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Crystal Growth and Design

Volumn 7, Issue 6, 2007, Pages 1038-1041

A novel supramolecular assembly constructed by cu/imidazole complex with 1,2-alternate p-sulfonatothiacalix[4]arene

(2) Guo, Dong Sheng a Liu, Yu a

a NANKAI UNIVERSITY (China)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 34347204537 PISSN: 15287483 EISSN: None Source Type: Journal
DOI: 10.1021/cg0700014 Document Type: Article

Times cited : (17)

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- 2O (148.2 mg, 0.4 mmol) and then imidazole (136.2 mg, 2.0 mmol). After being heated for a moment, the brown solution was allowed to stand for several hours. The crystalline compound suitable for X-ray structural analysis was then obtained as brown blocks with a yield of 72.8 mg (35%).
- 2O (148.2 mg, 0.4 mmol) and then imidazole (136.2 mg, 2.0 mmol). After being heated for a moment, the brown solution was allowed to stand for several hours. The crystalline compound suitable for X-ray structural analysis was then obtained as brown blocks with a yield of 72.8 mg (35%).

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- The X-ray intensity data for compound 1 were collected on a standard Siemens SMART CCD area detector system equipped with a normal-focus molybdenum-target X-ray tube (λ, 0.71073 Å) operated at 2.0 kW (50 kV, 40 mA) and a graphite monochromator at T, 293-(2) K. The structure was solved by using direct methods and refined employing full-matrix least squares on F2 (Siemens, SHELXTL-97, Crystal data for 1: C60H 78Cu4N24O27S8, M r, 2078.10, triclinic, space group P1̄, a, 11.426(4) Å, b= 13.704(4) Å, c, 14.625(5) Å, α, 110.958(5)°, β, 94.824(5)°, γ, 93.252(6)°, Z, 1, V, 2121.6-(11) Å3, Dc, 1.626 g/cm3, μ, 1.276 mm-1, Θmax, 26.44°, F(000, 1066, crystal dimensions 0.30 × 0.25 × 0.20 mm3, reflections collected/unique, 12187/8576 R
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