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2
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34248598121
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P. Claësson (Klason), Öfver di- och trithiocyanursyra, Bihang Till K. Svenska Vet.-Akad. Handlingar, 9(17) (1884) 21.
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9
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Kopel P., Trávníček Z., Kvítek L., Panchártková R., Biler M., Marek J., and Nádvorník M. Polyhedron 18 (1999) 1779
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34248583194
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Ainscough E.W., Brodie A.M., Coll R.K., Mair A.J.A., and Waters J.M. Inorg. Chim. Acta 214 (1993) 3069
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0001839998
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Dietrich B.L., Egbert J., Morris A.M., Wicholas M., Anderson O.P., and Miller S.M. Inorg. Chem. 44 (2005) 6476
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17644409038
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Balogh-Hergovich E., Speier G., Réglier M., Giorgi M., Kuzmann E., and Vértes A. Inorg. Chem. Commun. 8 (2005) 457
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Vértes, A.6
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26
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34248586662
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note
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3TMTA) was purchased from TCI America.
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27
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34248547896
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note
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2O). The resulting olive green suspension was stirred for 30 min. The precipitate was collected via vacuum filtration, washed with MeOH (3 × 10 mL) and dried in air. Recrystallization from hot chloroform afforded emerald green crystals (0.41 g, 81% yield). Calcd.: C 47.90, H 3.10, N 15.35 Found: C 47.63, H 3.08, N 15.24. ESI-MS: M+: 1343 (<5%); +805 (15%).
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28
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34248577826
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note
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Elemental microanalysis was performed by Robertson-Microlit (Madison, NJ). Electrospray mass spectra were obtained on a Micromass LC Platform with ESI mass analyzer at the Mass Spectrometry Laboratory at the University of Pennsylvania.
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29
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34248547895
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note
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2) is used only for calculating R-factors. (b) Molecular structures were created using Ortep 3 (version 1.08) (L.J. Farrugia, J. Appl. Cryst. 30 (1997) 556).
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30
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34248579324
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note
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2 = 0.1397 [I > 2σ(I)].
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31
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37049096497
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Addison A.W., Rao T.N., Reedijk J., van Rijn J., and Verschoor G.C. J. Chem. Soc., Dalton Trans. (1984) 1349
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33745231055
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Orpen A.G., Brammer L., Allen F.H., Kennard O., Watson D.G., and Taylor R. J. Chem. Soc., Dalton Trans. (1989) S1
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J. Chem. Soc., Dalton Trans.
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33
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0003376436
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Kopel P., Trávníček Z., Kvítek L., Biler M., Pavlíček M., and Šindelář Z. Polyhedron 18 (1999) 1779
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Kopel, P.1
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Pavlíček, M.5
Šindelář, Z.6
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34
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0034683462
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Balogh-Hergovich EA., Kaizer J., Speier G., Huttner G., and Jacobi A. Inorg. Chem. 39 (2000) 4224
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Balogh-Hergovich, EA.1
Kaizer, J.2
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Jacobi, A.5
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36
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34248512942
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note
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2 = 0.1491 [I > 2σ(I)].
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37
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37049074641
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Yamanari K., Kushi Y., Yamamoto M., Fuyuhiro A., Kaizaki S., Kawamoto T., and Kushi Y. J. Chem. Soc., Dalton Trans. (1993) 3715
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Fuyuhiro, A.4
Kaizaki, S.5
Kawamoto, T.6
Kushi, Y.7
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38
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34248572159
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note
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Electronic spectra were obtained on a Unicam UV-4 spectrophotometer. Infrared Spectra were carried out on a Thermo Nicolet Avatar 360 FT-IR equipped also with a Nicolet Smart MIRacle ATR diamond crystal accessory.
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43
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34248547894
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note
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Magnetic measurements were obtained with a Quantum Design Physical Properties Measurement System DC extraction magnetometer from 10 to 300 K at an applied field of 5000 Oe. Background corrections for the Teflon sample holder and diamagnetic components of the complex (Pascal's constants) were applied. Magnetic data was fit using MicroCal Origin 6.0. Initial estimates were obtained through quadratic extrapolation. Fitting iterations (1000 max) utilized a quasi-Newton search algorithm.
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46
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34248592945
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Tsukerblat B.S., Kuyavskaya B.Y., Belinskii M.I., Ablov A.V., Novotortsev V.M., and Kalinnikov V.T. Theor. Chim. Acta 38 (1975) 13
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Tsukerblat, B.S.1
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Ablov, A.V.4
Novotortsev, V.M.5
Kalinnikov, V.T.6
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