메뉴 건너뛰기




Volumn 42, Issue 5, 2007, Pages 481-490

Validation of an efficient method for the determination of pesticide residues in fruits and vegetables using ethyl acetate for extraction

Author keywords

Gas chromatography (GC); Multi residue pesticide analysis; Validation

Indexed keywords

ACETONITRILE; FRUITS; GAS CHROMATOGRAPHY; OPTIMIZATION; VEGETATION;

EID: 34250359773     PISSN: 03601234     EISSN: 15324109     Source Type: Journal    
DOI: 10.1080/19312450701392490     Document Type: Article
Times cited : (107)

References (29)
  • 1
    • 34250303546 scopus 로고    scopus 로고
    • Overview of analytical technologies available to regulatory laboratories for the determination of pesticide residues
    • Lee, P.W, Ed, Wiley & Sons: Chichester, England
    • Krynitsky, A.J.; Lehotay, S.J. Overview of analytical technologies available to regulatory laboratories for the determination of pesticide residues. In Handbook of Residue Analytical Methods for Agrochemicals; Lee, P.W., Ed.; Wiley & Sons: Chichester, England, 2002; 753-786.
    • (2002) Handbook of Residue Analytical Methods for Agrochemicals , pp. 753-786
    • Krynitsky, A.J.1    Lehotay, S.J.2
  • 2
    • 0001546070 scopus 로고
    • Rapid method for chlorinated. pesticide residues in nonfatty foods
    • Mills, P.A.; Onley, J.H.; Guither, R.A. Rapid method for chlorinated. pesticide residues in nonfatty foods. J. Assoc. Off. Anal. Chem. 1963, 46, 186-191.
    • (1963) J. Assoc. Off. Anal. Chem , vol.46 , pp. 186-191
    • Mills, P.A.1    Onley, J.H.2    Guither, R.A.3
  • 3
    • 0016550913 scopus 로고
    • Extraction and cleanup of organochlorine, organophosphate, organonitrogen, and hydrocarbon pesticides in produce for determination by gas-liquid chromatography
    • Luke, M.A.; Froberg, J.E.; Masumoto, H.T. Extraction and cleanup of organochlorine, organophosphate, organonitrogen, and hydrocarbon pesticides in produce for determination by gas-liquid chromatography. J. Assoc. Off. Anal. Chem. 1975, 58(5), 1020-1026.
    • (1975) J. Assoc. Off. Anal. Chem , vol.58 , Issue.5 , pp. 1020-1026
    • Luke, M.A.1    Froberg, J.E.2    Masumoto, H.T.3
  • 4
    • 0019305137 scopus 로고
    • Gas-chromatographic determination of pesticide residues after clean-up by gel-permeation chromatography and mini-silica gel-column chromatography. III. Communication. Clean-up of foods and feeds of vegetable and animal origin for multiresidue analysis of fat-soluble and water-soluble pesticides
    • Specht, W.; Tilkes, M. Gas-chromatographic determination of pesticide residues after clean-up by gel-permeation chromatography and mini-silica gel-column chromatography. III. Communication. Clean-up of foods and feeds of vegetable and animal origin for multiresidue analysis of fat-soluble and water-soluble pesticides. Fresenius Z. Anal. Chem. 1980, 301(4), 300-307.
    • (1980) Fresenius Z. Anal. Chem , vol.301 , Issue.4 , pp. 300-307
    • Specht, W.1    Tilkes, M.2
  • 5
    • 85178714537 scopus 로고    scopus 로고
    • Hemingway, R.J.; Aharonson, N; Greve, P.A.; Roberts, T.R.; Their, H.P. Improved cost-effective approaches to pesticide residues analysis. Pure Appl. Chem. 1984, 56(8), 1131-1152.
    • Hemingway, R.J.; Aharonson, N; Greve, P.A.; Roberts, T.R.; Their, H.P. Improved cost-effective approaches to pesticide residues analysis. Pure Appl. Chem. 1984, 56(8), 1131-1152.
  • 6
    • 0033037860 scopus 로고    scopus 로고
    • Guidelines for in-house validation of analytical methods for pesticide residues in food and animal feeds
