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33846983115
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X-ray data for 1: Monoclinic, P21/c, a, 12.826(3, b, 14.413(3, c, 14.939(3) Å, β, 111.948(3)°, V, 2561.5(9) Å3, Z, 4, dcalcd, 1.460 g/cm3, R1 (I > 2σ(I, 0.0603, wR2 (I > 2σ(I, 0.1773. For 2: P21/c, a, 12.8545(18) Å, b, 14.052(2, 11) Å, c, 14.440(2) Å, β, 110.881-(2)°, V, 2436.9(6) Å3, Z, 4, dcalcd, 1.419 g/cm 3, R1 (I > 2σ(I, 0.0512, wR2 (I > 2σ(I, 0.1353. For 3: Monoclinic, P21/c, a, 13.045-(2) Å, b, 14.520(2) Å, c, 14.917(2) Å, β, 112.884(2)°, V, 2603.1-(7) Å
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2 (I > 2σ(I)) = 0.1911.
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22
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0037127094
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Barthelet, K.; Marrot, J.; Riou, D.; Férey, G. Angew. Chem., Int. Ed. 2002, 41, 281.
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Barthelet, K.1
Marrot, J.2
Riou, D.3
Férey, G.4
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