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C19H19NO (277.35, crystal size 0.30 × 0.20 × 0.20 mm3, triclinic, a, 995.10(9, b, 1076.39(11, c, 1495.42(14) pm, α, 100.884(8, β, 96.444(8, γ, 106.121(8)°, V, 1.4879(2) nm3; Z, 4, space group P1, T, 133(2) K. ρ, 1.238 Mgm3, absorption coefficient, 0.076 mm -1. F0, 592, θ range for data collection, 2.02-24.61°, reflections collected, 20297, Rint, 4996 (0.1158, data/restraints/paramaters, 4996/0/380, GOF on F2, 0.825, final R indices [I > 2σa(I, R1, 0.0520, wR2, 0.0754, R indices (all data, R1, 0.1313. wR2, 0.0910, largest diff. peak and hole, 0.192 and -0.203 eÅ-3. CCDC-286026 (23c) contains the supplementary cristallographie data (excluding structure factors) for this paper. These data can be obtained free of charge from the Cambridge Cristallographie Data Centre, 12 Union Road. Cambrid
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-3. CCDC-286026 (23c) contains the supplementary cristallographie data (excluding structure factors) for this paper. These data can be obtained free of charge from the Cambridge Cristallographie Data Centre, 12 Union Road. Cambridge CB2 1EZ. UK (fax: (+44) 1223-336-033; e-mail: deposit@ccdc.cam.ac.uk) or at www.ccdc.cam.ac.uk/data_request.ci f.
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