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Volumn 36, Issue 2, 2007, Pages 250-251

Photo-controlled electrochemical switch based on photochromic tetraazaporphyrin containing ferrocene units

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EID: 34247266677 PISSN: 03667022 EISSN: None Source Type: Journal
DOI: 10.1246/cl.2007.250 Document Type: Article

Times cited : (21)

References (30)

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- Cyclic voltammetry measurements were performed using a platinum disk working electrode, a platinum wire counter electrode, an Ag/AgCl (in a saturated NaCl solution) reference electrode, and tetrabutylammonium perchlorate (0.1M) as the electrolyte. All results were referenced against ferrocene (0.50 V vs SCE).
- Cyclic voltammetry measurements were performed using a platinum disk working electrode, a platinum wire counter electrode, an Ag/AgCl (in a saturated NaCl solution) reference electrode, and tetrabutylammonium perchlorate (0.1M) as the electrolyte. All results were referenced against ferrocene (0.50 V vs SCE).

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- Synthesis of TPF: Magnesium powder 0.12 g (5 mmol) was added to 50 mL dry n-Bu(OH) and heated to boil under argon atmosphere. At the same time, a small chip of iodine was added to initiate the formation of Mg(BuO) 2, heating was continued for 24 h. Over the time a gray suspension of Mg(BuO)2 was formed. The solution then was cooled to room temperature. 2,3-Bis(5-ferrocenylethynyl-2-methylthiophen-3-yl)maleonitrile (3) 0.34 g (0.5 mmol) was added, and the reaction mixture was further heated under reflux for 48 h. The solvent was removed by distillation and the green-black crude product was purified by column chromatography on silica gel (hexane/dichloromethane, 2:1, Yield: 69 mg (20, 1HNMR (500MHz, CDCl3, δ 2.41 (s, 24H, 4.33 (m, 56H, 4.66 (s, 16H, 7.77 (s, 8H, MALDI-TOF-MS (m/z, calcd for (C152H 104Fe8MgN8S8) 2770.09, found: 2770.14
- 8) 2770.09, found: 2770.14.

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