    • Hill, A.R.; Reynolds, S.L. Guidelines for in-house validation of analytical methods for pesticide residues in food and animal feeds. Analyst 1999, 124(6), 953-958.
    • (1999) Analyst , vol.124 , Issue.6 , pp. 953-958
    • Hill, A.R.1    Reynolds, S.L.2
  • 7
    • 0003965975 scopus 로고    scopus 로고
    • Fajgelj, A, Ambrus, Á, Eds, Royal Society of Chemistry: Cambridge, England
    • Fajgelj, A., Ambrus, Á., Eds. Principles and Practices of Method Validation; Royal Society of Chemistry: Cambridge, England, 2000.
    • (2000) Principles and Practices of Method Validation
  • 8
    • 39549097135 scopus 로고    scopus 로고
    • Food and Agriculture Organization/World Health Organization FAO/WHO, Rome, Italy
    • Food and Agriculture Organization/World Health Organization FAO/WHO Guidelines on Good Laboratory Practice in Residue Analysis, CAC/GL 40-1993; Rome, Italy, 2003.
    • (2003) Guidelines on Good Laboratory Practice in Residue Analysis, CAC/GL , pp. 40-1993
  • 9
    • 33750918907 scopus 로고    scopus 로고
    • Residue analysis of 500 high priority pesticides: Better by GC-MS or LC-MS?
    • Alder, L.; Greulich, K.; Kempe, G.; Vieth, B. Residue analysis of 500 high priority pesticides: better by GC-MS or LC-MS? Mass Spectrom. Rev. 2006, 25(6), 838-865.
    • (2006) Mass Spectrom. Rev , vol.25 , Issue.6 , pp. 838-865
    • Alder, L.1    Greulich, K.2    Kempe, G.3    Vieth, B.4
  • 10
    • 0037359650 scopus 로고    scopus 로고
    • Fast and easy multiresidue method employing acetonitrile extraction/partitioning and "dispersive solid phase extraction" for the determination of pesticide residues in produce
    • Anastassiades, M.; Lehotay, S.J.; Štajnbaher, D.; Schenck, F.J. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and "dispersive solid phase extraction" for the determination of pesticide residues in produce. J. AOAC Int. 2003, 86(2), 412-431.
    • (2003) J. AOAC Int , vol.86 , Issue.2 , pp. 412-431
    • Anastassiades, M.1    Lehotay, S.J.2    Štajnbaher, D.3    Schenck, F.J.4
  • 11
    • 3142747481 scopus 로고    scopus 로고
    • Evaluation of the quick, easy, cheap, effective, rugged, and safe (QuEChERS) approach to pesticide residue analysis
    • Schenck, F.J.; Hobbs, J.E. Evaluation of the quick, easy, cheap, effective, rugged, and safe (QuEChERS) approach to pesticide residue analysis. Bull. Environ. Contam. Toxcol. 2004, 73(1), 24-30.
    • (2004) Bull. Environ. Contam. Toxcol , vol.73 , Issue.1 , pp. 24-30
    • Schenck, F.J.1    Hobbs, J.E.2
  • 12
    • 16644400972 scopus 로고    scopus 로고
    • Validation of a fast and easy method for the determination of 229 pesticides in fruits and vegetables using gas and liquid chromatography and mass spectrometric detection
    • Lehotay, S.J.; de Kok, A.; Hiemstra, M.; van Bodegraven, P. Validation of a fast and easy method for the determination of 229 pesticides in fruits and vegetables using gas and liquid chromatography and mass spectrometric detection. J. AOAC Int. 2005, 88(2), 595-614.
    • (2005) J. AOAC Int , vol.88 , Issue.2 , pp. 595-614
    • Lehotay, S.J.1    de Kok, A.2    Hiemstra, M.3    van Bodegraven, P.4
  • 13
    • 16644403077 scopus 로고    scopus 로고
    • Use of buffering and other means to improve results of problematic pesticides in a fast and easy method for residue analysis of fruits and vegetables
    • Lehotay, S.J.; Mastovska, K.; Lightfield, A.R. Use of buffering and other means to improve results of problematic pesticides in a fast and easy method for residue analysis of fruits and vegetables. J. AOAC Int. 2005, 88(2), 615-629.
