SCOPUS 정보 검색 플랫폼

Volumn 3, Issue 1, 2006, Pages 16-20

Efficient microwave and phosphane-free synthesis of trisubstituted olefins via heck coupling

Author keywords

Chemical library; Heck reaction; Microwave irradiation; Phosphane free procedure; Trisubstituted olefins

Indexed keywords

EID: 34247247618 PISSN: 15701786 EISSN: None Source Type: Journal
DOI: 10.2174/157017806774964549 Document Type: Article

Times cited : (7)

References (18)

1
- 34247221343
- submitted
- Collina, S.; Loddo, G.; Urbano, M.; Mamolo, M. G.; Zampieri, D.; Alcaro, S.; Gallelli, A.; Azzolina, O. Chirality, submitted.
- Chirality
- Collina, S.¹ Loddo, G.² Urbano, M.³ Mamolo, M.G.⁴ Zampieri, D.⁵ Alcaro, S.⁶ Gallelli, A.⁷ Azzolina, O.⁸

2
- 33748647785
- For reviews on the palladium-catalyzed Heck reaction, see: a
- For reviews on the palladium-catalyzed Heck reaction, see: (a) de Meijere, A.; Meyer, F. Angew. Chem. Int. Ed. 1994, 33, 2379;
- (1994) Angew. Chem. Int. Ed , vol.33 , pp. 2379
- de Meijere, A.¹ Meyer, F.²

3
- 0034249671
- (b) Beletskaya, I.; Cheprakov, A. Chem. Rev. 2000, 100, 3009;
- (2000) Chem. Rev , vol.100 , pp. 3009
- Beletskaya, I.¹ Cheprakov, A.²

4
- 34247266418
- Withcombe, N.; Hii (Mimi) K. K.; Gibson, S. Tetrahedron 2001, 57, 7449;
- (c) Withcombe, N.; Hii (Mimi) K. K.; Gibson, S. Tetrahedron 2001, 57, 7449;

5
- 0037112673
- (d) Littke, A.; Fu, G. Angew. Chem. Int. Ed. 2002, 41, 4176.
- (2002) Angew. Chem. Int. Ed , vol.41 , pp. 4176
- Littke, A.¹ Fu, G.²

6
- 0001551649
- Charette, A. B.; Boezio, A. A.; Janes, M. K. Org. Lett. 2000, 2, 3777;
- (2000) Org. Lett , vol.2 , pp. 3777
- Charette, A.B.¹ Boezio, A.A.² Janes, M.K.³

7
- 0035859339
- Lipshutz, B. H.; Blomgren, P. A. Org. Lett. 2001, 3, 1869.
- (2001) Org. Lett , vol.3 , pp. 1869
- Lipshutz, B.H.¹ Blomgren, P.A.²

8
- 37049111808
- Jeffery, T. J. Chem. Soc. Chem. Commun. 1984, 1287.
- (1984) J. Chem. Soc. Chem. Commun , pp. 1287
- Jeffery, T.¹

9
- 85078684394
- Gurtler, C.; Buchwald S.L. Chem Eur. J. 1999, 5, 3107.
- (1999) Chem Eur. J , vol.5 , pp. 3107
- Gurtler, C.¹ Buchwald, S.L.²

10
- 8144223301
- Collina, S.; Loddo, G.; Barbieri, A.; Linati, L.; Alcaro, S.; Cimenti, P.; Azzolina, O. Tetrahedron: Asymmetry 2004, 15, 3601.
- (2004) Tetrahedron: Asymmetry , vol.15 , pp. 3601
- Collina, S.¹ Loddo, G.² Barbieri, A.³ Linati, L.⁴ Alcaro, S.⁵ Cimenti, P.⁶ Azzolina, O.⁷

11
- 11144325118
- Kappe, C. O. Angew. Chem. Int. Ed. 2004, 43, 6250.
- (2004) Angew. Chem. Int. Ed , vol.43 , pp. 6250
- Kappe, C.O.¹

12
- 34247206353
- (a) Xingang, L.; Chen, B.; Han, J.; She, X.; Pan, X. Tetrahedron Letters 2004, 24, 809;
- (2004) Tetrahedron Letters , vol.24 , pp. 809
- Xingang, L.¹ Chen, B.² Han, J.³ She, X.⁴ Pan, X.⁵

13
- 34247215412
- (b) Villemin, D.; Nechab, B. JCR, 2000, 429.
- (2000) JCR , pp. 429
- Villemin, D.¹ Nechab, B.²

14
- 0000153468
- Larhed, M.; Hallberg, A. J. Org.Chem. 1996, 61, 9582.
- (1996) Org.Chem , vol.61 , pp. 9582
- Larhed, M.¹ Hallberg, A.J.²

15
- 34247189972
- 2O; [C] analysis (HPLC and GC-MS).
- 2O; [C] analysis (HPLC and GC-MS).

16
- 34247280077
- Column: Chrompack SI-60 (4.6 ×150 mm), eluent: 95/5 hexane/ethyl acetate (v/v), flow rate: 1 mL/min, UV detector 275 nm.
- Column: Chrompack SI-60 (4.6 ×150 mm), eluent: 95/5 hexane/ethyl acetate (v/v), flow rate: 1 mL/min, UV detector 275 nm.

17
- 34247264178
- ITS-Finnigan Mat ion trap GC-MS system; RTX5-MS capillary column, 30 m × 0.25 mm i.d. and 0.25 μm film thickness; carrier: He, flow rate 1.2 mL/min; injector temperature 220°C, injection: split with ratio 1:5; temperature program: 100°C, 10°C/min up to 250°C, 15 min isotherm.
- ITS-Finnigan Mat ion trap GC-MS system; RTX5-MS capillary column, 30 m × 0.25 mm i.d. and 0.25 μm film thickness; carrier: He, flow rate 1.2 mL/min; injector temperature 220°C, injection: split with ratio 1:5; temperature program: 100°C, 10°C/min up to 250°C, 15 min isotherm.

18
- 34247249673
- Flash chromatography: n-hexane/ethyl acetate 9:1 v/v. Physical data for new selected compounds. 1: IR (neat; cm-1) 3050-3020, 2978, 1705, 1624, 1174, 836, 773. 1H-NMR (CDCl3, TMS as internal reference, 400 MHz) δ: 7.76-7.68 (m, 4H, 7.61-7.56 (m, 2H, 7.54-7.49 (m, 2H, 7.43-7.36 (m, 1H, 6.12 (s, 1H, 3.82 (s, 3H, 2.61 (s, 3H, Anal. calcd for C17H16O2: C, 80.93; H, 6.39. Found: C, 80.94; H, 6.41. 2: IR (neat; cm-1) 3055-3040, 2980-2897, 1736, 1623, 1163, 743, 699. 1H-NMR (CDCl3, TMS as internal reference, 400 MHz) δ: 7.74-7.72 (m, 3H, 7.68-7.65 (m, 3H, 7.63-7.61 (m, 3H, 6.03 (q, 1H, J, 0.90 Hz, 3.77 (s, 3H, 2.11 (d, 3H, J, 0.90 Hz, Anal. calcd for C17H16O2: C, 80.93; H, 6.39. Found: C, 83.02; H, 6.41. 5: IR (neat; cm-1) 3007, 2949, 1711, 1603, 1251, 1166, 855, 746. 1H-NMR CDCl
- 3: C, 69.12; H, 5.39; N, 5.76. Found: C, 68.02; H. 5.35; N, 5.74.

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