; Schroeder, C.; et al. Nature 2005, 436, 49-54.
43. Rodríguez-Navarro, C.; Doehne, E. Earth Surf. Processes Landforms 1999, 24, 191-209.
44. Golcalves, T. D.; Rodrigues, J. D.; Abreu, N. H. J. Cult. Heritage 2006, 7 (3), 193-200.
45. Gutmann, V. The donor-acceptor approach to molecular interactions; Plenum Press: New York, 1978.
46. Jensen, W. B. The Lewis Acid-Base Concepts: An Overview; John Wiley & Sons: New York, 1980
47. Levy, H.; Lisensky, G. C. Acta Crystallogr, B 1978, 34, 3502-3510.
48. Baur, W. H. Acta Crystallogr. 1964, 17, 1361-1369.
49. CRC Handbook of Chemistry and Physics; CRC Press: Boca Raton, FL, 2005.
50. Tossell, J. A.; Vaughan, D. J. Theoretical Geochemistry: Applications of quantum Mechanics in the Earth and Mineral Sciences; Oxford University Press: Oxford, 1992.