    • (2005) J. AOAC Int , vol.88 , Issue.2 , pp. 615-629
    • Lehotay, S.J.1    Mastovska, K.2    Lightfield, A.R.3
  • 14
    • 16644368880 scopus 로고    scopus 로고
    • Evaluation of two fast and easy methods for pesticide residue analysis in fatty food matrices
    • Lehotay, S.J.; Mastovska, K.; Yun, S.-J. Evaluation of two fast and easy methods for pesticide residue analysis in fatty food matrices. J. AOAC Int.2005, 88(2), 630-638.
    • (2005) J. AOAC Int , vol.88 , Issue.2 , pp. 630-638
    • Lehotay, S.J.1    Mastovska, K.2    Yun, S.-J.3
  • 15
    • 34250304405 scopus 로고    scopus 로고
    • Determination of Pesticide Residues in Foods by Acetonitrile Extraction and Partitioning with Magnesium Sulfate: Collaborative Study
    • Lehotay, S.J. Determination of Pesticide Residues in Foods by Acetonitrile Extraction and Partitioning with Magnesium Sulfate: Collaborative Study. J. AOAC Int. 2007, 90, 485-520.
    • (2007) J. AOAC Int , vol.90 , pp. 485-520
    • Lehotay, S.J.1
  • 17
    • 19244368129 scopus 로고    scopus 로고
    • Evaluation of common organic solvents for gas chromatographic analysis and stability of multiclass pesticide residues
    • Mastovska, K.; Lehotay, S.J. Evaluation of common organic solvents for gas chromatographic analysis and stability of multiclass pesticide residues. J. Chromatogr. A 2004, 1040(2), 259-272.
    • (2004) J. Chromatogr. A , vol.1040 , Issue.2 , pp. 259-272
    • Mastovska, K.1    Lehotay, S.J.2
  • 18
    • 0141792778 scopus 로고    scopus 로고
    • Determination of polar organophosphorus pesticides in vegetables and fruits using liquid chromatography with tandem mass spectrometry: Selection of extraction solvent
    • Mol, H.G.J.; van Dam, R.C.J.; Steijger, O.M. Determination of polar organophosphorus pesticides in vegetables and fruits using liquid chromatography with tandem mass spectrometry: selection of extraction solvent. J. Chromatogr. A 2003, 1015, 119-127.
    • (2003) J. Chromatogr. A , vol.1015 , pp. 119-127
    • Mol, H.G.J.1    van Dam, R.C.J.2    Steijger, O.M.3
  • 19
    • 33749258859 scopus 로고    scopus 로고
    • Comparison of an acetonitrile extraction/partitioning and "dispersive solid-phase extraction" method with classical multi-residue methods for the extraction of herbicide residues in barley samples
    • Diez, C.; Traag, W.A.; Zommer, P.; Marinero, P.; Atienza, J. Comparison of an acetonitrile extraction/partitioning and "dispersive solid-phase extraction" method with classical multi-residue methods for the extraction of herbicide residues in barley samples. J. Chromatogr. A 2006, 1131, 11-23.
    • (2006) J. Chromatogr. A , vol.1131 , pp. 11-23
    • Diez, C.1    Traag, W.A.2    Zommer, P.3    Marinero, P.4    Atienza, J.5
  • 20
    • 0004335447 scopus 로고    scopus 로고
    • Estimation of significance of matrix-induced chromatographic effects
    • Fajgelj, A, Ambrus, Á, Eds, Royal Society of Chemistry: Cambridge, England
    • Soboleva, E.; Rathor, N.; Mageto, A.; Ámbrus, A. Estimation of significance of matrix-induced chromatographic effects. In Principles and Practices of Method Validation; Fajgelj, A., Ambrus, Á., Eds.; Royal Society of Chemistry: Cambridge, England, 2000; 138-156.
    • (2000) Principles and Practices of Method Validation , pp. 138-156
    • Soboleva, E.1    Rathor, N.2    Mageto, A.3    Ámbrus, A.4
  • 21
    • 34250322740 scopus 로고    scopus 로고
