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Angewandte Chemie - International Edition

Volumn 46, Issue 16, 2007, Pages 2869-2874

Monocapped trigonal-prismatic transition-metal heptaazides: Syntheses, properties, and structures of [Nb(N3)7]2- and [Ta(N3)7]2-

(4) Haiges, Ralf a Boatz, Jerry A b Yousufuddin, Muhammed a Christe, Karl O a

a UNIVERSITY OF SOUTHERN CALIFORNIA (United States)

b AIR FORCE RESEARCH LABORATORY (United States)

Author keywords

Azides; Niobium; Tantalum; Vibrational spectroscopy; X ray diffraction

Indexed keywords

MOLECULAR STRUCTURE; NEGATIVE IONS; NIOBIUM; SYNTHESIS (CHEMICAL); TANTALUM; VIBRATIONAL SPECTROSCOPY; X RAY DIFFRACTION;

HEPTAAZIDO ANIONS; PENTAGONAL-BIPYRAMIDAL ACTINIDE TRIANION; TRIGONAL-PRISMATIC STRUCTURES;

TRANSITION METALS;

EID: 34250813657 PISSN: 14337851 EISSN: None Source Type: Journal
DOI: 10.1002/anie.200604520 Document Type: Article

Times cited : (42)

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- Crystal data for C50H43N22NbP 2: Mr, 1106.91, triclinic, space group P1, a, 10.767(1, b, 11.229(1, c, 24.053(2) Å, α, 83.196(2, β, 81.576(2, γ, 61.545(1)°, V, 2525.2(4) Å3, F-(000, 1136, ρcalcd, 1.456 gc m-3, Z, 2, μ, 0363 mm-1, crystal size 0.32 x 0.25 x 0.09 mm3, θ range 1.71 to 27.45°, index ranges -13 ≤ h ≤ 13, 14 ≤ k ≤ 10, 25 ≤ l ≤ 31, MoKα (λ, 0.71073 Å, T, 133(2) K, 15 500 measured data (Bruker 3-circle, SMART APEX CCD with χ axis fixed at 54.74°, using the SMART V 5.625 program, Bruker AXS: Madison, WI, 2001, of which 10 839 (Rint, 0.0275) unique. Lorentz and polarization correction SAINT V 6.22 program, Bruker AXS: Madi
- 2 = 1.024. CCDC-269626 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from the Cambridge Crystallographic Data Centre via http://www.ccdc.cam.ac.uk/ data_request/cif.

50
- 34250837787
- Crystal data for C50H43N22P 2Ta: Mr, 1194.95, triclinic, space group P1, a, 10.7596(9, b, 11.243(1, c, 24.043(2) Å, α, 83.158(1, β, 81.591(1, γ, 61.617(1)°, V, 2527.3(4) Å3, F-(000, 1200, ρcalcd, 1.570 g cm-3, Z, 2, μ, 2.299 mm-1, crystal size 0.37 x 0.36 x 0.15 mm3, θ range 1.72 to 27.54°, index ranges -10 ≤ h ≤ 13, 10 ≤ k ≤ 14, 31 ≤ l ≤ 31, MoKα (A, 0.71073 Å, T, 123(2) K, 15609 measured data (Bruker 3-circle, SMART APEX CCD with x axis fixed at 54.74°, using the SMART V 5.625 program, Bruker AXS: Madison, WI, 2001, of which 10 936 (Rint, 0.0207) unique. Lorentz and polarization correction SAINT V 6.22 program, Bruker AXS: Madison, WI, 2001
- 2 = 1.041. CCDC-269627 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from the Cambridge Crystallographic Data Centre via http://www.ccdc.cam.ac.uk/data_request/cif.

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