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Angewandte Chemie - International Edition

Volumn 46, Issue 18, 2007, Pages 3346-3348

Conversion of a disilenide into a silene: Silyl-anion-substituted silene by a sila-peterson-type reaction from an sp2-type silyl anion

(3) Inoue, Shigeyoshi a Ichinohe, Masaaki a Sekiguchi, Akira a

a UNIVERSITY OF TSUKUBA (Japan)

Author keywords

Alkali metals; Peterson reaction; Silenes; Silicon; Structure elucidation

Indexed keywords

CHEMICAL BONDS; CRYSTAL STRUCTURE; DERIVATIVES; MOISTURE; REACTION KINETICS; SUBSTITUTION REACTIONS;

PETERSON REACTION; SILENES; STRUCTURE ELUCIDATION;

SILICON COMPOUNDS;

EID: 34250811447 PISSN: 14337851 EISSN: None Source Type: Journal
DOI: 10.1002/anie.200605140 Document Type: Article

Times cited : (46)

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- Crystal structure analysis of 5: The single crystals of 5 for X-ray diffraction were grown from a benzene solution. The X-ray crystallographic experiments were performed on a MacScience DIP2030 image plate diffractometer equipped with graphite-monochromatized MoKα radiation (λ, 0.71070 Å, Crystal data for 5·(C 6H6)0.5 at 120 K: C48H 96LiO3Si5, Mr, 868.64, monoclinic, space group P21/c, a, 11.6610(2, b, 22.0760(6, c, 23.6650(5) Å, β, 117.1191(10)°, V, 5422.3(2) Å3, Z, 4, Pcalcd, 1-064 gcm-3, GOF, 1.027. The final R factor was 0.0484 (Rw, 0.1418 for all data) for 10048 reflections with Io > 2σIo, The structure was solved by direct methods and refined b
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* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.