    • Maestroni, B.; Ghods, A.; El-Bidaoui, M.; Rathor, N.; Ton, T.; Ambrus, Á. Testing the efficiency and uncertainty of sample processing using 14C-labelled chlorpyrifos: part I. description of the methodology. In Principles and Practices of Method Validation; Fajgelj, A., Ambrus, Á., Eds.; The Royal Society of Chemistry: Cambridge, England, 2000; 49-58.
    • Maestroni, B.; Ghods, A.; El-Bidaoui, M.; Rathor, N.; Ton, T.; Ambrus, Á. Testing the efficiency and uncertainty of sample processing using 14C-labelled chlorpyrifos: part I. description of the methodology. In Principles and Practices of Method Validation; Fajgelj, A., Ambrus, Á., Eds.; The Royal Society of Chemistry: Cambridge, England, 2000; 49-58.
  • 22
    • 0009904304 scopus 로고    scopus 로고
    • Testing the efficiency and uncertainty of sample processing using 14C-labelled chlorpyrifos: Part II
    • Fajgelj, A, Ambrus, Á, Eds, The Royal Society of Chemistry: Cambridge, England
    • Maestroni, B.; Ghods, A.; El-Bidaoui, M.; Rathor, N.; Jarju, O.P.; Ton, T.; Ambrus, Á. Testing the efficiency and uncertainty of sample processing using 14C-labelled chlorpyrifos: part II. In Principles and Practices of Method Validation; Fajgelj, A., Ambrus, Á., Eds.; The Royal Society of Chemistry: Cambridge, England, 2000; 59-74.
    • (2000) Principles and Practices of Method Validation , pp. 59-74
    • Maestroni, B.1    Ghods, A.2    El-Bidaoui, M.3    Rathor, N.4    Jarju, O.P.5    Ton, T.6    Ambrus, A.7
  • 23
    • 34250350899 scopus 로고    scopus 로고
    • Performance validation of a multi-residue method for 170 pesticides in kiwifruit
    • Fajgelj, A, Ambrus, Á, Eds, The Royal Society of Chemistry: Cambridge, England
    • Holland, P.T.; Boyd, A.J.; Malcolm, C.P. Performance validation of a multi-residue method for 170 pesticides in kiwifruit. In Principles and Practices of Method Validation; Fajgelj, A., Ambrus, Á., Eds.; The Royal Society of Chemistry: Cambridge, England, 2000; 29-40.
    • (2000) Principles and Practices of Method Validation , pp. 29-40
    • Holland, P.T.1    Boyd, A.J.2    Malcolm, C.P.3
  • 24
    • 0002028539 scopus 로고
    • Column extraction of residues of several pesticides from fruits and vegetables: A simple multiresidue analysis method
    • Kadenczki, L.; Zoltan, A.; Gardi, I.; Ambrus, Á.; Gyorfi, L.; Reese, G.; Ebing, W. Column extraction of residues of several pesticides from fruits and vegetables: a simple multiresidue analysis method. J. AOAC Int. 1992, 75(1), 53-61.
    • (1992) J. AOAC Int , vol.75 , Issue.1 , pp. 53-61
    • Kadenczki, L.1    Zoltan, A.2    Gardi, I.3    Ambrus, A.4    Gyorfi, L.5    Reese, G.6    Ebing, W.7
  • 28
    • 32944471654 scopus 로고    scopus 로고
    • Estimation of sample processing uncertainty for chlorpyrifos residue in cucumber
    • Tiryaki, O.; Baysoyu, D. Estimation of sample processing uncertainty for chlorpyrifos residue in cucumber. Accred. Qual. Assur. 2006, 10, 550-553.
    • (2006) Accred. Qual. Assur , vol.10 , pp. 550-553
    • Tiryaki, O.1    Baysoyu, D.2
  • 29
    • 34250373388 scopus 로고    scopus 로고
    • - Statistics in calibration analysis
    • FAO/IAEA Training and Reference Centre for Food and Pesticide Control: Vienna, Australia
    • Miller, J.N.; Ambrus, Á. Chapter 9 - Statistics in calibration analysis (1). Manual on Basic Statistics, FAO/IAEA Training and Reference Centre for Food and Pesticide Control: Vienna, Australia 2000; 1-18.
    • (2000) Manual on Basic Statistics , pp. 1-18
    • Miller, J.N.1    Ambrus, A.2


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.